Towards tailoring basal texture of rolled Mg alloy sheet by recrystallization for high room-temperature formability: A review

Room-temperature(RT) formability is a key factor to broaden the applications of rolled Mg alloy sheets in the industry. However, rolled Mg alloy sheets generally form strong basal texture, where the(0001) poles align parallel to the normal direction(ND). This hinders the activation of(0001) [1120] basal slip, limiting the RT formability. Therefore, texture weakening, i.e., the inclination of the(0001) poles from the ND, plays an important role to improve the RT formability. Recrystallization is crucial to control the textural development in Mg,and currently, the texture weakening is commonly achieved using static recrystallization(SRX). However, the type of slipping and twinning,which are activated during rolling, affect the textural features after SRX. It is also demonstrated that shear bands and preferential grain growth are important factors to tailor the texture during SRX. Indeed, dynamic recrystallization(DRX) easily occurs during rolling in Mg, which also affects the final rolling texture, while the effect of DRX on the textural formation is not extensively studied for the development of RT-formable Mg alloy sheets. Therefore, the effect of these factors on the textural development in rolled Mg is reviewed in this manuscript.Additionally, the ideal microstructure and texture for RT-formable Mg alloy sheets are still controversial. The RT-formability includes stretch forming(biaxial tension), bending(plane strain tension), and deep-drawing. In particular, the stretch forming is commonly used to evaluate the RT-formability of rolled Mg. Although the stretch formability has been improved by recent studies, the further improvement is necessary owing to the relatively low formability of rolled Mg compared with that of rolled Fe and Al. Based on the relationship between the microstructure/texture and stretch formability provided in the literature, the design guidance for high stretch formability is proposed in this review.

Influence of bimodal non-basal texture on microstructure characteristics,texture evolution and deformation mechanisms of AZ31 magnesium alloy sheet rolled at liquid-nitrogen temperature

Cryogenic rolling experiments have been conducted on the AZ31 magnesium(Mg)alloy sheet with bimodal non-basal texture,which is fabricated via the newly developed equal channel angular rolling and continuous bending process with subsequent annealing(ECAR-CB-A)process.Results demonstrate that this sheet shows no edge cracks until the accumulated thickness reduction reaches about 18.5%,which is about 105.6%larger than that of the sheet with traditional basal texture.Characterization experiments including optical microstructure(OM),X-ray diffractometer(XRD),and electron backscatter diffraction(EBSD)measurements are then performed to explore the microstructure characteristics,texture evolution and deformation mechanisms during cryogenic rolling.Experimental observations confirm the occurrence of abundant{10–12}extension twins(ETs),twin-twin interactions among{10–12}ET variants and{10–12}-{10–12}double twins(DTs).The twinning behaviors as for{10–12}ETs are responsible for the concentration of c-axes of grains towards normal direction(ND)and the formation of transverse direction(TD)-component texture at the beginning of cryogenic rolling.The twinning behaviors with respect to{10–12}-{10–12}DTs are responsible for the disappearance of TD-component texture at the later stage of cryogenic rolling.The involved deformation mechanisms can be summarized as follows:Firstly{10–12}ETs dominate the plastic deformation.Subsequently,dislocation slip,especially basal<a>slip,starts to sustain more plastic strain,while{10–12}ETs occur more frequently and enlarge continuously,resulting in the formation of twin-twin interaction among{10–12}ET variants.With the increasing rolling passes,{10–12}-{10–12}DTs incorporate in the plastic deformation and dislocation slip serves as the major one to sustain plastic strain.The activities of basal<a>slip,{10–12}ETs and{10–12}-{10–12}DTs benefit in accommodating the plastic strain in sheet thickness,which contributes to the improved rolling formability in AZ31 Mg alloy sheet with bimodal non-basal texture during cryogenic rolling.

Edge crack damage analysis of AZ31 magnesium alloy hot-rolled plate improved by vertical roll pre-rolling

In the present study,through vertical roll pre-rolling of AZ31 magnesium alloy hot-rolled plate at room temperature,the effect of different vertical roll pre-rolling reduction on edge crack of the plate during flat rolling was systematically studied.The evolution of microstructure and texture in the edge and middle of the plate after vertical roll pre-rolling,heating and rolling was analyzed by using EBSD technology.The results show that during the vertical roll pre-rolling,{10–12}primary twins and{10–12}-{10–12}secondary twins dominated the edge deformation,while{10–12}primary twins dominated the middle deformation.With the increase of vertical roll pre-rolling reduction,the twin volume fraction of the edge and the middle increased,and the difference between them decreased gradually.After heating,the twin orientation caused by vertical roll pre-rolling was still maintained,and there was a significant difference in grain size between the edge and the middle.When the reduction rate of flat rolling was 30%,cracks have already appeared in the initial plate,while the vertical roll pre-rolled samples showed extremely high rolling performance.When the reduction rate of flat rolling was 50%,the 8PR sample still had no crack initiation.In addition,after flat rolling of 50%,the initial plate showed a strong basal texture,while the maximum pole density of the 8PR plate was small,and the texture distribution was very scattered,showing the characteristics of weak orientation.

Tailoring the texture and mechanical properties of 3%Y_(2)O_(3)p/ZGK200 composites fabricated by unidirectional and cross rolling followed by annealing

3%Y_(2)O_(3)p/ZGK200 composites were subjected to unidirectional rolling(UR)and cross rolling(CR)at 400℃and 350℃followed by annealing at 300℃for 1 h.The microstructure,texture and mechanical properties of rolled and annealed composites were systematically studied.The rolled composites exhibited a heterogeneous microstructure,consisting of deformed grains elongated along rolling direction(RD)and Y_(2)O_(3)particles bands distributed along RD.After annealing,static recrystallization(SRX)occurred and most deformed grains transformed into equiaxed grains.A non-basal texture with two strong T-texture components was obtained after UR while a non-basal elliptical/circle texture with circle multi-peaks was obtained after CR,indicating that rolling path had great influences on texture of the composites.After annealing process,R-texture component disappeared or weakened,as results,a non-basal texture with double peaks tilting from normal direction(ND)to transverse direction(TD)and a more random non-basal texture with circle multi-peaks were obtained for UR and CR composites,respectively.The yield strength of rolled composites after UR showed obvious anisotropy along RD and TD while a low anisotropic yield strength was obtained after CR.Some Y_(2)O_(3)particles broke during rolling.The fracture of the composites was attributed to the existence of Y_(2)O_(3)clusters and interfacial debonding between particles and matrix during tension,as a result,the ductility was not as superior as matrix alloy.

Unveiling the rolling texture variations ofα-Mg phases in a dual-phase Mg-Li alloy

LZ91 Mg-Li alloy plates with three types of initial texture were rolled by 70%reduction at both room temperature and 200℃to explore the rolling texture formation ofα-Mg phase.The results showed that the rolling texture is largely affected by the initial texture.All the samples exhibited two main texture components as RD-split double peaks texture and TD-split double peaks texture after large strain rolling.The intensity of the two texture components was strongly influenced by the initial orientation and rolling temperature.Extension twinning altered the large-split non-basal orientation to a near basal one at low rolling strain.The basal orientation induced by twinning is unstable,which finally transmitted to the RD-split texture.The strong TD-split texture formed due to slip-induced orientation transition from its initial orientation.The competition between prismatic and basal slip determined the intensity and tilt angle of the TD-split texture.By increasing the rolling temperature,the TD-split texture component was enhanced in all three samples.Limitation of extension twinning behavior and the promotion of prismatic slip at elevated temperature are the main reasons for the difference in hot and cold rolling texture.

Microstructure evolution and strengthening mechanism of high -performance powder metallurgy TA15 titanium alloy by hot rolling

Hot deformation of sintered billets by powder metallurgy(PM)is an effective preparation technique for titanium alloys,which is more significant for high-alloying alloys.In this study,Ti–6.5Al–2Zr–Mo–V(TA15)titanium alloy plates were prepared by cold press-ing sintering combined with high-temperature hot rolling.The microstructure and mechanical properties under different process paramet-ers were investigated.Optical microscope,electron backscatter diffraction,and others were applied to characterize the microstructure evolution and mechanical properties strengthening mechanism.The results showed that the chemical compositions were uniformly dif-fused without segregation during sintering,and the closing of the matrix craters was accelerated by increasing the sintering temperature.The block was hot rolled at 1200℃ with an 80%reduction under only two passes without annealing.The strength and elongation of the plate at 20–25℃ after solution and aging were 1247 MPa and 14.0%,respectively,which were increased by 24.5%and 40.0%,respect-ively,compared with the as-sintered alloy at 1300℃.The microstructure was significantly refined by continuous dynamic recrystalliza-tion,which was completed by the rotation and dislocation absorption of the substructure surrounded by low-angle grain boundaries.After hot rolling combined with heat treatment,the strength and plasticity of PM-TA15 were significantly improved,which resulted from the dense,uniform,and fine recrystallization structure and the synergistic effect of multiple slip systems.

Effect of annealing temperature on microstructure and mechanical properties of Mg-Zn-Zr-Nd alloy with large final rolling deformation

In this study,the Mg-3Zn-0.5Zr-χNd(χ=0,0.6)alloys were subjected to final rolling treatment with large deformation of 50%.The impact of annealing temperatures on the microstructure and mechanical properties was investigated.The rolled Mg-3Zn-0.5Zr-0.6Nd alloy exhibited an ultimate tensile strength of 386 MPa,a yield strength of 361 MPa,and an elongation of 7.1%.Annealing at different temperatures resulted in reduced strength and obviously increased elongation for both alloys.Optimal mechanical properties for the Mg-3Zn-0.5Zr-0.6Nd alloy were achieved after annealing at 200℃,with an ultimate tensile strength of 287 MPa,a yield strength of 235 MPa,and an elongation of 26.1%.The numerous deformed microstructures,twins,and precipitated phases in the rolled alloy could impede the deformation at room temperature and increase the work hardening rate.After annealing,a decrease in the work hardening effect and an increase in the dynamic recovery effect were obtained due to the formation of fine equiaxed grains,and the increased volume fraction of precipitated phases,which significantly improved the elongation of the alloy.Additionally,the addition of Nd element could enhance the annealing recrystallization rate,reduce the Schmid factor difference between basal and prismatic slip systems,facilitate multi-system slip initiation and improve the alloy plasticity.

Design,preparation,microstructure and mechanical property of the lightweight radiation-shielding Mg-Ta-Al composites basing differential temperature hot rolling

A novel lightweight,radiation-shielding Mg-Ta-Al layered metal-matrix composite(LMC)was successful designed by doping the extremely refractory metal(Ta)into Mg sheets.These Mg-based LMCs sheets shows excellent radiation-dose shield effect,about 145 krad·a^(−1),which is about 17 times of traditional Mg alloy,while its surface density is only about 0.9 g·cm^(−2),reducing by 60%than that of pure Ta.The quantitate relationship between radiation-dose and the materials’thickness was also confirmed to the logistic function when the surface density is in the range of 0.6-1.5 g·cm^(−2).Meantime,the rolling parameters,interface microstructure and mechanical properties in both as-rolled and annealing treated samples were evaluated.The sheets possess a special dissimilar atoms diffusion transitional zone containing an obvious inter-diffusion Mg-Al interface and the unique micro-corrugated Ta-Al interface,as well as a thin Al film with a thickness of about 10μm.The special zone could reduce the stress concentration and enhance the strength of Mg-Ta-Al LMCs.The interface bonding strength reaches up to 54-76 MPa.The ultimate tensile strength(UTS)and yield strength(TYS)of the Mg-Ta-Al sheet were high to 413 MPa and 263 MPa,respectively,along with an elongation of 5.8%.The molecular dynamics(MD)analysis results show that the two interfaces exhibit different formation mechanism,the Mg-Al interface primarily depended on Mg/Al atoms diffusion basing point defects movement,while the Ta-Al interface with a micro-interlock pining shape formed by close-packed planes slipping during high temperature strain-induced deformation process.

Online task planning method of anti-ship missile based on rolling optimization

Based on the wave attack task planning method in static complex environment and the rolling optimization framework, an online task planning method in dynamic complex environment based on rolling optimization is proposed. In the process of online task planning in dynamic complex environment,online task planning is based on event triggering including target information update event, new target addition event, target failure event, weapon failure event, etc., and the methods include defense area reanalysis, parameter space update, and mission re-planning. Simulation is conducted for different events and the result shows that the index value of the attack scenario after re-planning is better than that before re-planning and according to the probability distribution of statistical simulation method, the index value distribution after re-planning is obviously in the region of high index value, and the index value gap before and after re-planning is related to the degree of posture change.

Intelligent Fault Diagnosis Method of Rolling Bearings Based on Transfer Residual Swin Transformer with Shifted Windows

Due to their robust learning and expression ability for complex features,the deep learning(DL)model plays a vital role in bearing fault diagnosis.However,since there are fewer labeled samples in fault diagnosis,the depth of DL models in fault diagnosis is generally shallower than that of DL models in other fields,which limits the diagnostic performance.To solve this problem,a novel transfer residual Swin Transformer(RST)is proposed for rolling bearings in this paper.RST has 24 residual self-attention layers,which use the hierarchical design and the shifted window-based residual self-attention.Combined with transfer learning techniques,the transfer RST model uses pre-trained parameters from ImageNet.A new end-to-end method for fault diagnosis based on deep transfer RST is proposed.Firstly,wavelet transform transforms the vibration signal into a wavelet time-frequency diagram.The signal’s time-frequency domain representation can be represented simultaneously.Secondly,the wavelet time-frequency diagram is the input of the RST model to obtain the fault type.Finally,our method is verified on public and self-built datasets.Experimental results show the superior performance of our method by comparing it with a shallow neural network.

Carbon Fiber Breakage Mechanism in Aluminum(Al)/Carbon Fibers(CFs) Composite Sheet during Accumulative Roll Bonding(ARB) Process

We put forward a method of fabricating Aluminum(Al)/carbon fibers(CFs) composite sheets by the accumulative roll bonding(ARB) method. The finished Al/CFs composite sheet has CFs and pure Al sheets as sandwich and surface layers. After cross-section observation of the Al/CFs composite sheet, we found that the CFs discretely distributed within the sandwich layer. Besides, the tensile test showed that the contribution of the sandwich CFs layer to tensile strength was less than 11% compared with annealed pure Al sheet. With ex-situ observation of the CFs breakage evolution with-16%,-32%, and-45% rolling reduction during the ARB process, the plastic instability of the Al layer was found to bring shear damages to the CFs. At last, the bridging strengthening mechanism introduced by CFs was sacrificed. We provide new insight into and instruction on Al/CFs composite sheet preparation method and processing parameters.

Study of the Characteristics of Large-Diameter Iron Bars Obtained by Rolling at the ODHAV Foundry in the Republic of Guinea

This work consists of evaluating the quality of the mechanical parameters of large-diameter steels, i.e. 20, 25, 28 and 32, through a process of recycling scrap metal that fills garages, rubbish dumps, gutters and other abandoned sites, as well as imported concrete reinforcing steel sold in the Republic of Guinea. To carry out this important work, a number of mechanical tensile and bending tests and a microscopic analysis combining two devices, an electron microscope and a photographic camera, were carried out. The samples were taken from sampling areas in the major communes of Conakry, namely: Casse Sonfonia, Matoto and Kagbélen. The tensile strength values of the large dimensions 20, 25, 28 and 32 are given in the tables.

Improvement of Temperature Drop Model Parameters for 4200mm/3500mm Rolling of Baosteel Medium and Thick Plate

Based on the temperature situation during the rolling process of 4200 mm/3500 mm medium and thick plates at Baosteel,this article analyzes the influencing factors of temperature changes during the rolling process from the perspective of heat transfer theory and the temperature change law during the rolling process.The temperature loss during the four rolling processes is tracked on site,and the temperature drop model parameters during the rolling process of 4200mm/3500mm medium and thick plates at Baosteel are quantitatively provided.It is applied to actual rolling production and has achieved good results.

Influence of Production Sequence of Aluminum Alloy Hot Rolling on Strip Surface Quality

With the intensification of market competition in the aluminum alloy strip processing industry,it is dif-ficult to control the mass production of the same specifications,which is bound to affect the hot rolling production.This paper studied the effect of the hot rolling order of aluminum alloy on the surface quality of strip,such as roll printing,color difference,anodic oxidation,etc.,reasonable discharge sequence and corresponding optimization measures were formulated.

Shear deformation and plate shape control of hot-rolled aluminium alloy thick plate prepared by asymmetric rolling process

Asymmetric rolling （ASR）, as one of severe plastic deformation （SPD） methods to make ultra-fine materials with enhanced performance is mainly used to prepare foil and thin strip. The asymmetrical rolling was achieved by adjusting the diameters of the upper roll and the bottom roll and was used to prepare hot-rolled thick plate of 5182 aluminium alloy. The shear deformation and plate shape control were experimentally studied. The experimental results show that asymmetrical rolling has a significant effect on metal deformation stream and can somehow refine microstructure and improve the uniformity of microstructure and properties. The asymmetrical rolling process can also reduce the rolling force. However, bending of rolling plate often happens during asymmetrical rolling process. The factors affecting the bending were discussed.

Effect of calcium addition on microstructure and texture modification of Mg rolled sheets

The mechanical properties and texture of AM60（Mg-6.0Al-0.3Mn,mass fraction %） and ZXM200（Mg-1.6Zn-0.5Ca-0.2Mn） Mg alloys subjected to multi-pass hot rolling were investigated.The finer recrystallized grains usually exhibit particular preferred orientations and then alter the total texture feature of rolled sheets.Ca solid solution into Mg matrix serves to the formation of texture component with c-axis rotated away from normal direction towards transverse direction and then weakens the overall texture intensity,resulting in a similar anisotropic characteristic to RE-containing Mg alloys.

Microstructure and mechanical properties of cold-rolled Ti_(50)Ni_(47)Fe_3 shape memory alloy

Mechanical and shape memory properties of a Ti50Ni47Fe3 alloy annealed at 450-750 °C for 1 h after a cold-rolled reduction of 25% were investigated by phase transformation analysis and microstructure characterization using tensile tests, Vickers hardness tests, electrical resistivity-temperature tests, SEM and TEM. From the results of the tensile, it can be inferred that the fracture stress and yield stress decreased and the fracture elongation increased as the annealing temperature increased for the rolled Ti50Ni47Fe3 alloy. They reached stead values when the temperature was above 650 °C. The change in Vickers hardness corresponded to the change in the fracture stress and yield stress. The electrical resistivity-temperature curves suggest that a two- stage martensitic transformation（B2-R-B19′） occurred during cooling and heating. The transformation temperatures decreased to lower temperatures when the annealing temperature was increased and maintained the same after the annealing temperature reached 650 °C. TEM revealed the distinct processes occurring at elevated temperatures： recovery, polygonization, and recrystallization.

Microstructure and texture evolution during high-strain-rate superplastic deformation of coarse-grained Mg-Gd-Y-Zr rolled sheet

Microstructure and texture evolution during high-strain-rate superplastic deformation of the rolled Mg-Gd-Y-Zr sheet were investigated.The tensile tests at the strain rate of 0.01 s-1 achieved the elongations of 180%-266% in the deformation temperature range of 400-500 ℃.Post-deforming microstructures were characterized by optical microscopy,scanning electron microscopy and transmission electron microscopy,while crystallographic orientation information was obtained from macro-texture analysis.The results show that the high strain-rate superplasticity was attributed to class-I dislocation creep accommodated by dynamic recrystallization （DRX）.During preheating at 435 ℃ for 600 s,twinning-induced recrystallization occurred.The initial strain of 80% made original grains fragmented and produced homogenous DRX grains.The interaction between dynamic recrystallization and dynamic precipitation yielded out such a phenomenon that finer DRX grains were often accompanied by denser particles.The macro-texture evolution exhibited some characteristics of the crystal rotation arising from basal slip and prismatic slip despite the occurrence of DRX.

Study of residual stresses in tailor rolled blanked Al5J32-T4 sheets

Several automotive parts such as door panels have been manufactured by using load-adapted blanks for crash optimization and weight minimization. Recently, Tailor Rolled Blanks (TRB) has been introduced to remove the disadvantages of a welding process which was used in joining panel components. TRB offers better structural design capabilities due to the seamless transitions on the panels with different thicknesses. In spite of the advantages of the process, TRB leaves internal stresses in the panel. This residual stresses lower the formability of Tailor Rolled Blanked (TRBed) parts and cause cracks near severe curvature during subsequent forming processes. In this research, the residual stresses of TRBed Al5J32-T4 sheets were studied by X-ray stress analysis, and also microstructure was observed along the rolling direction. In addition, heat treatment was done after TRB process in order to compare the residual stresses to that of the TRBed sheets before the heat treatment.

Self-Learning and Its Application to Laminar Cooling Model of Hot Rolled Strip

The mathematical model for online controlling hot rolled steel cooling on run-out table （ROT for abbreviation） was analyzed, and water cooling is found to be the main cooling mode for hot rolled steel. The calculation of the drop in strip temperature by both water cooling and air cooling is summed up to obtain the change of heat transfer coefficient. It is found that the learning coefficient of heat transfer coefficient is the kernel coefficient of coiler temperature control （CTC） model tuning. To decrease the deviation between the calculated steel temperature and the measured one at coiler entrance, a laminar cooling control self-learning strategy is used. Using the data acquired in the field, the results of the self-learning model used in the field were analyzed. The analyzed results show that the self-learning function is effective.