A new three-arms-nine-chains discotic molecule has been synthesized,and the aggregation structure of the compound was measured by x-ray diffraction,infrared spectra,polarizing microscope,etc.From these evidences,the n...A new three-arms-nine-chains discotic molecule has been synthesized,and the aggregation structure of the compound was measured by x-ray diffraction,infrared spectra,polarizing microscope,etc.From these evidences,the new discotic liquid crystal is found to have the discotic lammelar phase.展开更多
A simple uniaxial oedometric system is developed to test the elastic modulus of granular materials. The stress- strain relationship is first measured under conditions of uniaxial compression with additional lateral st...A simple uniaxial oedometric system is developed to test the elastic modulus of granular materials. The stress- strain relationship is first measured under conditions of uniaxial compression with additional lateral stress and strain, then the elastic modulus of the material is determined by the linear fitting method. It is found that the modulus is positively correlated to the grain size and negatively correlated to the container size. Arching and dragging are revealed to be the mechanism of such correlations by using the digital image correlation method and the pressure film technology based on the statistical method.展开更多
A new blend of poly(2-hydroxyethyl methacrylate) (PHEMA) with poly (ethylene glycol) (PEG) was prepared. The results from solid-state NMR indicate that the PHEMA/PEG(88:12, w/w) blend is miscible on a molecular level.
1 Introduction In the present paper,MgCl2·6H2O,FeCl3·6H2O,and CeCl3·6H2O were used as raw materials in the precipitationhydrothermal method to synthesize MgF eC e hydrotalcite.The effects of the Fe:Ce m...1 Introduction In the present paper,MgCl2·6H2O,FeCl3·6H2O,and CeCl3·6H2O were used as raw materials in the precipitationhydrothermal method to synthesize MgF eC e hydrotalcite.The effects of the Fe:Ce molar ratio on the composition,crystal structure,and thermal stability of hydrotalcite are examined.Energy-dispersive X-ray spectroscopy(EDS),X-展开更多
A new aromatic thermotropic liquid crystalline polyester-ether sulfone(PEES)was prepared from 4,4-bis(4-hydroxyphenoxy)diphenyl sulfone(BHPDS),terephthalic acid(TPA)and p-hydroxybenzoic acid(P-HBA).Some factors that a...A new aromatic thermotropic liquid crystalline polyester-ether sulfone(PEES)was prepared from 4,4-bis(4-hydroxyphenoxy)diphenyl sulfone(BHPDS),terephthalic acid(TPA)and p-hydroxybenzoic acid(P-HBA).Some factors that affected melting viscosity of polymer such as prepolymerization reaction medium and post-polymerization etc,were discussed.The liquid crystalline properties were characterized by DSC,polarizing microscope with a hot stage and WAXD measurements.展开更多
In a double-well system, we investigate theoretically the population distribution of a particle perturbed by a weak sinusoidal signal with a Gaussian white noise accompanied. Our numerical simulation shows that the pr...In a double-well system, we investigate theoretically the population distribution of a particle perturbed by a weak sinusoidal signal with a Gaussian white noise accompanied. Our numerical simulation shows that the probability of the particle staying in the right potential well, Pn, exhibits an extreme value at specific noise intensity D depending on the frequency of the sinusoidal signal, which is a key feature of stochastic resonance. This is confirmed by calculating the power spectrum of the output signal, in which the extreme value of the amplitude locates at the same noise intensity. These results provide us with a new way to quantify the stochastic resonance by measuring the population distribution of the particle.展开更多
A new kind of amphiphilic copolymer was synthesized with azo bond functional side chains, and elementary studies about formation of I,B film, UV-visible spectra and photoelectrical properties of multilayers of this ki...A new kind of amphiphilic copolymer was synthesized with azo bond functional side chains, and elementary studies about formation of I,B film, UV-visible spectra and photoelectrical properties of multilayers of this kind of amphiphilic copolymer were reported.展开更多
In this paper,a new rare earth benzoate coordination compound,[TbL_3(HL)(H_2O)]_2 (HL=C_7H_6O_2=benzoic acid) is synthesized and characterized by elemental analysis DTA,TG,DTC,and IR spectra.The title compound crystal...In this paper,a new rare earth benzoate coordination compound,[TbL_3(HL)(H_2O)]_2 (HL=C_7H_6O_2=benzoic acid) is synthesized and characterized by elemental analysis DTA,TG,DTC,and IR spectra.The title compound crystallizes in triclinic,space.group P with a=9.148(1),b=11.460(2), c=13.506(2);α=112.76(1),β=91.83(1),γ=91.99(1)°;Z=1;V=1303.3.The final R factor is 0.0235.The rare earth ion is nine-coordinated to form a distorted monocapped square antiprism.展开更多
Low-Z materials, such as carbon-based materials and Be, are major plasma-facing material (PFM) for current, even in future fusion devices. In this paper, a new type of multielement-doped carbon-based materials develop...Low-Z materials, such as carbon-based materials and Be, are major plasma-facing material (PFM) for current, even in future fusion devices. In this paper, a new type of multielement-doped carbon-based materials developed are presented along with experimental re-sults of their properties. The results indicate a decrease in chemical sputtering yield by one order of magnitude, a decrease in both thermal shock resistance and radiation-enhanced sublimation, an evidently lower temperature desorption spectrum, and combined properties of exposing to plasma.展开更多
为增加马铃薯生产品种的数量,满足目前福建不同生态区域多样性和农户的需求,福建省农业科学院作物研究所与福建省种子总站于2007年联合从中国农业科学院蔬菜花卉研究所引进了中薯7号新品种。经过多点试验、省区域试验和生产试验,于2...为增加马铃薯生产品种的数量,满足目前福建不同生态区域多样性和农户的需求,福建省农业科学院作物研究所与福建省种子总站于2007年联合从中国农业科学院蔬菜花卉研究所引进了中薯7号新品种。经过多点试验、省区域试验和生产试验,于2012年通过福建省农作物品种审定。该品种生育期88 d ,叶片绿色,茎紫色,单株块茎数6~8个,薯型椭圆形,薯皮淡黄色、光滑,薯肉乳白色(闽审薯2012005),芽眼浅,干物质含量18.38%,食味品质较好,休眠期60 d左右,产量29716~32321 kg ·hm^-2,高感晚疫病。该品种在栽培技术上应注重地块选择与翻耕起垄、备种、播种期选择、密度控制、科学肥水管理、中耕培土、病虫害防治以及及时收获等措施。展开更多
文摘A new three-arms-nine-chains discotic molecule has been synthesized,and the aggregation structure of the compound was measured by x-ray diffraction,infrared spectra,polarizing microscope,etc.From these evidences,the new discotic liquid crystal is found to have the discotic lammelar phase.
基金Supported by the National Natural Science Foundation of China under Grant Nos 11372038 and 11402023
文摘A simple uniaxial oedometric system is developed to test the elastic modulus of granular materials. The stress- strain relationship is first measured under conditions of uniaxial compression with additional lateral stress and strain, then the elastic modulus of the material is determined by the linear fitting method. It is found that the modulus is positively correlated to the grain size and negatively correlated to the container size. Arching and dragging are revealed to be the mechanism of such correlations by using the digital image correlation method and the pressure film technology based on the statistical method.
文摘A new blend of poly(2-hydroxyethyl methacrylate) (PHEMA) with poly (ethylene glycol) (PEG) was prepared. The results from solid-state NMR indicate that the PHEMA/PEG(88:12, w/w) blend is miscible on a molecular level.
基金supported by China Postdoctoral Science Foundation(No.118918)West Light Foundation of the Chinese Academy of Science
文摘1 Introduction In the present paper,MgCl2·6H2O,FeCl3·6H2O,and CeCl3·6H2O were used as raw materials in the precipitationhydrothermal method to synthesize MgF eC e hydrotalcite.The effects of the Fe:Ce molar ratio on the composition,crystal structure,and thermal stability of hydrotalcite are examined.Energy-dispersive X-ray spectroscopy(EDS),X-
文摘A new aromatic thermotropic liquid crystalline polyester-ether sulfone(PEES)was prepared from 4,4-bis(4-hydroxyphenoxy)diphenyl sulfone(BHPDS),terephthalic acid(TPA)and p-hydroxybenzoic acid(P-HBA).Some factors that affected melting viscosity of polymer such as prepolymerization reaction medium and post-polymerization etc,were discussed.The liquid crystalline properties were characterized by DSC,polarizing microscope with a hot stage and WAXD measurements.
基金Supported by the National Basic Research Program of China under Grant Nos 2011CB922104 and 2011CBA00202the National Natural Science Foundation of China under Grant No 11474154+4 种基金the Natural Science Foundation of Jiangsu Province under Grant No BK2012013the Specialized Research Fund for the Doctoral Program of Higher Education of China under Grant No 20120091110030the Dengfeng Project B of Nanjing UniversityJiangsu Key Laboratory of Advanced Manipulating Techniques of Electromagnetic Wavesthe Priority Academic Program Development of Jiangsu Higher Education Institutions
文摘In a double-well system, we investigate theoretically the population distribution of a particle perturbed by a weak sinusoidal signal with a Gaussian white noise accompanied. Our numerical simulation shows that the probability of the particle staying in the right potential well, Pn, exhibits an extreme value at specific noise intensity D depending on the frequency of the sinusoidal signal, which is a key feature of stochastic resonance. This is confirmed by calculating the power spectrum of the output signal, in which the extreme value of the amplitude locates at the same noise intensity. These results provide us with a new way to quantify the stochastic resonance by measuring the population distribution of the particle.
基金The project is supported by the Key Laboratory of Molecular Spectroscopy and Structure, National Education Commission of China
文摘A new kind of amphiphilic copolymer was synthesized with azo bond functional side chains, and elementary studies about formation of I,B film, UV-visible spectra and photoelectrical properties of multilayers of this kind of amphiphilic copolymer were reported.
文摘In this paper,a new rare earth benzoate coordination compound,[TbL_3(HL)(H_2O)]_2 (HL=C_7H_6O_2=benzoic acid) is synthesized and characterized by elemental analysis DTA,TG,DTC,and IR spectra.The title compound crystallizes in triclinic,space.group P with a=9.148(1),b=11.460(2), c=13.506(2);α=112.76(1),β=91.83(1),γ=91.99(1)°;Z=1;V=1303.3.The final R factor is 0.0235.The rare earth ion is nine-coordinated to form a distorted monocapped square antiprism.
基金The work was supported by the National Nature Science Foundation of China No.19789503.
文摘Low-Z materials, such as carbon-based materials and Be, are major plasma-facing material (PFM) for current, even in future fusion devices. In this paper, a new type of multielement-doped carbon-based materials developed are presented along with experimental re-sults of their properties. The results indicate a decrease in chemical sputtering yield by one order of magnitude, a decrease in both thermal shock resistance and radiation-enhanced sublimation, an evidently lower temperature desorption spectrum, and combined properties of exposing to plasma.
文摘为增加马铃薯生产品种的数量,满足目前福建不同生态区域多样性和农户的需求,福建省农业科学院作物研究所与福建省种子总站于2007年联合从中国农业科学院蔬菜花卉研究所引进了中薯7号新品种。经过多点试验、省区域试验和生产试验,于2012年通过福建省农作物品种审定。该品种生育期88 d ,叶片绿色,茎紫色,单株块茎数6~8个,薯型椭圆形,薯皮淡黄色、光滑,薯肉乳白色(闽审薯2012005),芽眼浅,干物质含量18.38%,食味品质较好,休眠期60 d左右,产量29716~32321 kg ·hm^-2,高感晚疫病。该品种在栽培技术上应注重地块选择与翻耕起垄、备种、播种期选择、密度控制、科学肥水管理、中耕培土、病虫害防治以及及时收获等措施。