Silver powder was fabricated by spray pyrolysis, using 2%-20% AgNO3 solution, 336-500 mL/h flux of AgNO3 solution, 0.28-0.32 MPa flux of carrier gas and in the 620-820 ℃ temperature range. The effects of furnace set ...Silver powder was fabricated by spray pyrolysis, using 2%-20% AgNO3 solution, 336-500 mL/h flux of AgNO3 solution, 0.28-0.32 MPa flux of carrier gas and in the 620-820 ℃ temperature range. The effects of furnace set temperature, concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated. The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32 MPa flux of carrier gas at 720 ℃ furnace set temperature.展开更多
[Objectives]The effects of water chestnut powder on the gel properties and quality of silver carp surimi were investigated.[Methods]The surimi gel was prepared by adding 0%,1%,2%,3%,4%and 5%of water chestnut powder to...[Objectives]The effects of water chestnut powder on the gel properties and quality of silver carp surimi were investigated.[Methods]The surimi gel was prepared by adding 0%,1%,2%,3%,4%and 5%of water chestnut powder to the surimi of silver carp.The gel properties,water-holding capacity,cooking loss,whiteness value,puncture and texture profile analysis(TPA)indexes of surimi products were determined to assess the effects of adding different amounts of water chestnut powder on surimi gel.[Results]The results showed that the gel strength,breaking force and depression distance of surimi products increased first and then decreased with the increase of the addition of water chestnut powder.Compared with the control group,the hardness and chewiness of surimi gel in TPA could be significantly improved by adding water chestnut powder.When the addition of water chestnut powder was 2%,the maximum water-holding capacity was 83.68%;the cooking loss rate was the lowest;and the whiteness value was the highest.Adding 2%of water chestnut powder could significantly improve the gel properties of silver carp surimi and obtain a good gel product.[Conclusions]This study provides a scientific basis for the effective utilization of water chestnut resources and the development of new fish surimi products.展开更多
Antibacterial powders of titanium dioxide/silver sulfate were produced by heat-treatment of the metatitanic acid, as precursor, into which the silver nitrate was added. The influences of heating temperature on the str...Antibacterial powders of titanium dioxide/silver sulfate were produced by heat-treatment of the metatitanic acid, as precursor, into which the silver nitrate was added. The influences of heating temperature on the structure and composition of the product were investigated through XRD and SEM. The results show that the powder is spherical in the phase of TiO2-Ag2SO4. The granularity of the particles increases from 10.7nm to 28.7nm with the temperature of heat-treatment increasing from 300℃ to 800℃. The antibacterial activity of the powder was judged in the way of the minimum inhibitory contents (MiCs). When the content of silver sulfate is less than 2%, the photocatalysis of titanium dioxide and silver ions cooperate to kill bacteria. And the MiCs decrease and keep around 1.0×10 -41.5×10 -4 constantly with the increase of silver content. Furthermore, the MiCs decrease with the increase of temperature of heat-treatment when the temperature is lower than 500℃. But when the temperature is beyond 600℃ the MiCs increase quickly, which shows the inferior antibacterial performance.展开更多
Maki-e is a traditional Japanese decorative technique that uses the natural lacquer Urushi and metal powders. In 2014, there exist only two companies that manufacture silver powder for the purpose of Maki-e, and this ...Maki-e is a traditional Japanese decorative technique that uses the natural lacquer Urushi and metal powders. In 2014, there exist only two companies that manufacture silver powder for the purpose of Maki-e, and this study focuses on comparing the powders manufactured by them. Gloss and color of each silver powder were measured after Maki-e decoration was finished, and EDS (energy-dispersive X-ray spectroscopy) was used to determine the differences in their chemical composition. In addition, to verify the effect of polishing, residual gloss after sulfuration and polishing was measured. The study revealed that the shapes of the silver powders (Maru-fun, No. 1) manufactured by the two companies are different and it affects the occupancy rate of Urushi and powder, which in turn affects their gloss and color. Wakou silver has a very strong resistance to sulfuration;however, owing to its Pd content, its chroma is much lower than that of other powders. It was shown that sulfuration on powder surface can be removed by polishing irrespective of the shape and chemical composition ratio of the particles.展开更多
[Objectives]This study was conducted to improve the gel properties of freshwater surimi and its products. [Methods] Tuanfeng lotus seed powder was added to frozen silver carp, and the relationship between the addiamou...[Objectives]This study was conducted to improve the gel properties of freshwater surimi and its products. [Methods] Tuanfeng lotus seed powder was added to frozen silver carp, and the relationship between the addiamount of Tuanfeng lotus seed powder(1%, 2%, 3%, 4% and 5%) and the quality of surimi products was studied, so as to improve the quality of surimi products. [Results] The water holding capacity(86.71%±0.36%), hardness(3 566.64±51.15) g, chewiness(2 697.16±15.81) g and gel strength(692.54±23.19) of surimi products increased to the maximums when the addition amount of lotus seed powder was 3%. Meanwhile, the cooking loss rate was reduced to the minimum(13.00%±0.17%), and the sensory quality was the best, although the whiteness of surimi products decreased slightly with the increase of Tuanfeng lotus seed powder. Therefore, the quality of silver carp surimi products could be improved obviously when the dosage of Tuanfeng lotus seed powder was 3%. [Conclusions] This study provides more new ideas for improving the quality of silver carp surimi products, and simultaneously makes the development of lotus seed food more diversified.展开更多
文摘Silver powder was fabricated by spray pyrolysis, using 2%-20% AgNO3 solution, 336-500 mL/h flux of AgNO3 solution, 0.28-0.32 MPa flux of carrier gas and in the 620-820 ℃ temperature range. The effects of furnace set temperature, concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated. The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32 MPa flux of carrier gas at 720 ℃ furnace set temperature.
基金Supported by High-level Cultivation Project of Huanggang Normal University(04201711903).
文摘[Objectives]The effects of water chestnut powder on the gel properties and quality of silver carp surimi were investigated.[Methods]The surimi gel was prepared by adding 0%,1%,2%,3%,4%and 5%of water chestnut powder to the surimi of silver carp.The gel properties,water-holding capacity,cooking loss,whiteness value,puncture and texture profile analysis(TPA)indexes of surimi products were determined to assess the effects of adding different amounts of water chestnut powder on surimi gel.[Results]The results showed that the gel strength,breaking force and depression distance of surimi products increased first and then decreased with the increase of the addition of water chestnut powder.Compared with the control group,the hardness and chewiness of surimi gel in TPA could be significantly improved by adding water chestnut powder.When the addition of water chestnut powder was 2%,the maximum water-holding capacity was 83.68%;the cooking loss rate was the lowest;and the whiteness value was the highest.Adding 2%of water chestnut powder could significantly improve the gel properties of silver carp surimi and obtain a good gel product.[Conclusions]This study provides a scientific basis for the effective utilization of water chestnut resources and the development of new fish surimi products.
文摘Antibacterial powders of titanium dioxide/silver sulfate were produced by heat-treatment of the metatitanic acid, as precursor, into which the silver nitrate was added. The influences of heating temperature on the structure and composition of the product were investigated through XRD and SEM. The results show that the powder is spherical in the phase of TiO2-Ag2SO4. The granularity of the particles increases from 10.7nm to 28.7nm with the temperature of heat-treatment increasing from 300℃ to 800℃. The antibacterial activity of the powder was judged in the way of the minimum inhibitory contents (MiCs). When the content of silver sulfate is less than 2%, the photocatalysis of titanium dioxide and silver ions cooperate to kill bacteria. And the MiCs decrease and keep around 1.0×10 -41.5×10 -4 constantly with the increase of silver content. Furthermore, the MiCs decrease with the increase of temperature of heat-treatment when the temperature is lower than 500℃. But when the temperature is beyond 600℃ the MiCs increase quickly, which shows the inferior antibacterial performance.
文摘Maki-e is a traditional Japanese decorative technique that uses the natural lacquer Urushi and metal powders. In 2014, there exist only two companies that manufacture silver powder for the purpose of Maki-e, and this study focuses on comparing the powders manufactured by them. Gloss and color of each silver powder were measured after Maki-e decoration was finished, and EDS (energy-dispersive X-ray spectroscopy) was used to determine the differences in their chemical composition. In addition, to verify the effect of polishing, residual gloss after sulfuration and polishing was measured. The study revealed that the shapes of the silver powders (Maru-fun, No. 1) manufactured by the two companies are different and it affects the occupancy rate of Urushi and powder, which in turn affects their gloss and color. Wakou silver has a very strong resistance to sulfuration;however, owing to its Pd content, its chroma is much lower than that of other powders. It was shown that sulfuration on powder surface can be removed by polishing irrespective of the shape and chemical composition ratio of the particles.
基金Supported by Scientific Research Program Steering Group Project of Department of Education of Hubei Province (B2020166)。
文摘[Objectives]This study was conducted to improve the gel properties of freshwater surimi and its products. [Methods] Tuanfeng lotus seed powder was added to frozen silver carp, and the relationship between the addiamount of Tuanfeng lotus seed powder(1%, 2%, 3%, 4% and 5%) and the quality of surimi products was studied, so as to improve the quality of surimi products. [Results] The water holding capacity(86.71%±0.36%), hardness(3 566.64±51.15) g, chewiness(2 697.16±15.81) g and gel strength(692.54±23.19) of surimi products increased to the maximums when the addition amount of lotus seed powder was 3%. Meanwhile, the cooking loss rate was reduced to the minimum(13.00%±0.17%), and the sensory quality was the best, although the whiteness of surimi products decreased slightly with the increase of Tuanfeng lotus seed powder. Therefore, the quality of silver carp surimi products could be improved obviously when the dosage of Tuanfeng lotus seed powder was 3%. [Conclusions] This study provides more new ideas for improving the quality of silver carp surimi products, and simultaneously makes the development of lotus seed food more diversified.