The microstructure and mechanical properties of multi-layer multi-pass TIG welded joints of Al-Zn-Mg alloy plates were studied.The phase constituent and microstructure of different regions of the welded joints were ch...The microstructure and mechanical properties of multi-layer multi-pass TIG welded joints of Al-Zn-Mg alloy plates were studied.The phase constituent and microstructure of different regions of the welded joints were characterized by scanning electron microscopy(SEM),X-ray diffraction(XRD),transmission electron microscopy(TEM)and energy disperse spectrum(EDS),while the mechanical properties were evaluated according to the impact test.A dispersively distributed spherical and needle-likeη(MgZn2)phase was obtained in the welding seam.The phase composition of the heat-affected zone(HAZ)wasα(Al)+η(MgZn2)+Al6Mn,and there were a large number of dispersively precipitated nanoscale particles.The welded joint zone had the highest impact toughness as compared with the other parts of the joint.The MgZn2 phase in the weld zone contributed to the improved toughness of the joint.Al2 MgCu phase in HAZ was proven to act as a crack source during fracture.展开更多
Laser multi\|layer cladding experiments were performed on the substrate of DD3 single crystal with FGH95 powder as cladding material.The solidification microstructure in the sample was investigated.It was found that t...Laser multi\|layer cladding experiments were performed on the substrate of DD3 single crystal with FGH95 powder as cladding material.The solidification microstructure in the sample was investigated.It was found that the solidification microstructure was greatly influenced by the crystallography orientation of the substrate and the local solidification conditions.When the angle between the preferred orientation of the single crystal and the direction of heat flow in the cladding layer is less than 30°,single crystal cladding layers were acquired.Otherwise the crystallography orientation of the cladding layer will deviate from the orientation of the substrate and the microstructure with polycrystalline appears.Meanwhile,even when the experiments were performed on the same preferred crystal surface,the solidification microstructures will be different distinctly resulting from the variation of the local solidification conditions.The secondary arms were degenerated and the primary arm spacing was about 10\|20μm.Further investigation shows that the phases of the cladding layer are mainly made up ofγ,γ′,the flower\|likeγ/γ′eutectic and carbide.The morphology ofγ′was cubical and the size is less than 0.1μm.展开更多
In the present study, an Al/Cu/Mg multi-layered composite was produced by accumulative roll bonding(ARB) through seven passes, and its microstructure and mechanical properties were evaluated. The microstructure invest...In the present study, an Al/Cu/Mg multi-layered composite was produced by accumulative roll bonding(ARB) through seven passes, and its microstructure and mechanical properties were evaluated. The microstructure investigations show that plastic instability occurred in both the copper and magnesium reinforcements in the primary sandwich. In addition, a composite with a perfectly uniform distribution of copper and magnesium reinforcing layers was produced during the last pass. By increasing the number of ARB cycles, the microhardness of the layers including aluminum, copper, and magnesium was significantly increased. The ultimate tensile strength of the sandwich was enhanced continually and reached a maximum value of 355.5 MPa. This strength value was about 3.2, 2, and 2.1 times higher than the initial strength values for the aluminum, copper, and magnesium sheets, respectively. Investigation of tensile fracture surfaces during the ARB process indicated that the fracture mechanism changed to shear ductile at the seventh pass.展开更多
To address the relatively mediocre mechanical properties of single-phase multi-component carbide ceramics,a phase transition from a single phase to multiple phases was proposed to achieve superior mechanical propertie...To address the relatively mediocre mechanical properties of single-phase multi-component carbide ceramics,a phase transition from a single phase to multiple phases was proposed to achieve superior mechanical properties.A series of(TiZrV_(x)Nb)C_(0.8) ceramics with different V contents were fabricated by spark plasma sintering(SPS).The influence of the V content on the phase composition,microstructural evolution,and mechanical properties was investigated in detail.The transition behavior from a single phase to multiple phases is discovered and discussed.The formation of the Zr-rich phase and Zr-poor phase can be attributed to the increase in lattice distortion and mixed enthalpy caused by the addition of V.A nanometer lamellar structure with a semi-coherent interface obtained via in situ decomposition is reported for the first time in multi-component carbide ceramics.The semi-coherent interfaces with high dislocation density and strain concentration effectively improve the mechanical properties,grain refinement,and multi-phase formation.The optimal comprehensive mechanical properties of the Vickers hardness(26.3 GPa),flexural strength(369 MPa),and fracture toughness(3.1 MPa·m^(1/2))were achieved for the sample with 20 mol%V.展开更多
Ni Co Cr-based multi-component alloys have drawn much attention due to their exceptional ductility and strain hardening capacity.However,insufficient strength-ductility synergy of NiCoCr alloy has always been an issue...Ni Co Cr-based multi-component alloys have drawn much attention due to their exceptional ductility and strain hardening capacity.However,insufficient strength-ductility synergy of NiCoCr alloy has always been an issue that prevents it from extensive applications.According to our previous research,the precipitation ofγ”phase can significantly improve the strength-ductility synergy of this alloy system at room temperature.In this study,the effects of V addition onγ”phase stability and high-temperature mechanical properties have been explicitly investigated.The results indicate that V addition can stabilize the metastableγ”phase in this alloy system and prevent it from transforming into a stableδphase at grain boundaries upon 650℃aging,resulting in improved mechanical properties at elevated temperatures.The specific strength ofγ”-strengthened multi-component NiCoCr-based alloy can reach up to 86.2 MPa gcmat 650℃,which is higher than those of Ni-based superalloys,IN 939 and Waspaloy.This work provides theoretical guidance for the novel design of γ”-strengthened alloy for high-temperature applications.展开更多
基金Project(ZR2016EEQ03) supported by the Shandong Province Natural Science Foundation,ChinaProject(2018M641822) supported by the China Postdoctoral Science Foundation-General ProgramProject(HIT.NSRIF.201703) supported by the Natural Scientific Research Innovation Foundation in HIT,China
文摘The microstructure and mechanical properties of multi-layer multi-pass TIG welded joints of Al-Zn-Mg alloy plates were studied.The phase constituent and microstructure of different regions of the welded joints were characterized by scanning electron microscopy(SEM),X-ray diffraction(XRD),transmission electron microscopy(TEM)and energy disperse spectrum(EDS),while the mechanical properties were evaluated according to the impact test.A dispersively distributed spherical and needle-likeη(MgZn2)phase was obtained in the welding seam.The phase composition of the heat-affected zone(HAZ)wasα(Al)+η(MgZn2)+Al6Mn,and there were a large number of dispersively precipitated nanoscale particles.The welded joint zone had the highest impact toughness as compared with the other parts of the joint.The MgZn2 phase in the weld zone contributed to the improved toughness of the joint.Al2 MgCu phase in HAZ was proven to act as a crack source during fracture.
基金National Key Basic Research Development Program me of china(No.G2000067205-3)
文摘Laser multi\|layer cladding experiments were performed on the substrate of DD3 single crystal with FGH95 powder as cladding material.The solidification microstructure in the sample was investigated.It was found that the solidification microstructure was greatly influenced by the crystallography orientation of the substrate and the local solidification conditions.When the angle between the preferred orientation of the single crystal and the direction of heat flow in the cladding layer is less than 30°,single crystal cladding layers were acquired.Otherwise the crystallography orientation of the cladding layer will deviate from the orientation of the substrate and the microstructure with polycrystalline appears.Meanwhile,even when the experiments were performed on the same preferred crystal surface,the solidification microstructures will be different distinctly resulting from the variation of the local solidification conditions.The secondary arms were degenerated and the primary arm spacing was about 10\|20μm.Further investigation shows that the phases of the cladding layer are mainly made up ofγ,γ′,the flower\|likeγ/γ′eutectic and carbide.The morphology ofγ′was cubical and the size is less than 0.1μm.
文摘In the present study, an Al/Cu/Mg multi-layered composite was produced by accumulative roll bonding(ARB) through seven passes, and its microstructure and mechanical properties were evaluated. The microstructure investigations show that plastic instability occurred in both the copper and magnesium reinforcements in the primary sandwich. In addition, a composite with a perfectly uniform distribution of copper and magnesium reinforcing layers was produced during the last pass. By increasing the number of ARB cycles, the microhardness of the layers including aluminum, copper, and magnesium was significantly increased. The ultimate tensile strength of the sandwich was enhanced continually and reached a maximum value of 355.5 MPa. This strength value was about 3.2, 2, and 2.1 times higher than the initial strength values for the aluminum, copper, and magnesium sheets, respectively. Investigation of tensile fracture surfaces during the ARB process indicated that the fracture mechanism changed to shear ductile at the seventh pass.
基金the National Natural Science Foundation of China (Nos. 52032002, 52372060, 51972081, and U22A20128)the National Safety Academic Foundation (No. U2130103)+4 种基金the National Key R&D Program of China (No. 2021YFB3701400)the China Postdoctoral Science Foundation (No. 2023M730839)the Heilongjiang Postdoctoral Fund (No. LBH-Z22025)the National Key Laboratory of Precision Hot Processing of Metals (No. 61429092300305)the Heilongjiang Touyan Team Program are gratefully acknowledged. The authors thank Professor Suk-Joong L. Kang (Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Republic of Korea) for his assistance in editing. The support of the thermodynamic calculations with FactSage software provided by Professor Yudong Fu (College of Material Science and Chemical Engineering, Harbin Engineering University, China) is also acknowledged.
文摘To address the relatively mediocre mechanical properties of single-phase multi-component carbide ceramics,a phase transition from a single phase to multiple phases was proposed to achieve superior mechanical properties.A series of(TiZrV_(x)Nb)C_(0.8) ceramics with different V contents were fabricated by spark plasma sintering(SPS).The influence of the V content on the phase composition,microstructural evolution,and mechanical properties was investigated in detail.The transition behavior from a single phase to multiple phases is discovered and discussed.The formation of the Zr-rich phase and Zr-poor phase can be attributed to the increase in lattice distortion and mixed enthalpy caused by the addition of V.A nanometer lamellar structure with a semi-coherent interface obtained via in situ decomposition is reported for the first time in multi-component carbide ceramics.The semi-coherent interfaces with high dislocation density and strain concentration effectively improve the mechanical properties,grain refinement,and multi-phase formation.The optimal comprehensive mechanical properties of the Vickers hardness(26.3 GPa),flexural strength(369 MPa),and fracture toughness(3.1 MPa·m^(1/2))were achieved for the sample with 20 mol%V.
基金financially supported by the National Science and Technology Major Project of China(Nos.J2019-VI-0004–0117 and 2017-VI0013–0085)the National Natural Science Foundation of China(Nos.52071205,52001205 and 51771118)。
文摘Ni Co Cr-based multi-component alloys have drawn much attention due to their exceptional ductility and strain hardening capacity.However,insufficient strength-ductility synergy of NiCoCr alloy has always been an issue that prevents it from extensive applications.According to our previous research,the precipitation ofγ”phase can significantly improve the strength-ductility synergy of this alloy system at room temperature.In this study,the effects of V addition onγ”phase stability and high-temperature mechanical properties have been explicitly investigated.The results indicate that V addition can stabilize the metastableγ”phase in this alloy system and prevent it from transforming into a stableδphase at grain boundaries upon 650℃aging,resulting in improved mechanical properties at elevated temperatures.The specific strength ofγ”-strengthened multi-component NiCoCr-based alloy can reach up to 86.2 MPa gcmat 650℃,which is higher than those of Ni-based superalloys,IN 939 and Waspaloy.This work provides theoretical guidance for the novel design of γ”-strengthened alloy for high-temperature applications.