The objective of this work is using the online measurement method to study the process of precipitation of nickel hydroxide in a single-feed semi-batch stirred reactor with an internal diameter ofD = 240mm. The effect...The objective of this work is using the online measurement method to study the process of precipitation of nickel hydroxide in a single-feed semi-batch stirred reactor with an internal diameter ofD = 240mm. The effects of impeller speed, impeller type, impeller diameter and feed location on the mean particle size d43 and particle size distribution （PSD） were investigated, d43 and PSD were measured online using a Malvern Insitec Liquid Pro- cess Sizer every 20 s. It was found that d43 varied between 13 kwh and 26 lain under different operating conditions, and it decreased with increasing impeller diameter. When feeding at the off-bottom distance of D/2 under lower impeller speeds, d43 was significantly smaller than that at D/3. PSDs were slightly influenced by operating conditions.展开更多
Baffles with shape of ＂-＂ （single baffle）, ＂＋＂ （cross-baffles with four arms） and （baffles with 6 arms） are used to enhance the mixing of particles in a rotating drum mixer. A micro-dynamics study of mixing...Baffles with shape of ＂-＂ （single baffle）, ＂＋＂ （cross-baffles with four arms） and （baffles with 6 arms） are used to enhance the mixing of particles in a rotating drum mixer. A micro-dynamics study of mixing and segregation ofa bi-disperse system of two particle sizes in the rotating drum with these three kinds of baffles is carried out using the discrete element method （DEM）. The effect of the baffles on mixing, and the mechanisms of mixing enhancement by the baffles are discussed and analyzed. Simulation results show that in an unbaffled drum mixer, particle convection, particle diffusion, and size segregation of hi- disperse particles, all play important roles in the mixing process; whereas size segregation will be largely restrained when the drum mixer has a baffle, regardless of its shape, and the degree of mixing is higher than that in an unbaffled drum mixer. The different mixing characteristics for ＂-＂ shaped baffle, ＂＋＂ baffle, and baffle are revealed by the simulation results. For ＂＋＂ or style baffles, there is an optimal size of baffles for the mixing of particles, and the ootimal mixing efficiency is higher than that for ＂-＂ baffle.展开更多
基金the State Key Development Program for Basic Research of China(2013CB632601)the National High Technology Research and Development Program of China(2011AA060704)+1 种基金the National Natural Science Foundation of China(21476236,91434126)the National Science Fund for Distinguished Young Scholars(21025627)
文摘The objective of this work is using the online measurement method to study the process of precipitation of nickel hydroxide in a single-feed semi-batch stirred reactor with an internal diameter ofD = 240mm. The effects of impeller speed, impeller type, impeller diameter and feed location on the mean particle size d43 and particle size distribution （PSD） were investigated, d43 and PSD were measured online using a Malvern Insitec Liquid Pro- cess Sizer every 20 s. It was found that d43 varied between 13 kwh and 26 lain under different operating conditions, and it decreased with increasing impeller diameter. When feeding at the off-bottom distance of D/2 under lower impeller speeds, d43 was significantly smaller than that at D/3. PSDs were slightly influenced by operating conditions.
基金supported by the Science Foundation of Chinese Universitythe Zhejiang Provincial Natural Science Foundation of China (Grant No. Y1100636)
文摘Baffles with shape of ＂-＂ （single baffle）, ＂＋＂ （cross-baffles with four arms） and （baffles with 6 arms） are used to enhance the mixing of particles in a rotating drum mixer. A micro-dynamics study of mixing and segregation ofa bi-disperse system of two particle sizes in the rotating drum with these three kinds of baffles is carried out using the discrete element method （DEM）. The effect of the baffles on mixing, and the mechanisms of mixing enhancement by the baffles are discussed and analyzed. Simulation results show that in an unbaffled drum mixer, particle convection, particle diffusion, and size segregation of hi- disperse particles, all play important roles in the mixing process; whereas size segregation will be largely restrained when the drum mixer has a baffle, regardless of its shape, and the degree of mixing is higher than that in an unbaffled drum mixer. The different mixing characteristics for ＂-＂ shaped baffle, ＂＋＂ baffle, and baffle are revealed by the simulation results. For ＂＋＂ or style baffles, there is an optimal size of baffles for the mixing of particles, and the ootimal mixing efficiency is higher than that for ＂-＂ baffle.
