Dynamic and static aging precipitation of Mg17Al12 phases in AZ80 magnesium alloy was studied by multidirectional forging（MDF） with decreasing temperatures from 410 to 300 ℃ and subsequent aging process. The result...Dynamic and static aging precipitation of Mg17Al12 phases in AZ80 magnesium alloy was studied by multidirectional forging（MDF） with decreasing temperatures from 410 to 300 ℃ and subsequent aging process. The results show that the morphology of the β-Mg17Al12 phases during forging process dynamically precipitates and aging process（statically precipitation） exhibited granular and laminar shapes, respectively. During the MDF, the inhomogeneous dynamic precipitation of the β-Mg17Al12 phases results in the uniformity on grain size, which is fine in the area with many granular Mg17Al12 phases but the grain is still coarse where there is no Mg17Al12 phases. During the aging process, the morphology of newly formed β-Mg17Al12 phases depends on the structural character of the forged sample. The newly precipitated β-Mg17Al12 phases are coarse laminar and needle-like shape in area with coarse grain. While, the fine newly precipitated β-Mg17Al12 phases are fine granular and needle-like in the area with fine grain.展开更多
The microstructural evolution and mechanical properties of ultrafine-grained(UFG)CP-Ti after an innovative large-volume equal channel angular pressing(L-ECAP)and multi-directional forging(MDF)were systematically exami...The microstructural evolution and mechanical properties of ultrafine-grained(UFG)CP-Ti after an innovative large-volume equal channel angular pressing(L-ECAP)and multi-directional forging(MDF)were systematically examined using monotonic tensile tests combined with transmission electron microscope(TEM)and electron backscatter diffraction(EBSD)techniques.Substantially refined and homogeneous microstructures were achieved after L-ECAP(8-pass and 12-pass)and MDF(2-cycle and 3-cycle),respectively,where the grain size distribution conformed to lognormal distribution.The grain refinement of450℃L-ECAP is dominated by dynamic recrystallization(DRX)and dynamic recovery(DRV),while that of MDF is dominated by DRX.The iron impurities promote recrystallization by pinning-induced dislocation accumulation so that DRX is prone to occur at iron segregation regions during L-ECAP.The monotonic tensile results show that the strain hardening rate of CP-Ti increases with the decrease of grain size,while the continuous strain hardening ability decreases.The relationship between the average grain size and yield strength is in accordance with Hall-Petch relationship.Meanwhile,the individual strengthening mechanisms were quantitatively examined by the modified model.The results indicate that the strengthening contribution of dislocation accumulation to yield strength is greater than that of grain refinement.展开更多
基金supported by the National Natural Science Foundation of China (Nos.51204053,51674078 and 51374067)the Fundamental Research Fund for Central Universities (Nos.N160913002,N130409005 and N130209001)A Project supported by Scientific Research Fund of Liaoning Province (No.2015022003)
文摘Dynamic and static aging precipitation of Mg17Al12 phases in AZ80 magnesium alloy was studied by multidirectional forging（MDF） with decreasing temperatures from 410 to 300 ℃ and subsequent aging process. The results show that the morphology of the β-Mg17Al12 phases during forging process dynamically precipitates and aging process（statically precipitation） exhibited granular and laminar shapes, respectively. During the MDF, the inhomogeneous dynamic precipitation of the β-Mg17Al12 phases results in the uniformity on grain size, which is fine in the area with many granular Mg17Al12 phases but the grain is still coarse where there is no Mg17Al12 phases. During the aging process, the morphology of newly formed β-Mg17Al12 phases depends on the structural character of the forged sample. The newly precipitated β-Mg17Al12 phases are coarse laminar and needle-like shape in area with coarse grain. While, the fine newly precipitated β-Mg17Al12 phases are fine granular and needle-like in the area with fine grain.
基金financially supported by the National Natural Science Foundation of China(Nos.51725503 and 51975211)the Shanghai Super Postdoctoral Incentive Plan,Shanghai Rising-Star Program(No.20QA1402500)the Innovation Program of Shanghai Municipal Education Commission(No.2019-01-07-0002-E00068)。
文摘The microstructural evolution and mechanical properties of ultrafine-grained(UFG)CP-Ti after an innovative large-volume equal channel angular pressing(L-ECAP)and multi-directional forging(MDF)were systematically examined using monotonic tensile tests combined with transmission electron microscope(TEM)and electron backscatter diffraction(EBSD)techniques.Substantially refined and homogeneous microstructures were achieved after L-ECAP(8-pass and 12-pass)and MDF(2-cycle and 3-cycle),respectively,where the grain size distribution conformed to lognormal distribution.The grain refinement of450℃L-ECAP is dominated by dynamic recrystallization(DRX)and dynamic recovery(DRV),while that of MDF is dominated by DRX.The iron impurities promote recrystallization by pinning-induced dislocation accumulation so that DRX is prone to occur at iron segregation regions during L-ECAP.The monotonic tensile results show that the strain hardening rate of CP-Ti increases with the decrease of grain size,while the continuous strain hardening ability decreases.The relationship between the average grain size and yield strength is in accordance with Hall-Petch relationship.Meanwhile,the individual strengthening mechanisms were quantitatively examined by the modified model.The results indicate that the strengthening contribution of dislocation accumulation to yield strength is greater than that of grain refinement.
