A temperature programmed decomposition (TPD) apparatus with metal tube structure, in which Ar is used as the carrier gas, is established and the TPD spectrum of titanium hydride is acquired. Using consulting table met...A temperature programmed decomposition (TPD) apparatus with metal tube structure, in which Ar is used as the carrier gas, is established and the TPD spectrum of titanium hydride is acquired. Using consulting table method (CTM), spectrum superposition method (SSM) and differential spectrum technique, TPD spectrum of titanium hydride is separated and a set of thermal decomposition kinetics equations are acquired. According to these equations, the relationship between decomposition quantity and time for titanium hydride at the temperature of 940 K is obtained and the result well coincides with the AI alloy melt foaming process.展开更多
In the present study, closed-cell aluminum foams with different percentages of erbium （Er） element were successfully prepared. The distribution and existence form of erbium （Er） element and its effect on the compr...In the present study, closed-cell aluminum foams with different percentages of erbium （Er） element were successfully prepared. The distribution and existence form of erbium （Er） element and its effect on the compressive properties of the foams were investigated. Results show that Er uniformly distributes in the cell walls in the forms of Al3Er intermetallic compound and AI-Er solid solutions. Compared with commercially pure aluminum foam, Er-containing foams possess higher micro-hardness, compressive strength and energy absorption capacity due to solid solution strengthening and second phase strengthening effects. Additionally, the amount of Er element should be controlled in the range of 0.10wt.%-0.50wt.% in order to obtain a good combination of compressive strength and energy absorption properties.展开更多
基金This work was supported by the National Natural Science Foundation of China(Grant Nos.50231010,50081002,90205005 and 19982001).
文摘A temperature programmed decomposition (TPD) apparatus with metal tube structure, in which Ar is used as the carrier gas, is established and the TPD spectrum of titanium hydride is acquired. Using consulting table method (CTM), spectrum superposition method (SSM) and differential spectrum technique, TPD spectrum of titanium hydride is separated and a set of thermal decomposition kinetics equations are acquired. According to these equations, the relationship between decomposition quantity and time for titanium hydride at the temperature of 940 K is obtained and the result well coincides with the AI alloy melt foaming process.
基金supported by the National Natural Science Foundation of China(No.51501053 and 51475138)Science and Technology Plan Projects of Hebei Province(No.15211026)
文摘In the present study, closed-cell aluminum foams with different percentages of erbium （Er） element were successfully prepared. The distribution and existence form of erbium （Er） element and its effect on the compressive properties of the foams were investigated. Results show that Er uniformly distributes in the cell walls in the forms of Al3Er intermetallic compound and AI-Er solid solutions. Compared with commercially pure aluminum foam, Er-containing foams possess higher micro-hardness, compressive strength and energy absorption capacity due to solid solution strengthening and second phase strengthening effects. Additionally, the amount of Er element should be controlled in the range of 0.10wt.%-0.50wt.% in order to obtain a good combination of compressive strength and energy absorption properties.
