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Optimization of synthesis of upconversion luminescence material NaYF_4:Er^(3+),Yb^(3+) nanometer-phosphor by low-temperature combustion synthesis method 被引量:6
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作者 卢利平 张希艳 《Journal of Rare Earths》 SCIE EI CAS CSCD 2013年第1期8-12,共5页
A kind of Er^3+-yb^3+ co-doped natrium yttrium fluoride nanometer-phosphor sensitive to 980 nm was syntlaeslzecl by me low-temperature combustion synthesis method, which expanded the application range of the low-tem... A kind of Er^3+-yb^3+ co-doped natrium yttrium fluoride nanometer-phosphor sensitive to 980 nm was syntlaeslzecl by me low-temperature combustion synthesis method, which expanded the application range of the low-temperature combustion synthesis (LCS) method which is always used in the synthesis of oxides and compotmd oxides. The synthesis conditions were optimized with orthogonal experiments and the optimum technological parameters were obtained. Intense upconversion emissions at 522, 540 and 653 nm corresponding to the 2H11/2, 4S3/2, and 4F9/2 transitions to the 4115/2 ground state were observed when excited by continuous wave- length (CW) laser radiation at 980 nm. The effect of the carbamide amount on the phase formation and the luminescence intensity was analyzed. The average particle size of the sample was 3040 nm. 展开更多
关键词 upconversion luminescence nanometer-phosphor orthogonal experiment LCS method rare earths
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