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Analysis of Flow Structure and Calculation of Drag Coefficient for Concurrent-up Gas-Solid Flow 被引量:5
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作者 杨宁 王维 +1 位作者 葛蔚 李静海 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2003年第1期79-84,共6页
This study investigates the heterogeneous structure and its influence on drag coefficient for concurrent-up gas-solid flow. The energy-minimization multi-scale (EMMS) model is modified to simulate the variation of str... This study investigates the heterogeneous structure and its influence on drag coefficient for concurrent-up gas-solid flow. The energy-minimization multi-scale (EMMS) model is modified to simulate the variation of structure parameters with solids concentration, showing the tendency for particles to aggregate to form clusters and for fluid to pass around clusters. The global drag coefficient is resolved into that for the dense phase, for the dilute phase and for the so-called inter-phase, all of which can be obtained from their respective phase-specific structure parameters. The computational results show that the drag coefficients of the different phases are quite different, and the global drag coefficient calculated from the EMMS approach is much lower than that from the correlation of Wen and Yu. The simulation results demonstrate that the EMMS approach can well describe the heterogeneous flow structure, and is very promising for incorporation into the two-fluid model or the discrete particle model as the closure law for drag coefficient. 展开更多
关键词 drag coefficient two-phase flow multi-scale flow structure two-fluid model
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On the Coefficients of Several Classes of Bi-univalent Functions Defined by Convolution 被引量:5
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作者 Guo Dong Li Zong-tao 《Communications in Mathematical Research》 CSCD 2018年第1期65-76,共12页
In this paper, we introduce several new subclasses of the function class Σ of bi-univalent functions analytic in the open unit disc defined by convolution.Furthermore, we investigate the bounds of the coefficients |a... In this paper, we introduce several new subclasses of the function class Σ of bi-univalent functions analytic in the open unit disc defined by convolution.Furthermore, we investigate the bounds of the coefficients |a2| and |a3| for functions in these new subclasses. The results presented in this paper improve or generalize the recent works of other authors. 展开更多
关键词 analytic and univalent functions coefficient bi-univalent function Hadamard product CONVOLUTION
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Analysis of burnup performance and temperature coefficient for a small modular molten‑salt reactor started with plutonium 被引量:4
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作者 Xue‑Chao Zhao Yang Zou +1 位作者 Rui Yan Xiang‑Zhou Cai 《Nuclear Science and Techniques》 SCIE EI CAS CSCD 2023年第1期178-189,共12页
In a thorium-based molten salt reactor(TMSR),it is difficult to achieve the pure 232Th–^(233)U fuel cycle without sufficient^(233)U fuel supply.Therefore,the original molten salt reactor was designed to use enriched ... In a thorium-based molten salt reactor(TMSR),it is difficult to achieve the pure 232Th–^(233)U fuel cycle without sufficient^(233)U fuel supply.Therefore,the original molten salt reactor was designed to use enriched uranium or plutonium as the starting fuel.By exploiting plutonium as the starting fuel and thorium as the fertile fuel,the high-purity^(233)U produced can be separated from the spent fuel by fluorination volatilization.Therefore,the molten salt reactor started with plutonium can be designed as a^(233)U breeder with the burning plutonium extracted from a pressurized water reactor(PWR).Combining these advantages,the study of the physical properties of plutonium-activated salt reactors is attractive.This study mainly focused on the burnup performance and temperature reactivity coefficient of a small modular molten-salt reactor started with plutonium(SM-MSR-Pu).The neutron spectra,^(233)U production,plutonium incineration,minor actinide(MA)residues,and temperature reactivity coefficients for different fuel salt volume fractions(VF)and hexagon pitch(P)sizes were calculated to analyze the burnup behavior in the SM-SMR-Pu.Based on the comparative analysis results of the burn-up calculation,a lower VF and larger P size are more beneficial for improving the burnup performance.However,from a passive safety perspective,a higher fuel volume fraction and smaller hexagon pitch size are necessary to achieve a deep negative feedback coefficient.Therefore,an excellent burnup performance and a deep negative temperature feedback coefficient are incompatible,and the optimal design range is relatively narrow in the optimized design of an SM-MSR-Pu.In a comprehensive consideration,P=20 cm and VF=20%are considered to be relatively balanced design parameters.Based on the fuel off-line batching scheme,a 250 MWth SM-MSR-Pu can produce approximately 29.83 kg of ^(233)U,incinerate 98.29 kg of plutonium,and accumulate 14.70 kg of MAs per year,and the temperature reactivity coefficient can always be lower than−4.0pcm/K. 展开更多
关键词 Molten salt fuel Incinerate plutonium 233U production Temperature reactivity coefficient
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Influence of Density on Sound Absorption Coefficient of Fibre Board 被引量:1
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作者 Anand Nandanwar M. C. Kiran K. Ch. Varadarajulu 《Open Journal of Acoustics》 2017年第1期1-9,共9页
For acoustic applications such as theaters, cinema halls, auditoriums the data on acoustic properties i.e. sound absorption coefficient and sound transmission loss are required to evaluate the acoustic behavior of pan... For acoustic applications such as theaters, cinema halls, auditoriums the data on acoustic properties i.e. sound absorption coefficient and sound transmission loss are required to evaluate the acoustic behavior of panel products and to facilitate the necessary design computations. Fibre boards are widely used in private and commercial buildings, but not much data are available on acoustic efficiency of fibre boards. The study was carried using acoustic pulse tester based on standing wave method for evaluating sound absorption coefficient. Wood fibre boards of different densities ranging from 200 to 800 kg/m3 were taken and their sound absorption coefficients at frequencies ranging from 125 Hz to 4000 Hz were evaluated in third octave band. Noise reduction coefficient of the samples was also computed. From the study, it is observed that low density fibre board possess high sound absorption coefficient and noise reduction coefficient when compared with high density fibre boards. It was seen that sound absorption coefficient increases with decrease in density and vice versa. 展开更多
关键词 SOUND Absorption coefficient SOUND Transmission LOSS Acoustic Efficiency PANEL products
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Ecological Geochemistry of Selenium in the Production Base of Zhangqiu Green Chinese Onion 被引量:3
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作者 庞绪贵 高宗军 +1 位作者 王敏 王增辉 《Agricultural Science & Technology》 CAS 2010年第11期39-43,共5页
Based on the achievement of local ecological geochemical survey,the selenium in surface layer soil of Zhangqiu green Chinese onion within production area is systematically studied in this study.And the ecological geoc... Based on the achievement of local ecological geochemical survey,the selenium in surface layer soil of Zhangqiu green Chinese onion within production area is systematically studied in this study.And the ecological geochemical characters of selenium both in surface layer soil and in green Chinese onions are analyzed,and the relationship between the selenium in plant and soil is discussed.The results show that soil in Zhangqiu is rich in selenium,and it is suitable to develop the selenium-rich green Chinese onion products. 展开更多
关键词 Ecological geochemistry Zhangqiu green Chinese onion Selenium-rich agricultural products Available selenium Biological accumulation coefficient
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基于县域尺度的“襄十随神”城市群粮食生产时空格局演变分析
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作者 张又天 于婧 +4 位作者 唐曦文 夏建军 陈朝霞 李明 焦文轩 《湖北大学学报(自然科学版)》 CAS 2025年第1期75-83,共9页
探析粮食生产格局的变化可准确把握粮食供需情况,对科学指导粮食供需平衡、制定相关粮食补贴政策以及有效解决粮食安全问题具有重要的现实意义。基于2000—2020年湖北省“襄十随神”城市群21个县域行政区划的面板数据,采用离散系数探析... 探析粮食生产格局的变化可准确把握粮食供需情况,对科学指导粮食供需平衡、制定相关粮食补贴政策以及有效解决粮食安全问题具有重要的现实意义。基于2000—2020年湖北省“襄十随神”城市群21个县域行政区划的面板数据,采用离散系数探析其区域粮食生产稳定性,利用重心模型及标准差椭圆方法分析区域粮食生产重心的演变过程,并通过空间自相关分析区域的空间集聚分布特征。结果显示,研究区域粮食总产在研究期间内主要经历了从上升到略微下降2个阶段,而粮食生产稳定性呈现上升后陡然下降再逐渐趋于稳定;研究区域内粮食生产存在显著的空间差异,粮食生产重心整体有向东南方向移动的演变趋势,襄阳、随州已发展为全域主要粮食高产区;粮食生产空间集聚趋势加强,区域间空间溢出效应明显。为此,结合当前研究区域发展状况,提出可协调粮食生产区域与经济发展的关系,加强粮食安全在社会发展综合考核中的重视程度;因势利导、因时制宜来制定不同农业政策,优化粮食生产空间布局;推进农业生产服务体系建设,建立区域内粮食主产县域长效粮食生产利益补偿机制等,以促进“襄十随神”城市群粮食生产区域分工更加清晰合理,确保粮食生产区域协调发展。 展开更多
关键词 粮食生产 时空格局演变 “襄十随神”城市群 离散系数 标准差椭圆
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Frame-indifference of cross products,rotations,and the permutation tensor 被引量:1
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作者 Maolin Du 《Theoretical & Applied Mechanics Letters》 CAS CSCD 2020年第2期116-119,共4页
Under improper transformations,the traditional transformation laws for cross products,the permutation tensor,and rotations are incorrect.For a cross product,using a counter-example the left-hand rule is proved wrong.T... Under improper transformations,the traditional transformation laws for cross products,the permutation tensor,and rotations are incorrect.For a cross product,using a counter-example the left-hand rule is proved wrong.The unique rule for a cross product is the right-hand rule.Coordinate systems have handedness,while a cross product is frame-indifference.Since the permutation tensor is defined as a triple product including a cross product,the law for the permutation tensor is false.For a rotation,its pseudovector representation is incorrect,because the mirror is an auxiliary device to produce the virtual image rather than a new coordinate system or reference frame. 展开更多
关键词 Pseudovector Cross product IMPROPER transformation Handed coefficient PERMUTATION TENSOR
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Automated Dimensioning Method of Engineering Drawings for Mechanical Products Based on Curve Chain 被引量:1
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作者 Gui Li Peng Yang 《Computers, Materials & Continua》 SCIE EI 2020年第10期847-863,共17页
An automated method based on the curve chain was proposed for dimensioning of engineering drawings for the mechanical products.According to the internal relation between the features of 3D model feature and elements o... An automated method based on the curve chain was proposed for dimensioning of engineering drawings for the mechanical products.According to the internal relation between the features of 3D model feature and elements of 2D drawing,the curve chain was established to reflect the geometric topological structure between the elements.It divides the dimensions into the absolute dimensions within the cure chain and the relative dimensions between the curve chains.The parallel and lengthy relationship between the drawing elements of the constructed X and Y parallel matrix was solved to remove redundant elements in the curve chain and labeled the absolute dimensions of the remaining valid elements.The average minimum weight coefficient was introduced to judge the dependence on the relative dimensions between curve chains.Through the analysis of the overlap between the circular rectangular areas,including all the absolute dimensions of the curve chains,overlapping curve chains were merged,and their dimensions were rearranged to avoid the cross interference between them.The method was seamlessly integrated into the drafting module of product design software NX,and it developed an automated dimensioning system.The examples show that the system has excellent interactivity and robustness in the dimensioning of product engineering drawings.The dimension information is complete,accurate and reliable. 展开更多
关键词 Automated dimensioning engineering drawing curve chain mechanical product weight coefficient
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Impact of Education on Productivity:A Model in China
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作者 戴昌钧 高建兵 《Journal of China Textile University(English Edition)》 EI CAS 2000年第2期113-116,共4页
Improving the quality of human resources through edu-cation and training is of great strategic significance.However, few people have done in depth and systematicstudies on the relationship between education and pro-du... Improving the quality of human resources through edu-cation and training is of great strategic significance.However, few people have done in depth and systematicstudies on the relationship between education and pro-ducttvity in China. This study developed an educationproductivity transform model and empirically tested themodel using data on the most districts of China. The ba-sic notion is that the effect depends both on the capabilityresulted from education, and on the environment inwhich this capability can be exercised, the effect is a re-sult of two factors combined. 展开更多
关键词 EDUCATION - productIVITY TRANSFORM MODEL CAPABILITY function technology management coefficient
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Ratio-Cum-Product Estimator Using Multiple Auxiliary Attributes in Single Phase Sampling 被引量:4
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作者 John Kung’u Leo Odongo 《Open Journal of Statistics》 2014年第4期239-245,共7页
In this paper, we have proposed a class of ratio-cum-product estimator for estimating population mean of study variable for single phase sampling using multi-auxiliary attributes. The expressions for mean square error... In this paper, we have proposed a class of ratio-cum-product estimator for estimating population mean of study variable for single phase sampling using multi-auxiliary attributes. The expressions for mean square error are derived. An empirical study is given to compare the performance of the estimator with existing estimators. It has been found that the ratio-cum-product estimator using multiple auxiliary attributes is more efficient than mean per unit, product and ratio estimators using one auxiliary attribute, and Product and Ratio estimators using multiple auxiliary attributes in single phase sampling. 展开更多
关键词 Ratio-Cum-product ESTIMATOR MULTIPLE AUXILIARY Attributes Single Phase Sampling Bi-Serial Correlation coefficient
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Using Multivariable Linear Regression Technique for Modeling Productivity Construction in Iraq
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作者 Faiq Mohammed Sarhan Al-Zwainy Mohammed Hashim Abdulmajeed Hadi Salih Mijwel Aljumaily 《Open Journal of Civil Engineering》 2013年第3期127-135,共9页
Productivity is a very important element in the process of construction project management especially with regard to the estimation of the duration of the construction activities, this study aims at developing constru... Productivity is a very important element in the process of construction project management especially with regard to the estimation of the duration of the construction activities, this study aims at developing construction productivity estimating model for marble finishing works of floors using Multivariable Linear Regression technique (MLR). The model was developed based on 100 set of data collected in Iraq for different types of projects such as residential, commercial and educational projects. Which these are used in developing the model and evaluating its performance. Ten influencing factors are utilized for productivity forecasting by MLR model, and they include age, experience, number of the assist labor, height of the floor, size of the marbles tiles, security conditions, health status for the work team, weather conditions, site condition, and availability of construction materials. One model was built for the prediction of the productivity of marble finishing works for floors. It was found that MLR have the ability to predict the productivity for finishing works with excellent degree of accuracy of the coefficient of correlation (R) 90.6%, and average accuracy percentage of 96.3%. This indicates that the relationship between the independent and independent variables of the developed models is good and the predicted values from a forecast model fit with the real-life data. 展开更多
关键词 MULTIVARIABLE Linear Regression Techniques CONSTRUCTION productIVITY FINISHING WORK coefficient of Correlation
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Natural Solar Drying and Charcoal Production by Pyrolysis of Empty Shells of Cocoa Pods Using a Carbonisation Stove Fitted with a Chimney
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作者 Siaka Touré Adjo Christelle Ogo Modibo Sidibé 《Journal of Energy and Power Engineering》 CAS 2023年第4期109-120,共12页
The world’s production of cocoa highly has grown since 1960.In West Africa,the production reached about 3,000,000 tons in 2012.More than 50%of the world’s production of cocoa comes nowadays from Côte d’Ivoire ... The world’s production of cocoa highly has grown since 1960.In West Africa,the production reached about 3,000,000 tons in 2012.More than 50%of the world’s production of cocoa comes nowadays from Côte d’Ivoire and Ghana and Côte d’Ivoire is the biggest producer.After harvesting,the empty shells,considered as non-useful wastes,are abandoned in the fields where they become a source of pollution.That yields millions of tons of biomass that can be converted into charcoal,instead of being sources of pollution.In the present work,the drying kinetics of the empty wet shells were studied.Then,charcoal production by pyrolysis of those empty shells of cocoa pods was performed,using a carbonisation stove fitted with a chimney.The study showed that the empty shells have a high moisture content.The different phases of the drying were observed.The study compared the drying rates and the diffusion coefficients of a small sample and a big sample.Two experiences of carbonisation of the empty shells were successfully carried out.For the first experiment,the pyrolysis temperatures were recorded and the charcoal mass efficiency calculated.For the second experiment,the temperatures were higher and the result was colored charcoals.The colorations disappeared after some hours. 展开更多
关键词 Shells of cocoa pods solar drying diffusion coefficient charcoal production carbonisation stove.
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Energy consumption hierarchical analysis based on interpretative structural model for ethylene production
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作者 韩永明 耿志强 +1 位作者 朱群雄 林晓勇 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2015年第12期2029-2036,共8页
Interpretative structural model(ISM) can transform a multivariate problem into several sub-variable problems to analyze a complex industrial structure in a more efficient way by building a multi-level hierarchical str... Interpretative structural model(ISM) can transform a multivariate problem into several sub-variable problems to analyze a complex industrial structure in a more efficient way by building a multi-level hierarchical structure model. To build an ISM of a production system, the partial correlation coefficient method is proposed to obtain the adjacency matrix, which can be transformed to ISM. According to estimation of correlation coefficient, the result can give actual variable correlations and eliminate effects of intermediate variables. Furthermore, this paper proposes an effective approach using ISM to analyze the main factors and basic mechanisms that affect the energy consumption in an ethylene production system. The case study shows that the proposed energy consumption analysis method is valid and efficient in improvement of energy efficiency in ethylene production. 展开更多
关键词 Partial correlation coefficient Interpretative structural model Energy consumption Hierarchical analysis Ethylene production Chemical processes
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新质生产力水平的统计测度与时空演变特征研究 被引量:27
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作者 李阳 陈海龙 田茂再 《统计与决策》 CSSCI 北大核心 2024年第9期11-17,共7页
文章基于新质生产力的内涵和主要特征,测算了2010—2021年中国30个省份的新质生产力水平,并分析了新质生产力水平的区域差异及动态演变特征,结果显示:(1)研究期内,中国新质生产力水平整体上呈现上升趋势,地区间差异较大,形成“东高西低... 文章基于新质生产力的内涵和主要特征,测算了2010—2021年中国30个省份的新质生产力水平,并分析了新质生产力水平的区域差异及动态演变特征,结果显示:(1)研究期内,中国新质生产力水平整体上呈现上升趋势,地区间差异较大,形成“东高西低”的区域发展格局。(2)新质生产力水平存在显著的区域异质性特征,东部地区内部的新质生产力水平差异大于中西部地区,东-西部及东-中部的地区间差异是导致中国新质生产力水平区域差异扩大的主要原因。(3)从新质生产力水平的分布及演变特征来看,全国及东西部地区的新质生产力水平均存在极化现象。从时空动态演进特征看,中国新质生产力水平不存在跨越式跃迁,整体上呈现梯度上升趋势,新质生产力水平较高的省份能够发挥辐射带动作用,促进邻近省份的发展,而当邻近省份的新质生产力水平较低时,该省份将趋于保持相对稳定的状态。 展开更多
关键词 新质生产力 时空演变 Dagum基尼系数 核密度估计 空间Markov链
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中国新质生产力水平、区域差异与时空演进特征 被引量:29
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作者 王珂 郭晓曦 《统计与决策》 CSSCI 北大核心 2024年第9期30-36,共7页
文章构建新质生产力水平测度指标体系,运用熵值法测算2012—2021年中国31个省份的新质生产力水平,通过Dagum基尼系数法分析其差异及来源,最后采用空间相关性检验探索中国新质生产力的时空集聚特征和动态跃迁情况。研究发现:中国新质生... 文章构建新质生产力水平测度指标体系,运用熵值法测算2012—2021年中国31个省份的新质生产力水平,通过Dagum基尼系数法分析其差异及来源,最后采用空间相关性检验探索中国新质生产力的时空集聚特征和动态跃迁情况。研究发现:中国新质生产力水平逐年上升,但整体水平不高且存在区域差异;劳动者维度和劳动对象维度中的新质产业发展是制约新质生产力水平提升的主要因素;四大地区新质生产力水平差异较大,区域差异的主要来源始终是区域间差异;中国新质生产力水平明显集聚于高效型和低效型,且具有较强的空间稳定性;中国新质生产力水平跃迁更多转向极化型和空心型,较少转向高效型,区域协调发展战略效果不同,虹吸效应与带动效应并存。 展开更多
关键词 新质生产力 区域差异 时空演进 熵值法 基尼系数 莫兰指数
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多向加权Tsallis熵最大化导向的自动阈值分割方法 被引量:1
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作者 邹耀斌 邓世成 +3 位作者 孟祥丹 周欢 孙水发 陈鹏 《电子学报》 EI CAS CSCD 北大核心 2024年第1期129-143,共15页
受噪声或随机细节、目标和背景的大小比例、成像时的点扩散等不同因素的影响,许多图像的灰度直方图呈现为无模态、单模态、双模态或者多模态样式.为了在统一框架内处理这4种不同模态情形下的自动阈值选择问题,本文提出了一种多向加权Tsa... 受噪声或随机细节、目标和背景的大小比例、成像时的点扩散等不同因素的影响,许多图像的灰度直方图呈现为无模态、单模态、双模态或者多模态样式.为了在统一框架内处理这4种不同模态情形下的自动阈值选择问题,本文提出了一种多向加权Tsallis熵最大化导向的自动阈值分割方法(Multi-directional Weighted Tsallis Entropy,MWTE).基于新设计的反正切方向性卷积核的多尺度乘积效应,该方法将不同模态的灰度直方图转化为统一的单模态右偏灰度直方图.在4个不同方向上提取出这种特殊的单模态右偏灰度直方图后,通过多向加权策略构建出与原始图像灰度值紧密相关的加权Tsallis熵目标函数,并以该目标函数取最大值时对应的灰度值作为最终分割阈值.本文将提出的方法和3个阈值分割方法、1个软分割方法、1个活动轮廓分割方法以及1个自动聚类分割方法进行了比较.在4种不同模态情形下的4幅合成图像和50幅真实世界图像上的实验结果表明,本文提出的方法虽然在计算效率方面不占有优势,但它对不同模态的测试图像具有更稳健的分割适应性,且在量化分割精度所用的马修斯相关系数方面优于其他6个分割方法. 展开更多
关键词 阈值分割 Tsallis熵差 加权Tsallis熵 反正切方向性卷积核 多尺度乘积效应 马修斯相关系数
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Ratio-Cum-Product Estimator Using Multiple Auxiliary Attributes in Two-Phase Sampling
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作者 John Kung’u Leo Odongo 《Open Journal of Statistics》 2014年第4期246-257,共12页
In this paper, we have proposed three classes of ratio-cum-product estimators for estimating population mean of study variable for two-phase sampling using multi-auxiliary attributes for full information, partial info... In this paper, we have proposed three classes of ratio-cum-product estimators for estimating population mean of study variable for two-phase sampling using multi-auxiliary attributes for full information, partial information and no information cases. The expressions for mean square errors are derived. An empirical study is given to compare the performance of the estimator with the existing estimator that utilizes auxiliary attribute or multiple auxiliary attributes. The ratio-cum-product estimator in two-phase sampling for full information case has been found to be more efficient than existing estimators and also ratio-cum-product estimator in two-phase sampling for both partial and no information case. Finally, ratio-cum-product estimator in two-phase sampling for partial information case has been found to be more efficient than ratio-cum-product estimator in two-phase sampling for no information case. 展开更多
关键词 Ratio-Cum-product ESTIMATOR MULTIPLE AUXILIARY Attributes Two-Phase Sampling and Bi-Serial Correlation coefficient
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炉腹煤气量指数和透气阻力系数在马钢2号高炉的应用
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作者 尤石 高鹏 +3 位作者 王志堂 彭鹏 梁晨 吴示宇 《炼铁》 CAS 北大核心 2024年第2期15-19,共5页
对炉腹煤气量指数X_(BG)和透气阻力系数K在马钢2号高炉的应用进行了总结。通过对2号高炉1年多的生产数据跟踪分析,结果表明:X_(BG)控制在63~64m/min,对应炉腹煤气量V_(BG)控制在6300~6400m^(3)/min时,高炉稳定顺行,燃料比较为稳定;针对... 对炉腹煤气量指数X_(BG)和透气阻力系数K在马钢2号高炉的应用进行了总结。通过对2号高炉1年多的生产数据跟踪分析,结果表明:X_(BG)控制在63~64m/min,对应炉腹煤气量V_(BG)控制在6300~6400m^(3)/min时,高炉稳定顺行,燃料比较为稳定;针对2号高炉炉腹渣皮厚、炉腹温度整体偏低现象,风压控制在靠上限水平,K值实际控制在4.25~4.75为宜,高炉运行状态良好。认为炉腹煤气量指数和透气阻力系数都是综合操作参数,在高炉日常操作中,可以用此来判断炉况,衡量强化程度,使炉况保持稳定顺行,技术经济指标改善。 展开更多
关键词 高炉 炉腹煤气量指数 透气阻力系数 利用系数 燃料比
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改进和优化黑果枸杞及其制品中花青素测定的pH示差法 被引量:1
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作者 谭亮 杲秀珍 +2 位作者 王环 赵静 李玉林 《食品与发酵工业》 CAS CSCD 北大核心 2024年第4期267-278,共12页
建立一种基于美国官方分析化学师协会(Association of Official Analytical Chemists,AOAC)方法检测黑果枸杞及其制品中花青素含量的改进pH示差法。考察了黑果枸杞及其制品中花青素的最佳提取和检测条件,通过液相色谱-三重四级杆串联质... 建立一种基于美国官方分析化学师协会(Association of Official Analytical Chemists,AOAC)方法检测黑果枸杞及其制品中花青素含量的改进pH示差法。考察了黑果枸杞及其制品中花青素的最佳提取和检测条件,通过液相色谱-三重四级杆串联质谱法鉴别出黑果枸杞中花青素的具体化学结构,并计算出混合花青素的平均摩尔质量。通过分光光度法测得混合花青素的平均摩尔消光系数,对改进后的pH示差法进行方法学验证和花青素的含量测定。结果显示,最佳提取和检测条件如下:黑果枸杞花青素提取溶剂为盐酸-80%(体积分数)乙醇(3∶97,体积比),料液比为1∶100(g∶mL),提取温度为50℃,提取时间为30 min,缓冲溶液稀释5倍后静置平衡20 min。液相色谱-三重四级杆串联质谱法鉴别黑果枸杞中主要以矮牵牛素类花青素为主(占97.96%),黑果枸杞特有的混合花青素平均摩尔质量为912.7 g/mol,平均摩尔消光系数为29591 L/(mol·cm)。pH示差法改进后能够满足方法学验证要求,固体样品和液体样品最低检出限分别为28.2 mg/100 g、0.282 mg/100 mL。方法改进后花青素提取增长率均大于20%,静置平衡20 min后单次检测结果精密度小于0.3%。以矮牵牛素类花青素代替矢车菊素-3-O-葡萄糖苷计算花青素含量平均提高了2.41倍,能真实地反映黑果枸杞及其制品中花青素的含量。 展开更多
关键词 黑果枸杞及其制品 花青素 AOAC法 pH示差法改进 提取和检测条件优化 液相色谱-三重四级杆串联质谱法鉴别 平均摩尔质量和平均摩尔消光系数优化
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断控缝洞型碳酸盐岩立式板状油藏注采井网构建
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作者 邓兴梁 张仕帆 +2 位作者 汪鹏 王彭 张杰 《西南石油大学学报(自然科学版)》 CAS CSCD 北大核心 2024年第4期74-84,共11页
断控缝洞型碳酸盐岩油藏缝洞结构和连通关系复杂,传统井网部署易产生低产能井,需构建立体注采井网以提高产能。通过油藏数值模拟研究了不同因素对塔里木富满油田满深3和满深4井区立体注采井网波及系数的影响,并设计了先导试验方案预测... 断控缝洞型碳酸盐岩油藏缝洞结构和连通关系复杂,传统井网部署易产生低产能井,需构建立体注采井网以提高产能。通过油藏数值模拟研究了不同因素对塔里木富满油田满深3和满深4井区立体注采井网波及系数的影响,并设计了先导试验方案预测产能。结果表明,满深3井区注气井与采油井单个交错排状分布时波及系数最大;采油井纵向深度越大,波及系数越大;平面注采井距在500~1000m波及系数相对稳定,井距增至1500m时,波及系数大幅度减小。满深4井区注气井、注水井与采油井单个交错排状分布时波及系数最大。先导试验中,满深3和满深4井区分别采取“浅部注N_(2),深部采油”和“顶部注N_(2),底部注水,中部采油”的井网构建方案,阶段末采出程度分别达到21.3%与22.4%,相比于基础衰竭式开发和注水开发方案有了显著提升。 展开更多
关键词 富满油田 断控缝洞型油藏 碳酸盐岩 立体注采井网 井网构建 波及系数
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