In order to find an effective and environmentally friendly method to fix compressive deformation of wood, we determined or measured the recovery ratio, surface hardness, modulus of elasticity （MOE） and the modulus o...In order to find an effective and environmentally friendly method to fix compressive deformation of wood, we determined or measured the recovery ratio, surface hardness, modulus of elasticity （MOE） and the modulus of rupture （MOR） of poplar （Populus cathayana Rehd.） samples pretreated by 40-60% glycerin solutions and then compressed at 160℃ for 10-120 min. We analyzed the data statistically by using two-factor analysis of variance. The chemical compositions of thermal treated wood were also analyzed and compared with untreated control samples. The results showed that the compressive deformation of wood can be properly fixed by glycerin pretreatment. The recovery ratio of compressed wood decreased with prolonging compression time and increasing concent-ration of the glycerin solution. However, the mechanical properties of compressed wood decreased after a long time of compression. The optimal fixation of compressive deformation is to pretreat the wood by a solution of 50% glycerin and compression at 160℃ for 60 min. The analysis of chemical composition showed that glycerin displayed an accelerating effect on degradation of hemicelluloses and lignin during heat-treatment, which explains the main reason of the effect of acceleration of glycerin on deformation fixation of compressed wood.展开更多
Influence of severe cold deformation of titanium alloy Ti-1.5%A1-6.8%Mo-4.5%Fe in metastable β condition on the evolution of phase composition, microstructure, and tensile properties during continuous rapid heating w...Influence of severe cold deformation of titanium alloy Ti-1.5%A1-6.8%Mo-4.5%Fe in metastable β condition on the evolution of phase composition, microstructure, and tensile properties during continuous rapid heating was studied. As-deformed alloy was characterized by quasi-amorphous single-phase β condition with an abnormal temperature dependence of electric resistance that was normalized after 48 h exposure at room temperature as a result of isothermal ω phase precipitation. Subsequent rapid heating with a rate of 5 ℃/s caused recovery and recrystallization. Tensile properties of the alloy after different treatments were determined and discussed.展开更多
The independently designed and manufactured ultra-high-strength aluminum alloy Al-12.18 Zn-3.31 Mg-1.43 Cu-0.20 Zr-0.04 Sr was investigated via scanning electron microscopy observations, X-ray diffraction analysis, ha...The independently designed and manufactured ultra-high-strength aluminum alloy Al-12.18 Zn-3.31 Mg-1.43 Cu-0.20 Zr-0.04 Sr was investigated via scanning electron microscopy observations, X-ray diffraction analysis, hardness tests, electrical conductivity tests, tensile tests, intergranular corrosion tests, and exfoliation corrosion tests. The effect of pre-recovery on the microstructure and mechanical properties of this aluminum alloy was also studied. The results show that the pre-recovery heat treatment releases deformation energy, inhibits recrystallization, and decreases the dislocation density. Although the pre-recovery heat treatment has little effect on the hardness, electrical conductivity, and elongation of this aluminum alloy, it can dramatically improve the alloy's tensile strength(the maximum tensile strength increased from 785.0 MPa to 809.2 MPa). Moreover, the tensile properties of this aluminum alloy have a certain degree of isotropy, and the pre-recovery heat treatment does not affect this property. In addition, the rolled aluminum alloy exhibits good corrosion resistance, but the effect of the pre-recovery heat treatment on the alloy's resistance to intergranular and exfoliation corrosion is negligible.展开更多
The high temperature mechanical properties(250 ℃) and microstructure of a die-forged Al-5.87 Zn-2.07 Mg-2.42 Cu alloy after T6 heat treatment were investigated. High temperature tensile tests show that as the tempera...The high temperature mechanical properties(250 ℃) and microstructure of a die-forged Al-5.87 Zn-2.07 Mg-2.42 Cu alloy after T6 heat treatment were investigated. High temperature tensile tests show that as the temperature increases from room temperature to 250 ℃, the ultimate tensile strength of the alloy decreases from 638 to 304 MPa, and the elongation rises from 13.6% to 20.4%. Transmission electron microscopy(TEM) and electron backscattered diffraction(EBSD) were applied for microstructure characterization, which indicates that the increase of tensile temperature can lead to the coarsening of precipitates, drop of dislocation density, and increase of dynamic recovery. After tensile testing at 250 ℃, a sub-grain structure composed of a high fraction of small-angle grain boundary is formed.展开更多
In this paper, the authors aim to propose the use of waste plastics as a binder in a coconut shell reinforcement for the development of an 8/6 size composite rafter to replace the natural 8/6 size backbone in construc...In this paper, the authors aim to propose the use of waste plastics as a binder in a coconut shell reinforcement for the development of an 8/6 size composite rafter to replace the natural 8/6 size backbone in construction. Following a study into the choice of the best proportions, a total of 30 size 8/6 composite rafters with different proportions of 20%, 25%, 30%, 35%, 40% and 50% plastic content were developed. All the 8/6 composite rafters were subjected to mechanical (3-point bending strength and Monnin hardness) and physical (bulk density and water absorption) characterization analyses. The results show that flexural strength increases from 27.56 MPa to 33.30 MPa for proportions ranging from 20% to 35% plastic content. Above 35% plastic, the strength drops to 19.60 MPa for a 50% plastic content. Similarly, the Monnin hardness drops from 9 mm to 5 mm when the plastic content varies from 20 to 50%. As for the results of the physical characterisation, the values obtained for apparent density vary from 0.89 to 1 for proportions varying from 20% to 35% plastic content and drop to 0.94 for 50% plastic content. As for water absorption, values drop from 6.82% to 2.45% when the plastic content increases from 20% to 50%. These mechanical strengths stabilise at 35% plastic content. The development of an 8/6 chevron composite material based on plastic and coconut shell could therefore be a way of recovering waste and solving the problem of deforestation.展开更多
The microstructure and mechanical properties of 105 mm thick 5083 aluminum alloy hot rolled plate were investigated by metallurgical microscope, scanning electron microscope and tensile testing machine, and three majo...The microstructure and mechanical properties of 105 mm thick 5083 aluminum alloy hot rolled plate were investigated by metallurgical microscope, scanning electron microscope and tensile testing machine, and three major characteristic problems in mechanical properties inhomogeneity were explained. The results show that the mechanical properties of the rolled plate are inhomogeneous along the thickness direction. From the surface to the center, the strength shows an inverted "N" shape change and the elongation presents a semi "U" shape change. Several similar structural units composed of long fibrous grains(LFG) and short fibrous grains bands(SFGB) exist in a special layer(Layer 2) adjacent to the surface. This alternating layered distribution of LFG and SFGB is conducive to improving the plasticity by dispersing the plastic deformation concentrated on the boundary line(BL) between them. However, their different deformability will cause the alternation of additional stresses during the hot rolling, leading to the strength reduction. The closer the location to the center of the plate is, the more likely the recovery rather than the recrystallization occurs. This is the possible reason for the unnegligible difference in strength near the central region(Layer 4 and Layer 5).展开更多
The effects of rolling driving methods and technical factors on the microstructures and mechanical properties of aluminum foils based on the industrial trials were studied by TEM, tensile test and texture analysis. Th...The effects of rolling driving methods and technical factors on the microstructures and mechanical properties of aluminum foils based on the industrial trials were studied by TEM, tensile test and texture analysis. The results show that there exist obvious dynamic recovery and primary location re crystallization phenomena in the aluminum foils during high speed rolling. Meanwhile the phenomena become more obvious as the rolling speed or the reduction increases, especially in the asymmetrical rolling process with single roller driving, the dynamic primary location recrystallization is more likely to come into being. The effects of the dynamic recovery phenomena and the dynamic primary location recrystallization on the comprehensive final product ratio and the quality of aluminum foils were discussed.展开更多
In the present work,the microstructure features,martensitic transformation,mechanical properties and strain recovery characteristics of Ti-Ta based shape memory alloys were tailored by changing Hf contents.The single...In the present work,the microstructure features,martensitic transformation,mechanical properties and strain recovery characteristics of Ti-Ta based shape memory alloys were tailored by changing Hf contents.The singleα"martensite phase was dominated in Ti-Ta alloy with 2 at.%H f.Upon Hf content exceeded2 at.%,βphase started to appear.Moreover,the amount ofβphase gradually increased with Hf content increasing.The martensitic transformation temperatures continuously decreased with the increased Hf content,which was attributed to the rising of valence electron concentration.Meanwhile,Hf addition improved the thermal cycling stability of Ti-Ta alloys due to the suppression ofωprecipitation.The yield stress of Ti-Ta based alloys firstly decreased and then increased with Hf content increasing.In addition,the completely recoverable strain of 4%can be obtained in Ti-Ta alloy with 6 at.%Hf as a consequence of the higher critical stress for dislocation slip.Besieds,the Ti-Ta based alloy containing 8 at.%Hf had the superior superelasticity behavior with the fully recoverable strain of 2%at room temperature.展开更多
基金supported by the National Natural Science Foundation of China (NSFC) (Grant No.30500386)
文摘In order to find an effective and environmentally friendly method to fix compressive deformation of wood, we determined or measured the recovery ratio, surface hardness, modulus of elasticity （MOE） and the modulus of rupture （MOR） of poplar （Populus cathayana Rehd.） samples pretreated by 40-60% glycerin solutions and then compressed at 160℃ for 10-120 min. We analyzed the data statistically by using two-factor analysis of variance. The chemical compositions of thermal treated wood were also analyzed and compared with untreated control samples. The results showed that the compressive deformation of wood can be properly fixed by glycerin pretreatment. The recovery ratio of compressed wood decreased with prolonging compression time and increasing concent-ration of the glycerin solution. However, the mechanical properties of compressed wood decreased after a long time of compression. The optimal fixation of compressive deformation is to pretreat the wood by a solution of 50% glycerin and compression at 160℃ for 60 min. The analysis of chemical composition showed that glycerin displayed an accelerating effect on degradation of hemicelluloses and lignin during heat-treatment, which explains the main reason of the effect of acceleration of glycerin on deformation fixation of compressed wood.
文摘Influence of severe cold deformation of titanium alloy Ti-1.5%A1-6.8%Mo-4.5%Fe in metastable β condition on the evolution of phase composition, microstructure, and tensile properties during continuous rapid heating was studied. As-deformed alloy was characterized by quasi-amorphous single-phase β condition with an abnormal temperature dependence of electric resistance that was normalized after 48 h exposure at room temperature as a result of isothermal ω phase precipitation. Subsequent rapid heating with a rate of 5 ℃/s caused recovery and recrystallization. Tensile properties of the alloy after different treatments were determined and discussed.
基金financially supported by the Jiangsu Provincial Industrial Science and Technology Support Program (No. BE2008118)the Basic Research on Isotropic Ultra-high Strength Aluminum Matrix Composite (No. 6140922010201)
文摘The independently designed and manufactured ultra-high-strength aluminum alloy Al-12.18 Zn-3.31 Mg-1.43 Cu-0.20 Zr-0.04 Sr was investigated via scanning electron microscopy observations, X-ray diffraction analysis, hardness tests, electrical conductivity tests, tensile tests, intergranular corrosion tests, and exfoliation corrosion tests. The effect of pre-recovery on the microstructure and mechanical properties of this aluminum alloy was also studied. The results show that the pre-recovery heat treatment releases deformation energy, inhibits recrystallization, and decreases the dislocation density. Although the pre-recovery heat treatment has little effect on the hardness, electrical conductivity, and elongation of this aluminum alloy, it can dramatically improve the alloy's tensile strength(the maximum tensile strength increased from 785.0 MPa to 809.2 MPa). Moreover, the tensile properties of this aluminum alloy have a certain degree of isotropy, and the pre-recovery heat treatment does not affect this property. In addition, the rolled aluminum alloy exhibits good corrosion resistance, but the effect of the pre-recovery heat treatment on the alloy's resistance to intergranular and exfoliation corrosion is negligible.
基金Project(220636)supported by the Postdoctoral Science Foundation of the Central South University,ChinaProject(2016B090931004)supported by the Guangdong Province Science and Research Plan,ChinaProject(51601229)supported by the National Natural Science Foundation of China。
文摘The high temperature mechanical properties(250 ℃) and microstructure of a die-forged Al-5.87 Zn-2.07 Mg-2.42 Cu alloy after T6 heat treatment were investigated. High temperature tensile tests show that as the temperature increases from room temperature to 250 ℃, the ultimate tensile strength of the alloy decreases from 638 to 304 MPa, and the elongation rises from 13.6% to 20.4%. Transmission electron microscopy(TEM) and electron backscattered diffraction(EBSD) were applied for microstructure characterization, which indicates that the increase of tensile temperature can lead to the coarsening of precipitates, drop of dislocation density, and increase of dynamic recovery. After tensile testing at 250 ℃, a sub-grain structure composed of a high fraction of small-angle grain boundary is formed.
文摘In this paper, the authors aim to propose the use of waste plastics as a binder in a coconut shell reinforcement for the development of an 8/6 size composite rafter to replace the natural 8/6 size backbone in construction. Following a study into the choice of the best proportions, a total of 30 size 8/6 composite rafters with different proportions of 20%, 25%, 30%, 35%, 40% and 50% plastic content were developed. All the 8/6 composite rafters were subjected to mechanical (3-point bending strength and Monnin hardness) and physical (bulk density and water absorption) characterization analyses. The results show that flexural strength increases from 27.56 MPa to 33.30 MPa for proportions ranging from 20% to 35% plastic content. Above 35% plastic, the strength drops to 19.60 MPa for a 50% plastic content. Similarly, the Monnin hardness drops from 9 mm to 5 mm when the plastic content varies from 20 to 50%. As for the results of the physical characterisation, the values obtained for apparent density vary from 0.89 to 1 for proportions varying from 20% to 35% plastic content and drop to 0.94 for 50% plastic content. As for water absorption, values drop from 6.82% to 2.45% when the plastic content increases from 20% to 50%. These mechanical strengths stabilise at 35% plastic content. The development of an 8/6 chevron composite material based on plastic and coconut shell could therefore be a way of recovering waste and solving the problem of deforestation.
基金Project(2011DFR50950)supported by the International Science and Technology Cooperation Program of ChinaProject(51971183)supported by the National Natural Science Foundation of ChinaProject(cstc2019jcyj-msxmX0594)supported by the Natural Science Foundation of Chongqing,China。
文摘The microstructure and mechanical properties of 105 mm thick 5083 aluminum alloy hot rolled plate were investigated by metallurgical microscope, scanning electron microscope and tensile testing machine, and three major characteristic problems in mechanical properties inhomogeneity were explained. The results show that the mechanical properties of the rolled plate are inhomogeneous along the thickness direction. From the surface to the center, the strength shows an inverted "N" shape change and the elongation presents a semi "U" shape change. Several similar structural units composed of long fibrous grains(LFG) and short fibrous grains bands(SFGB) exist in a special layer(Layer 2) adjacent to the surface. This alternating layered distribution of LFG and SFGB is conducive to improving the plasticity by dispersing the plastic deformation concentrated on the boundary line(BL) between them. However, their different deformability will cause the alternation of additional stresses during the hot rolling, leading to the strength reduction. The closer the location to the center of the plate is, the more likely the recovery rather than the recrystallization occurs. This is the possible reason for the unnegligible difference in strength near the central region(Layer 4 and Layer 5).
文摘The effects of rolling driving methods and technical factors on the microstructures and mechanical properties of aluminum foils based on the industrial trials were studied by TEM, tensile test and texture analysis. The results show that there exist obvious dynamic recovery and primary location re crystallization phenomena in the aluminum foils during high speed rolling. Meanwhile the phenomena become more obvious as the rolling speed or the reduction increases, especially in the asymmetrical rolling process with single roller driving, the dynamic primary location recrystallization is more likely to come into being. The effects of the dynamic recovery phenomena and the dynamic primary location recrystallization on the comprehensive final product ratio and the quality of aluminum foils were discussed.
基金financially supported by the National Natural Science Foundation of China(Nos.51871080,51931004 and 51571073)the Talent Training Program for Shandong Province Higher Educational Youth Innovative Teams(2019)。
文摘In the present work,the microstructure features,martensitic transformation,mechanical properties and strain recovery characteristics of Ti-Ta based shape memory alloys were tailored by changing Hf contents.The singleα"martensite phase was dominated in Ti-Ta alloy with 2 at.%H f.Upon Hf content exceeded2 at.%,βphase started to appear.Moreover,the amount ofβphase gradually increased with Hf content increasing.The martensitic transformation temperatures continuously decreased with the increased Hf content,which was attributed to the rising of valence electron concentration.Meanwhile,Hf addition improved the thermal cycling stability of Ti-Ta alloys due to the suppression ofωprecipitation.The yield stress of Ti-Ta based alloys firstly decreased and then increased with Hf content increasing.In addition,the completely recoverable strain of 4%can be obtained in Ti-Ta alloy with 6 at.%Hf as a consequence of the higher critical stress for dislocation slip.Besieds,the Ti-Ta based alloy containing 8 at.%Hf had the superior superelasticity behavior with the fully recoverable strain of 2%at room temperature.
