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Research on Infrared Emissivity and Laser Reflectivity of Sn_(1−x)Er_(x)O_(2)Micro/Nanofibers Based on First-Principles 被引量:1
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作者 Yuanjia Xia Fang Zhao +2 位作者 Zhizun Li Zhaogang Cheng Jianwei Hu 《Journal of Renewable Materials》 SCIE EI 2023年第2期921-936,共16页
Sn_(1−x)Er_(x)O_(2)(x=0%,8%,16%,24%)micro/nanofibers were prepared by electrospinning combined with heat treatment using erbium nitrate,stannous chloride and polyvinylpyrrolidone(PVP)as raw materials.The target produc... Sn_(1−x)Er_(x)O_(2)(x=0%,8%,16%,24%)micro/nanofibers were prepared by electrospinning combined with heat treatment using erbium nitrate,stannous chloride and polyvinylpyrrolidone(PVP)as raw materials.The target products were characterized by thermogravimetric analyzer,X-ray diffrotometer,fourier transform infrared spectrometer,scanning electron microscope,spectrophotometer and infrared emissivity tester,and the effects of Er^(3+)doping on its infrared and laser emissivity were studied.At the same time,the Sn_(1−x)Er_(x)O_(2)(x=0%,16%)doping models were constructed based on the first principles of density functional theory,and the related optoelectronic properties such as their energy band structure,density of states,reflectivity and dielectric constant were analyzed,and further explained the mechanism of Er^(3+)doping on SnO_(2)infrared emissivity and laser absorption from the point of electronic structure.The results showed that after calcination at 600℃,single rutile type SnO_(2)was formed,and the crystal structure was not changed by doping Er^(3+).The calcined products showed good fiber morphology,and the average fiber diameter was 402 nm.The infrared emissivity and resistivity of the samples both decreased first and then increased with the increase of Er^(3+)doping amount.When x=16%,the infrared emis-sivity of the sample was at least 0.71;and Er^(3+)doping can effectively reduce the reflectivity of SnO_(2)at 1.06μm and 1.55μm,when x=16%,its reflectivity at 1.06μm and 1.55μm are 50.5%and 40%,respectively,when x=24%,the reflectivity at 1.06μm and 1.55μm wavelengths are 47.3%and 42.1%,respectively.At the same time,the change of carrier concentration and electron transition before and after Er^(3+)doping were described by first-principle calculation,and the regulation mechanism of infrared emissivity and laser reflectivity was explained.This study provides a certain experimental and theoretical basis for the development of a single-type,light-weight and easily prepared infrared and laser compatible-stealth material. 展开更多
关键词 micro/nano fibers Er^(3+)doping SnO_(2) laser and infrared compatible stealth material
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Optical Micro/Nano Fibers Enabled Smart Textiles for Human-Machine Interface 被引量:13
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作者 Shuqi Ma Xiaoyu Wang +9 位作者 Pan Li Ni Yao Jianliang Xiao Haitao Liu Zhang Zhang Longteng Yu Guangming Tao Xiong Li Limin Tong Lei Zhang 《Advanced Fiber Materials》 SCIE EI 2022年第5期1108-1117,共10页
Wearable human-machine interface(HMI)is an advanced technology that has a wide range of applications from robotics to augmented/virtual reality(AR/VR).In this study,an optically driven wearable human-interactive smart... Wearable human-machine interface(HMI)is an advanced technology that has a wide range of applications from robotics to augmented/virtual reality(AR/VR).In this study,an optically driven wearable human-interactive smart textile is proposed by integrating a polydimethylsiloxane(PDMS)patch embedded with optical micro/nanofibers(MNF)array with a piece of textiles.Enabled by the highly sensitive pressure dependent bending loss of MNF,the smart textile shows high sensitivity(65.5 kPa^(−1))and fast response(25 ms)for touch sensing.Benefiting from the warp and weft structure of the textile,the optical smart textile can feel slight finger slip along the MNF.Furthermore,machine learning is utilized to classify the touch manners,achieving a recognition accuracy as high as 98.1%.As a proof-of-concept,a remote-control robotic hand and a smart interactive doll are demonstrated based on the optical smart textile.This optical smart textile represents an ideal HMI for AR/VR and robotics applications. 展开更多
关键词 Smart textiles HUMAN-MACHINE interfaces OPTICAL micro/nano fiber TACTILE sensor Augmented/virtual REALITY Robotics
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Spectra of spontaneous Raman scattering in taper-drawn micro/nano-fibers 被引量:1
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作者 徐颖鑫 崔亮 +5 位作者 李小英 郭骋 李宇航 徐忠扬 王力军 方伟 《Chinese Physics B》 SCIE EI CAS CSCD 2016年第12期266-270,共5页
We study the spontaneous Raman scattering (RS) in taper-drawn micro/nano-fibers (MNFs) by employing the photon counting technique. The spectra of RS in five MNFs, which are fabricated by using different heating fl... We study the spontaneous Raman scattering (RS) in taper-drawn micro/nano-fibers (MNFs) by employing the photon counting technique. The spectra of RS in five MNFs, which are fabricated by using different heating flames (hydrogen flame or butane flame) and with different diameters, are measured within a frequency shift range of 1435 cm- 1_3200 cm- 1. From the measured spectra, we observe the RS peaks originated from silica and a unique RS peak with a frequency shift of - 2905 cm-1 (- 87.2 THz). Unlike the former ones, the latter one is not observable in conventional optical fibers. Furthermore, the unique peak becomes obvious and starts to rapidly increase with the decrease of the diameter of MNFs when the diameter is smaller than 2 μm, and the intensity of the unique peak significantly depends on the heating flame used in the fabricating process. Our investigation is useful for the entanglement generation or optical sensing using taper-drawn MNFs. 展开更多
关键词 nonlinear optics micro/nano-fibers Raman scattering
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On-Chip Micro Temperature Controllers Based on Freestanding Thermoelectric Nano Films for Low-Power Electronics
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作者 Qun Jin Tianxiao Guo +4 位作者 Nicolas Perez Nianjun Yang Xin Jiang Kornelius Nielsch Heiko Reith 《Nano-Micro Letters》 SCIE EI CAS CSCD 2024年第7期98-108,共11页
Multidimensional integration and multifunctional com-ponent assembly have been greatly explored in recent years to extend Moore’s Law of modern microelectronics.However,this inevitably exac-erbates the inhomogeneity ... Multidimensional integration and multifunctional com-ponent assembly have been greatly explored in recent years to extend Moore’s Law of modern microelectronics.However,this inevitably exac-erbates the inhomogeneity of temperature distribution in microsystems,making precise temperature control for electronic components extremely challenging.Herein,we report an on-chip micro temperature controller including a pair of thermoelectric legs with a total area of 50×50μm^(2),which are fabricated from dense and flat freestanding Bi2Te3-based ther-moelectric nano films deposited on a newly developed nano graphene oxide membrane substrate.Its tunable equivalent thermal resistance is controlled by electrical currents to achieve energy-efficient temperature control for low-power electronics.A large cooling temperature difference of 44.5 K at 380 K is achieved with a power consumption of only 445μW,resulting in an ultrahigh temperature control capability over 100 K mW^(-1).Moreover,an ultra-fast cooling rate exceeding 2000 K s^(-1) and excellent reliability of up to 1 million cycles are observed.Our proposed on-chip temperature controller is expected to enable further miniaturization and multifunctional integration on a single chip for microelectronics. 展开更多
关键词 Temperature control Low-power electronics On-chip micro temperature controller Freestanding thermoelectric nano films Temperature-sensitive components
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Active Micro-Nano-Collaborative Bioelectronic Device for Advanced Electrophysiological Recording
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作者 Yuting Xiang Keda Shi +7 位作者 Ying Li Jiajin Xue Zhicheng Tong Huiming Li Zhongjun Li Chong Teng Jiaru Fang Ning Hu 《Nano-Micro Letters》 SCIE EI CAS CSCD 2024年第7期244-264,共21页
The development of precise and sensitive electrophysiological recording platforms holds the utmost importance for research in the fields of cardiology and neuroscience.In recent years,active micro/nano-bioelectronic d... The development of precise and sensitive electrophysiological recording platforms holds the utmost importance for research in the fields of cardiology and neuroscience.In recent years,active micro/nano-bioelectronic devices have undergone significant advancements,thereby facilitating the study of electrophysiology.The distinctive configuration and exceptional functionality of these active micro-nano-collaborative bioelectronic devices offer the potential for the recording of high-fidelity action potential signals on a large scale.In this paper,we review three-dimensional active nano-transistors and planar active micro-transistors in terms of their applications in electroexcitable cells,focusing on the evaluation of the effects of active micro/nano-bioelectronic devices on electrophysiological signals.Looking forward to the possibilities,challenges,and wide prospects of active micro-nano-devices,we expect to advance their progress to satisfy the demands of theoretical investigations and medical implementations within the domains of cardiology and neuroscience research. 展开更多
关键词 Active micro/nano collaborative bioelectronic device Three-dimensional active nano-transistor Planar active microtransistor ELECTROPHYSIOLOGY
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Ignition processes and characteristics of charring conductive polymers with a cavity geometry in precombustion chamber for applications in micro/nano satellite hybrid rocket motors
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作者 Zhiyuan Zhang Hanyu Deng +2 位作者 Wenhe Liao Bin Yu Zai Yu 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第2期55-66,共12页
The arc ignition system based on charring polymers has advantages of simple structure,low ignition power consumption and multiple ignitions,which bringing it broadly application prospect in hybrid propulsion system of... The arc ignition system based on charring polymers has advantages of simple structure,low ignition power consumption and multiple ignitions,which bringing it broadly application prospect in hybrid propulsion system of micro/nano satellite.However,charring polymers alone need a relatively high input voltage to achieve pyrolysis and ignition,which increases the burden and cost of the power system of micro/nano satellite in practical application.Adding conductive substance into charring polymers can effectively decrease the conducting voltage which can realize low voltage and low power consumption repeated ignition of arc ignition system.In this paper,a charring conductive polymer ignition grain with a cavity geometry in precombustion chamber,which is composed of PLA and multiwall carbon nanotubes(MWCNT)was proposed.The detailed ignition processes were analyzed and two different ignition mechanisms in the cavity of charring conductive polymers were revealed.The ignition characteristics of charring conductive polymers were also investigated at different input voltages,ignition grain structures,ignition locations and injection schemes in a visual ignition combustor.The results demonstrated that the ignition delay and external energy required for ignition were inversely correlated with the voltages applied to ignition grain.Moreover,the incremental depth of cavity shortened the ignition delay and external energy required for ignition while accelerated the propagation of flame.As the depth of cavity increased from 2 to 6 mm(at 50 V),the time of flame propagating out of ignition grain changed from 235.6 to 108 ms,and values of mean ignition delay time and mean external energy required for ignition decreased from 462.8 to 320 ms and 16.2 to 10.75 J,respectively.The rear side of the cavity was the ideal ignition position which had a shorter ignition delay and a faster flame propagation speed in comparison to other ignition positions.Compared to direct injection scheme,swirling injection provided a more favorable flow field environment in the cavity,which was beneficial to ignition and initial flame propagation,but the ignition position needed to be away from the outlet of swirling injector.At last,the repeated ignition characteristic of charring conductive polymers was also investigated.The ignition delay time and external energy required for ignition decreased with repeated ignition times but the variation was decreasing gradually. 展开更多
关键词 micro/nano satellite hybrid propulsion Arc ignition Charring conductive polymer Ignition mechanism Ignition characteristic Repeated ignition
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Research on the Development of Fibroin and Nano-Fiber from Silk Cocoons for Regenerated Tissue Engineering Applications by Electro-Spinning
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作者 Md Kamrul Hasan Xinbo Ding 《Advances in Nanoparticles》 CAS 2024年第1期1-9,共9页
In this paper, the main goal is to prepare silk fibroin nano-fiber, which is used for regenerated tissue applications. Silk scaffold nano-fibers made by electro-spinning technology can be used in regenerated tissue ap... In this paper, the main goal is to prepare silk fibroin nano-fiber, which is used for regenerated tissue applications. Silk scaffold nano-fibers made by electro-spinning technology can be used in regenerated tissue applications. The purpose of the research is to prepare a silk-fibroin nano-fiber solution for potential applications in tissue engineering. Using a degumming process, pure silk fibroin protein is extracted from silk cocoons. The protein solution for fibroin is purified, and the protein content is determined. The precise chemical composition, exact temperature, time, voltage, distance, ratio, and humidity all have a huge impact on degumming, solubility, and electro-spinning nano-fibers. The SEM investigates the morphology of silk fibroin nano-fibres at different magnifications. It also reveals the surface condition, fiber orientation, and fiber thickness of the silk fibroin nano-fiber. The results show that regenerated silk fibroin and nano-fiber can be used in silk fibroin scaffolds for various tissue engineering applications. 展开更多
关键词 Silk fibroin SCAFFOLD electro-spinning nano-fiber Tissue Engineering
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Impacts of Micro- and Nano-Plastics on Soil Properties and Plant Production in Agroecosystems: A Mini-Review
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作者 Dafeng Hui Faisal Hayat +1 位作者 Muhammad Salam Prabodh Illukpitiya 《Agricultural Sciences》 2024年第10期1089-1111,共23页
Micro- and nano-plastics (MNPs) are tiny plastic particles resulting from plastic product degradation. Soil MNPs have been identified as potential influential factors affecting various soil properties and crop biomass... Micro- and nano-plastics (MNPs) are tiny plastic particles resulting from plastic product degradation. Soil MNPs have been identified as potential influential factors affecting various soil properties and crop biomass productivity. This mini-review provides a synthesis of recent findings concerning their effects on soil physicochemical properties, microorganisms, organic carbon content, soil nutrients, greenhouse gas emissions, soil fauna, and their impacts on plant ecophysiology, growth, and production. The results indicate that MNPs may markedly impede soil aggregation ability, increase porosity, decrease soil bulk density, enhance water retention capacity, influence soil pH and electrical conductivity, and escalate soil water evaporation. Exposure to MNPs may predominantly induce changes in soil microbial composition, reducing the diversity and complexity of microbial communities and microbial activity while enhancing soil organic carbon stability, influencing soil nutrient dynamics, and stimulating organic carbon decomposition and denitrification processes, leading to elevated soil respiration and methane emissions, and potentially decreasing soil nitrous oxide emission. Additionally, MNPs may adversely affect soil fauna, diminish seed germination rates, promote plant root growth, yet impair plant photosynthetic efficacy and biomass productivity. These findings contribute to a better understanding of the impacts and mechanistic foundations of MNPs. Future research avenues are suggested to further explore the impacts and economic implications. 展开更多
关键词 Soil Property micro- and nano-Plastics Crop Yield Soil microorganism Soil Fauna Soil Greenhouse Gas Emissions
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Recent development of LiNi_xCo_yMn_zO_2:Impact of micro/nano structures for imparting improvements in lithium batteries 被引量:8
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作者 潘成迟 Craig E.BANKS +3 位作者 宋维鑫 王驰伟 陈启元 纪效波 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第1期108-119,共12页
The recent advancement in the design,synthesis,and fabrication of micro/nano structured LiNixCoyMnzO2 with one-,two-,and three-dimensional morphologies was reviewed.The major goal is to highlight LiNixCoyMnzO2 materia... The recent advancement in the design,synthesis,and fabrication of micro/nano structured LiNixCoyMnzO2 with one-,two-,and three-dimensional morphologies was reviewed.The major goal is to highlight LiNixCoyMnzO2 materials,which have been utilized in lithium ion batteries with enhanced energy and power density,high energy efficiency,superior rate capability and excellent cycling stability resulting from the doping,surface coating,nanocomposites and nano-architecturing. 展开更多
关键词 lithium-ion battery micro/nano structures LiNixCoyMnzO2 DOPING surface coating composite materials
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Correlation of Microstructure of Leaf Sheath Epidermis and Nutrient Composition of Palm Plants with the Damage Degree of Red Palm Fiber Elephant 被引量:1
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作者 申晓萍 欧善生 +3 位作者 谢彦洁 王小欣 覃连红 侯亮 《Plant Diseases and Pests》 CAS 2010年第2期58-62,共5页
[ Objective] Correlation of microstructure of leaf sheath epidermis and nutrient composition of palm plants with the damage degree of red palm fiber elephant in four kinds of plants in Nanning were analyzed in order t... [ Objective] Correlation of microstructure of leaf sheath epidermis and nutrient composition of palm plants with the damage degree of red palm fiber elephant in four kinds of plants in Nanning were analyzed in order to control the occurrence and damage of this insect in Nanning. [Method] Taken 4 kinds of Palmae plants in Nanning including Ravenea fivulafis, Washingtonia filifera, Phoenix canafiensis, Roystonea regia (HBK.)O. F. Cook as materials, damage situation of the red palm fiber elephant was investigated, microstructure of leaf sheath epidermis and nutrient composition of palm plants were analyzed and determined. [ Result] The results showed that there was direct correlation between the microstructure of leaf sheath epidermis and nutrient composition with the physical resistance of palm plant against red palm fiber elephant. The extend of damage from red palm fiber elephant had negatively relation with the thickness of corneum and leaf epidermis. The damage degree caused by red palm fiber elephant increased with the content of crude protein, crude ash and nitrogen free extract increasing, also increased with the content of rude fiber decreasing. [Condusion] The damage degree of red palm fiber elephant had a relationship with microstructure of leaf sheath epidermis and nutrient composition of palm plants. 展开更多
关键词 PALM Leaf sheath epidermis micro/structure Nutrition ingredients Red palm fiber elephant
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Stability Analysis of Contact Scanning Probe for Micro/Nano Coordinate Measuring Machine 被引量:2
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作者 李瑞君 范光照 +3 位作者 钱剑钊 黄强先 龚伟 苗晋伟 《纳米技术与精密工程》 EI CAS CSCD 2012年第2期125-131,共7页
关键词 微纳米三坐标测量机 扫描探头 稳定性分析 传感哭喊中
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DISTRIBUTED MICROBEND FIBER-OPTIC STRAIN SENSOR
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作者 孟爱东 骆飞 袁慎芳 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2000年第2期224-227,共4页
The distributed strain sensor has significant application in real time measurement of strain status for large and important engineering structures such as aircraft, bridge and dam. In this paper, a quasi distributed... The distributed strain sensor has significant application in real time measurement of strain status for large and important engineering structures such as aircraft, bridge and dam. In this paper, a quasi distributed optical fiber strain sensor system is set up using optical time domain reflect technique. The local strain sensors based on a novel microbend configuration are designed and applied to measure local strains along the optical fiber. As the result of the experimental research, the microbend sensors show high sensitivity, good linearity and repeatability in certain operation range. 展开更多
关键词 strain measurement strain sensor optical fiber sensor DISTRIBUTED micro bend
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Synthesis of porous nano/micro structured LiFePO_4/C cathode materials for lithium-ion batteries by spray-drying method 被引量:1
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作者 管晓梅 李国军 +1 位作者 黎春阳 任瑞铭 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2017年第1期141-147,共7页
In order to enhance electrochemical properties of LiFePO4 (LFP) cathode materials, spherical porous nano/micro structured LFP/C cathode materials were synthesized by spray drying, followed by calcination. The result... In order to enhance electrochemical properties of LiFePO4 (LFP) cathode materials, spherical porous nano/micro structured LFP/C cathode materials were synthesized by spray drying, followed by calcination. The results show that the spherical precursors with the sizes of 0.5-5 μm can be completely converted to LFP/C when the calcination temperature is higher than 500 ℃. The LFP/C microspheres obtained at calcination temperature of 700 ℃ are composed of numerous particles with sizes of -20 nm, and have well-developed interconnected pore structure and large specific surface area of 28.77 mE/g. The specific discharge capacities of the LFP/C obtained at 700 ℃ are 162.43, 154.35 and 144.03 mA.h/g at 0.5C, 1C and 2C, respectively. Meanwhile, the capacity retentions can reach up to 100% after 50 cycles. The improved electrochemical properties of the materials are ascribed to a small Li+ diffusion resistance and special structure of LFP/C microspheres. 展开更多
关键词 LiFePO4/C cathode nano/micro structure porous material spray drying electrochemical properties
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TPU/Nano-ZnO复合改性沥青的性能研究及微观机制
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作者 田小革 李光耀 +4 位作者 陈功 姚世林 黄雪梅 王俊杰 陆劲州 《材料导报》 EI CAS CSCD 北大核心 2024年第16期98-107,共10页
为促进聚合物/纳米改性沥青在耐久性路面中的应用,在实验室将不同掺量的聚氨酯及纳米氧化锌添加到A-70#基质沥青中制备了复合改性沥青。采用传统物理性能试验、动态剪切流变试验(DSR)、弯曲梁流变试验(BBR)研究了其物理性能与流变特性,... 为促进聚合物/纳米改性沥青在耐久性路面中的应用,在实验室将不同掺量的聚氨酯及纳米氧化锌添加到A-70#基质沥青中制备了复合改性沥青。采用传统物理性能试验、动态剪切流变试验(DSR)、弯曲梁流变试验(BBR)研究了其物理性能与流变特性,基于响应面法的优化设计来明确两种改性剂的最佳掺量。借助傅里叶红外光谱试验(FTIR)对其微观改性机理进行探讨。采用高压紫外汞灯环境箱对改性沥青进行不同时间的紫外老化,分析其抗紫外老化能力,并基于主成分分析法评价了老化性能测试指标的显著性。结果表明:聚氨酯与纳米氧化锌的共同作用提高了基质沥青的高温稳定性及低温抗裂性,两种改性剂的最佳掺量分别为5%、3%。根据FTIR结果,复合改性沥青的改性过程既存在物理共混,又有化学加成反应。聚氨酯及纳米氧化锌的加入在基质沥青紫外老化过程中能够抑制羰基、亚砜基等极性基团的生成,复数剪切模量、羰基指数、劲度模量及亚砜基指数对沥青紫外老化性能的影响最为显著。 展开更多
关键词 聚氨酯 纳米氧化锌 复合改性沥青 宏观性能 微观机理
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Synthesis of hierarchical dendritic micro–nano structure ZnFe_2O_4 and photocatalytic activities for water splitting 被引量:5
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作者 Zhongping Yao Yajun Zhang +2 位作者 Yaqiong He Qixing Xia Zhaohua Jiang 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2016年第8期1112-1116,共5页
Hierarchical dendritic micro–nano structure Zn Fe_2O_4 have been prepared by electrochemical reduction and thermal oxidation method in this work. X-ray diffractometry, Raman spectra and field-emission scanning electr... Hierarchical dendritic micro–nano structure Zn Fe_2O_4 have been prepared by electrochemical reduction and thermal oxidation method in this work. X-ray diffractometry, Raman spectra and field-emission scanning electron microscopy were used to characterize the crystal structure, size and morphology. The results show that the sample(S-2) is composed of pure ZnFe_2O_4 when the molar ratio of Zn^(2+)/Fe^(2+)in the electrolyte is 0.35. Decreasing the molar ratio of Zn^(2+)/Fe^(2+), the sample(S-1) is composed of ZnFe_2O_4 and α-Fe_2O_3, whereas increasing the molar ratio of Zn^(2+)/Fe^(2+), the sample(S-3) is composed of ZnFe_2O_4 and Zn O. The lattice parameters of ZnFe_2O_4 are influenced by the molar ratio of Zn^(2+)/Fe: Zn at excess decreases the cell volume whereas Fe at excess increases the cell volume of Zn Fe_2O_4. All the samples have the dendritic structure, of which S-2 has micron-sized lush branches with nano-sized leaves. UV–Vis diffuse reflectance spectra were acquired by a spectrophotometer. The absorption edges gradually blue shift with the increase of the molar ratio of Zn^(2+)/Fe^(2+). Photocatalytic activities for water splitting were investigated under Xe light irradiation in an aqueous olution containing 0.1 mol·L^(-1)Na_2S/0.02 mol·L^(-1)Na_2SO_3 in a glass reactor. The relatively highest photocatalytic activity with 1.41 μmol·h-1· 0.02 g^(-1)was achieved by pure ZnFe_2O_4sample(S-2). The photocatalytic activity of the mixture phase of Zn Fe_2O_4 and α-Fe_2O_3(S-1) is better than ZnF e_2O_4 and ZnO(S-3). 展开更多
关键词 ZNFE2O4 ELECTROCHEMICAL reduction and thermal OXIDATION DENDRITIC micronano structure Hydrogen production
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Micro/nano Indentation and Single Grit Diamond Grinding Mechanism on Ultra Pure Fused Silica 被引量:11
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作者 ZHAO Qingliang GUO Bing +1 位作者 STEPHENSIN David CORBETT John 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2011年第6期963-970,共8页
The existing research about ductile grinding of fused silica glass was mainly focused on how to carry out ductile regime material removal for generating very "smoothed" surface and investigate the machining-induced ... The existing research about ductile grinding of fused silica glass was mainly focused on how to carry out ductile regime material removal for generating very "smoothed" surface and investigate the machining-induced damage in the grinding in order to reduce or eliminate the subsurface damage.The brittle/ductile transition behavior of optical glass materials and the wear of diamond wheel are the most important factors for ductile grinding of optical glass.In this paper,the critical brittle/ductile depth,the influence factors on brittle/ductile transition behavior,the wear of diamond grits in diamond grinding of ultra pure fused silica(UPFS) are investigated by means of micro/nano indentation technique,as well as single grit diamond grinding on an ultra-stiff machine tool,Tetraform "C".The single grit grinding processes are in-process monitored using acoustic emission(AE) and force dynamometer simultaneously.The wear of diamond grits,morphology and subsurface integrity of the machined groves are examined with atomic force microscope(AFM) and scanning electron microscope(SEM).The critical brittle/ductile depth of more than 0.5 μm is achieved.When compared to the using roof-like grits,by using pyramidal diamonds leads to higher critical depths of scratch with identical grinding parameters.However,the influence of grit shapes on the critical depth is not significant as supposed.The grinding force increased linearly with depth of cut in the ductile removal regime,but in brittle removal regime,there are large fluctuations instead of forces increase.The SEM photographs of the cross-section profile show that the median cracks dominate the crack patterns beneath the single grooves.Furthermore,The SEM photographs show multi worn patterns of diamond grits,indicating an inhomogeneous wear mechanism of diamond grits in grinding of fused silica with diamond grinding wheels.The proposed research provides the basal technical theory for improving the ultra-precision grinding of UPFS. 展开更多
关键词 ultra pure fused silica (UPFS) micro/nano indentation single grit diamond grinding ductile material removal subsurface integrity diamond grits wear
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Micro Model of Carbon Fiber/Cyanate Ester Composites and Analysis of Machining Damage Mechanism 被引量:3
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作者 Haitao Liu Jie Lin +1 位作者 Yazhou Sun Jinyang Zhang 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2019年第3期198-208,共11页
Machining damage occurs on the surface of carbon fiber reinforced polymer (CFRP) composites during processing. In the current simulation model of CFRP, the initial defects on the carbon fiber and the periodic random d... Machining damage occurs on the surface of carbon fiber reinforced polymer (CFRP) composites during processing. In the current simulation model of CFRP, the initial defects on the carbon fiber and the periodic random distribution of the reinforcement phase in the matrix are not considered in detail, which makes the characteristics of the cutting model significantly different from the actual processing conditions. In this paper, a novel three-phase model of carbon fiber/cyanate ester composites is proposed to simulate the machining damage of the composites. The periodic random distribution of the carbon fiber reinforced phase in the matrix was realized using a double perturbation algorithm. To achieve the stochastic distribution of the strength of a single carbon fiber, a novel method that combines the Weibull intensity distribution theory with the Monte Carlo method is presented. The mechanical properties of the cyanate matrix were characterized by fitting the stress-strain curves, and the cohesive zone model was employed to simulate the interface. Based on the model, the machining damage mechanism of the composites was revealed using finite element simulations and by conducting a theoretical analysis. Furthermore, the milling surfaces of the composites were observed using a scanning electron microscope, to verify the accuracy of the simulation results. In this study, the simulations and theoretical analysis of the carbon fiber/cyanate ester composite processing were carried out based on a novel three-phase model, which revealed the material failure and machining damage mechanism more accurately. 展开更多
关键词 Carbon fiber reinforced polymer COMPOSITES micro simulation model MACHINING damage mechanism MILLING and observation experiment Theoretical ANALYSIS
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Preparation of micro/nano-structured ceramic coatings on Ti6Al4V alloy by plasma electrolytic oxidation process 被引量:9
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作者 Da-jun ZHAI Ke-qin FENG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2019年第12期2546-2555,共10页
In order to improve the osseointegration and antibacterial activity of titanium alloys,micro/nano-structured ceramic coatings doped with antibacterial element F were prepared by plasma electrolytic oxidation(PEO)proce... In order to improve the osseointegration and antibacterial activity of titanium alloys,micro/nano-structured ceramic coatings doped with antibacterial element F were prepared by plasma electrolytic oxidation(PEO)process on Ti6Al4V alloy in NaF electrolyte.The influence of NaF concentration(0.15-0.50 mol/L)on the PEO process,microstructure,phase composition,corrosion resistance and thickness of the coatings was investigated using scanning/transmission electron microscopy,energy dispersive spectroscopy,atomic force microscopy,X-ray diffractometer,and potentiodynamic polarization.The results demonstrated that Ti6Al4V alloy had low PEO voltage(less than 200 V)in NaF electrolyte,which decreased further as the NaF concentration increased.A micro/nano-structured coating with 10-15μm pits and 200-800 nm pores was formed in NaF electrolyte;the morphology was different from the typical pancake structure obtained with other electrolytes.The coating formed in NaF electrolyte had low surface roughness and was thin(<4μm).The NaF concentration had a small effect on the phase transition from metastable anatase phase to stable rutile phase,but greatly affected the corrosion resistance.In general,as the NaF concentration increased,the surface roughness,phase(anatase and rutile)contents,corrosion resistance,and thickness of the coating first increased and then decreased,reaching the maximum values at 0.25 mol/L NaF. 展开更多
关键词 plasma electrolytic oxidation Ti6Al4V alloy micro/nano structure NAF surface modification
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Dropwise condensation heat transfer enhancement on surfaces micro/nano structured by a two-step electrodeposition process 被引量:4
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作者 Hamid Reza TALESH BAHRAMI Alireza AZIZI Hamid SAFFARI 《Journal of Central South University》 SCIE EI CAS CSCD 2019年第5期1065-1076,共12页
Condensation is an important regime of heat transfer which has wide applications in different industries such as power plants,heating,ventilating and air conditioning,and refrigeration.Condensation occurs in two diffe... Condensation is an important regime of heat transfer which has wide applications in different industries such as power plants,heating,ventilating and air conditioning,and refrigeration.Condensation occurs in two different modes including filmwise (FWC) and dropwise (DWC) condensation.DWC occurring on hydrophobic and superhydrophobic surfaces has a much higher heat transfer capacity than FWC.Therefore,wide investigations have been done to produce DWC in recent years.Superhydrophobic surfaces have micro/nano structures with low surface energy.In this study,a two-step electrodeposition process is used to produce micro/nano structures on copper specimens.The surface energy of specimens is reduced by a self-assembled monolayer using ethanol and 1-octadecanethiol solution.The results show that there is an optimum condition for electrodeposition parameters.For example,a surface prepared by 2000 s step time has 5 times greater heat transfer than FWC while a surface with 4000 s step time has nearly the same heat transfer as FWC.The surfaces of the fabricated specimens are examined using XRD and SEM analyses.The SEM analyses of the surfaces show that there are some micro-structures on the surfaces and the surface porosities are reduced by increasing the second step electrodeposition time. 展开更多
关键词 dropwise condensation heat transfer ELECTRODEPOSITION micro/nano structure POROSITY
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“Smart”micro/nano container-based self-healing coatings on magnesium alloys:A review 被引量:4
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作者 Yonghua Chen Liang Wu +7 位作者 Wenhui Yao Jiahao Wu Maria Serdechnova Carsten Blawert Mikhail L.Zheludkevich Yuan Yuan Zhihui Xie Fusheng Pan 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第7期2230-2259,共30页
Coating technologies are a commonly used way to protect metals against corrosion.However,with more and more severe service environments of materials,many protective coating systems often are not environmentally friend... Coating technologies are a commonly used way to protect metals against corrosion.However,with more and more severe service environments of materials,many protective coating systems often are not environmentally friendly or toxic as in the case of chromates.Based on the world’s abundant ideal magnesium(Mg)and its alloy,the smart self-healing anticorrosive coating can autonomously restore the damaged part of the coating according to the environmental changes,strengthen the corrosion protection ability,and prolong its service life.This paper reviews the research progress of smart self-healing coatings on Mg alloys.These coatings mostly contain suitable corrosion inhibitors encapsulated into micro/nano containers.Moreover,the different self-healing mechanisms and functionalities of micro/nano containers are discussed.The micro/nano containers range from inorganic nanocontainers such as mesoporous nanoparticles(silica(SiO_(2)),titanium dioxide(TiO_(2)),etc.),over inorganic clays(halloysite,hydrotalcite-like,zeolite),to organic nanocontainers such as polymer microcapsules,nanofibers,chitosan(CS)and cyclodextrin(CD),as well as,carbon materials such as graphene and carbon nanotubes and hybrids such as metal organic frameworks.The functioning of micro/nano containers can be divided in two principal groups:autonomous(based on defect filling and corrosion inhibition)and non-autonomous(based on dynamic bonds and shape memory polymers).Moreover,multi functionalities and composite applications of various micro/nano containers are summarized.At present,significant progress has been made in the preparation methods and technologies of micro/nano containers.Achieving long-term self-healing properties of coatings sensing of coating failure and early warning after self-healing function failure can be expected as the main development direction of self-healing corrosion protection coatings in the future. 展开更多
关键词 Magnesium alloy Self-healing coating micro/nano containers Mechanism Corrosion protection
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