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PLOT柱分离GC-MS法测定酿酒发酵产品中的微量丁二酮和苯乙烯 被引量:3
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作者 刘绍从 吕刚 +2 位作者 赵好力宝 李德泉 刘军 《分析测试学报》 CAS CSCD 北大核心 2006年第1期127-129,共3页
用PLOT柱分离,气相色谱-质谱联用对酿酒发酵产品中微量丁二酮和苯乙烯含量进行测定。GC条件为:毛细管色谱柱,HP-PLOTU,30m×0.32mm×10μm;载气(He)流速,1.5mL/min;进样口温度,200℃;柱温,180℃;分流比。50:1... 用PLOT柱分离,气相色谱-质谱联用对酿酒发酵产品中微量丁二酮和苯乙烯含量进行测定。GC条件为:毛细管色谱柱,HP-PLOTU,30m×0.32mm×10μm;载气(He)流速,1.5mL/min;进样口温度,200℃;柱温,180℃;分流比。50:1;进样量0.5μL。MS条件:电子轰击电离源能量。70eV;选择离子扫描方式;溶剂延迟。3.0min。结果表明:丁二酬和乙醇达到基线分离。在25min内一次完成对酿酒发酵产品中微量丁二酮和苯乙烯含量的分离测定。方法的检出限为0.01mg/L,相对标准偏差小于2.0%,平均加标回收率为95%~104%。 展开更多
关键词 plot 气相色谱-质谱 丁二酮 苯乙烯 酿酒发酵产品
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Test of Normality of Waist Measurement Data of Young Male and Female Adults based on the Quantile - Quantile Plot
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作者 F. Z. Okwonu J. N. Igabari 《Journal of Statistical Science and Application》 2017年第3期118-126,共9页
This paper investigates the normality of some real data set obtained from waist measurements of a group of 49 young adults. The quantile - quantile (Q-Q) plot and the analysis of correlation coefficients for the Q-Q... This paper investigates the normality of some real data set obtained from waist measurements of a group of 49 young adults. The quantile - quantile (Q-Q) plot and the analysis of correlation coefficients for the Q-Q plot is used to determine the normality or otherwise of the data set. In this regards, the probabilities of the quantiles were computed, modified and plotted. Thereafter the correlation coefficients for the quantile - quantile plots were obtained. Results indicate that at 0.1 level of significance, the data for young adult males of the sample were not normally distributed, and had a mean value that is within the range of low risk, healthwise, whereas the distribution of the data for young female adults showed reasonable normality, but also with a mean value that is within the range of low risk in terms of health condition. 展开更多
关键词 Correlation coefficient probability plot quantile - quantile plot test of normality waist measurement young adults.
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Home Textile Trends 2011-2012
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作者 Wang Ting 《China Textile》 2010年第9期50-52,共3页
During the China International Trade Fair for Home textiles and Accessories(Intertextile Shanghai Home textile),held from Aug.24th to 26 th,2010,in the city of Shanghai,the Intertextile Direction Trend Committee relea... During the China International Trade Fair for Home textiles and Accessories(Intertextile Shanghai Home textile),held from Aug.24th to 26 th,2010,in the city of Shanghai,the Intertextile Direction Trend Committee released the latest home textile trends for Autumn and Winter 2011 and 2012. 展开更多
关键词 Home Textile trends 2011-2012
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气相色谱-质谱法测定食用酒精中的微量丁二酮和苯乙烯 被引量:2
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作者 刘绍从 吕刚 +2 位作者 张莱 赵好力宝 孙书军 《色谱》 CAS CSCD 北大核心 2006年第2期210-210,共1页
关键词 plot柱(plot column) 气相色谱-质谱(gas chromatography-mass spectrometry) 丁二酮(2 3-butanedione) 苯乙烯(styrene) 食用酒精(drinkable alcohol)
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Research and Development Trend of Shape Control for Cold Rolling Strip 被引量:23
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作者 Dong-Cheng Wang Hong-Min Liu Jun Liu 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2017年第5期1248-1261,共14页
Shape is an important quality index of cold rolling strip. Up to now, many problems in the shape control domain have not been solved satisfactorily, and a review on the research progress in the shape control domain ca... Shape is an important quality index of cold rolling strip. Up to now, many problems in the shape control domain have not been solved satisfactorily, and a review on the research progress in the shape control domain can help to seek new breakthrough directions. In the past 10 years, researches and applications of shape control models, shape control means, shape detection technology, and shape con- trol system have achieved significant progress. In the aspect of shape control models, the researches in the past improve the accuracy, speed and robustness of the models. The intelligentization of shape control models should be strengthened in the future. In the aspect of the shape control means, the researches in the past focus on the roll opti- mization, mill type selection, process optimization, local strip shape control, edge drop control, and so on. In the future, more attention should be paid to the coordination control of both strip shape and other quality indexes, and the refinement of control objective should be strengthened. In the aspects of shape detection technology and shape control system, some new types of shape detection meters and shape control systems are developed and have successfully indus- trial applications. In the future, the standardization of shape detection technology and shape control system should be promoted to solve the problem of compatibility. In general,the four expected development trends of shape control for cold roiling strip in the future are intelligentization, coordi- nation, refinement, and standardization. The proposed research provides new breakthrough directions for improv- ing shape quality. 展开更多
关键词 Cold rolling strip - Shape control Development trend Theory models Shape detectionControl system
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中国东北地区气象数据的空间平稳性检验$ 被引量:4
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作者 许家琦 李颜伶 舒红 《华中师范大学学报(自然科学版)》 CAS 北大核心 2014年第2期279-283,共5页
现有的空间统计模型多是以随机场平稳为前提条件来建立的,然而在现实中这个前提条件未必成立.因此在统计建模前,需要检验数据在空间上的平稳性.针对中国东北地区的气象数据(日气温、日风速和月降水),设计了散点图法、趋势线法和邻域圆... 现有的空间统计模型多是以随机场平稳为前提条件来建立的,然而在现实中这个前提条件未必成立.因此在统计建模前,需要检验数据在空间上的平稳性.针对中国东北地区的气象数据(日气温、日风速和月降水),设计了散点图法、趋势线法和邻域圆法的空间数据平稳性检验算法.结果显示日气温值有南高北低的趋势,月降水值有东高西低,南高北低的趋势,日风速值在空间上平稳.实验分析结果较好地反映了东北地区气象变化规律,说明了所设计的空间数据平稳性检验方法的有效性. 展开更多
关键词 平稳性 空间数据 散点图法 趋势线法 邻域圆法
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递归趋势分析在汉语语音声韵母切分中的应用研究 被引量:5
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作者 闫润强 祖漪清 朱贻盛 《信号处理》 CSCD 北大核心 2007年第4期521-525,共5页
基于隐马尔可夫模型(HMM)的连续语音自动切分方法由于较高的切分精度得到了广泛的应用,然而其切分结果还不能够直接应用于基于脚本的语音拼接合成系统,需要音素边界的再调整。本文分析了不同的汉语语音音素的非线性动力学物理模型在其... 基于隐马尔可夫模型(HMM)的连续语音自动切分方法由于较高的切分精度得到了广泛的应用,然而其切分结果还不能够直接应用于基于脚本的语音拼接合成系统,需要音素边界的再调整。本文分析了不同的汉语语音音素的非线性动力学物理模型在其递归图(RP)上的表现,通过递归趋势(RT)这一衡量系统稳定性程度的量化参数,揭示了语音产生过程中的不稳定性。结合基于HMM的连续语音初始切分结果,从定位语音动力学特性突变点的角度,调整声韵母切分边界,在10、20、30毫秒基准范围内,切分精度分别提高了13.88%、4.19%、3.19%。 展开更多
关键词 隐马尔可夫模型 基于脚本的语音拼接合成系统 语音动力学 递归图 递归趋势分析
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我国情节犯立法的历程与趋向 被引量:13
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作者 张庆立 《犯罪研究》 2021年第2期72-84,共13页
与域外刑法往往坚持"立法定性而不定量"不同,情节犯是我国刑事立法的特色。我国的情节犯立法源起于1979年《刑法》,后在1997年《刑法》修订时得以发展。经数次刑法修正后,截至目前,情节犯的数量已经达到135个罪名。除危害国... 与域外刑法往往坚持"立法定性而不定量"不同,情节犯是我国刑事立法的特色。我国的情节犯立法源起于1979年《刑法》,后在1997年《刑法》修订时得以发展。经数次刑法修正后,截至目前,情节犯的数量已经达到135个罪名。除危害国家安全罪一章没有情节犯外,其他章节均有情节犯的规定,且情节犯的法定刑已经涵盖了所有的主刑与附加刑。从趋势看,情节犯立法呈现的动向为:修正数量日益增多,且以增设新罪名为主;修正为情节犯和修正出情节犯并存,但修正为情节犯的数量居多;多为侵害非个人法益的犯罪;刑罚配置从重等。 展开更多
关键词 情节犯 刑事立法 发展历程 立法特点 发展趋向
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西江下游月枯季径流特征研究 被引量:3
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作者 陈立华 刘为福 +3 位作者 潘子豪 滕翔 严诚 张利娜 《水利水电技术》 CSCD 北大核心 2018年第9期49-55,共7页
通过分析变化环境下西江下游枯季径流变化特征,为西江流域枯季水量的统一调度提供参考。基于梧州水文站1950—2015年逐日流量资料,采用Mann-Kendall趋势分析法、R/S法、滑动T检验等多种方法分析了枯季平均流量和各月径流分配均匀程度和... 通过分析变化环境下西江下游枯季径流变化特征,为西江流域枯季水量的统一调度提供参考。基于梧州水文站1950—2015年逐日流量资料,采用Mann-Kendall趋势分析法、R/S法、滑动T检验等多种方法分析了枯季平均流量和各月径流分配均匀程度和变化幅度的趋势性和变异性。结果表明:西江下游60多年来枯季流量未发生变异,且以5. 11 m3/(s·年)的增长率呈不显著增长趋势,具正持续性。枯季各月流量分配的均匀度显著地趋于均匀,变化幅度显著减小。枯季月均流量连续最小3个月主要在1—3月,可见后枯水期补水形势依然严峻。采用PPCC法对以枯季流量序列为频率分析特征指标的5种假设分布进行适用性量化裁定,得出LP-Ⅲ型分布更适用于表征西江枯季流量的频率分布,该分布显示极端枯水事件发生频率有从前期的1. 52%到后期的4. 55%的增大趋势。 展开更多
关键词 枯季径流 趋势变化 变异特征 频率分析 PPCC检验法 西江
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王蒙小说的“非情节化”解读 被引量:1
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作者 刘慧敏 《齐齐哈尔大学学报(哲学社会科学版)》 2008年第1期106-107,共2页
80年代初中期,王蒙的小说大都是运用一些"非情节化"的因素来结构的,通过大量的心理描写来大跨度地思考历史和现实,充分发挥自己的艺术才华,展现了小说艺术的新面貌。
关键词 意识流小说 非情节化 话语类型
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Investigating long-term trends of climate change and their spatial variations caused by regional and local environments through data mining 被引量:2
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作者 XIE Yichun ZHANG Yang +3 位作者 LAN Hai MAO Lishen ZENG Shi CHEN Yulu 《Journal of Geographical Sciences》 SCIE CSCD 2018年第6期802-818,共17页
Climate change is a global phenomenon but is modified by regional and local environmental conditions.Moreover,climate change exhibits remarkable cyclical oscillations and disturbances,which often mask and distort the ... Climate change is a global phenomenon but is modified by regional and local environmental conditions.Moreover,climate change exhibits remarkable cyclical oscillations and disturbances,which often mask and distort the long-term trends of climate change we would like to identify.Inspired by recent advancements in data mining,we experimented with empirical mode decomposition(EMD)technique to extract long-term change trends from climate data.We applied GIS elevation model to construct 3 D EMD trend surface to visualize spatial variations of climate change over regions and biomes.We then computed various time-series similarity measures and plot them to examine spatial patterns across meteorological stations.We conducted a case study in Inner Mongolia based on daily records of precipitation and temperature at 45 meteorological stations from 1959 to 2010.The EMD curves effectively illustrated the long-term trends of climate change.The EMD 3 D surfaces revealed regional variations of climate change,while the EMD similarity plots disclosed cross-station deviations.In brief,the change trends of temperature were significantly different from those of precipitation.Noticeable regional patterns and local disturbances of the changes in both temperature and precipitation were identified.The trends of change were modified by regional and local topographies and land covers. 展开更多
关键词 climate change empirical mode decomposition Inner Mongolia similarity plot trend surface
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标号模糊阴影效果设计与实现
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作者 康帅宁 聂芸 《电子设计工程》 2018年第3期70-75,80,共7页
文中针对现有的二维态势标绘系统中标号视觉效果单一,不具备立体显示效果的问题,结合二维态势标绘系统的实际应用场景,构建了适合二维态势标绘系统的阴影模型和光照模型,提出了一种通过平行投影和图像滤波的技术手段给二维标号添加模糊... 文中针对现有的二维态势标绘系统中标号视觉效果单一,不具备立体显示效果的问题,结合二维态势标绘系统的实际应用场景,构建了适合二维态势标绘系统的阴影模型和光照模型,提出了一种通过平行投影和图像滤波的技术手段给二维标号添加模糊阴影的方法。结合一系列的对比实验,对比了均值滤波、高斯滤波和中值滤波3种滤波手段对阴影的模糊效果,实现了二维标号阴影的模糊效果。通过给标号添加模糊阴影,改善了标号的可视化效果,提升了二维态势标绘系统的能力。 展开更多
关键词 标号 模糊阴影 战场态势可视化 态势标绘 高斯滤波 均值滤波
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Global changes explain the long-term demographic trend of the Eurasian common lizard (Squamata: Lacertidae)
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作者 Jose L.HORREO Patrick S.FITZE 《Current Zoology》 SCIE CAS CSCD 2022年第2期221-228,共8页
The demographic trend of a species depends on the dynamics of its local populations,which can be compromised by local or by global phenomena.However,the relevance of local and global phenomena has rarely been investig... The demographic trend of a species depends on the dynamics of its local populations,which can be compromised by local or by global phenomena.However,the relevance of local and global phenomena has rarely been investigated simultaneously.Here,we tested whether local phenomena compromised a species'demographic trend using the Eurasian common lizard Zootoca vivipara,the terrestrial reptile exhibiting the widest geographic distribution,as a model species.We analyzed the species'ancient demographic trend using genetic data from its 6 allopatric genetic clades and tested whether its demographic trend mainly depended on single clades or on global phenomena.Zootoca vivipara's effective population size increased since 2.3 million years ago and started to increase steeply and continuously from 0.531 million years ago.Population growth rate exhibited 2 maxima,both occurring during global climatic changes and important vegetation changes on the northern hemisphere.Effective population size and growth rate were negatively correlated with global surface temperatures,in line with global parameters driving long-term demographic trends.Zootoca vivipara's ancient demography was neither driven by a single clade,nor by the 2 clades that colonized huge geographic areas after the last glaciation.The low importance of local phenomena,suggests that the experimentally demonstrated high sensitivity of this species to short-term ecological changes is a response in order to cope with short-term and local changes.This suggests that what affected its long-term demographic trend the most,were not these local changes/responses,but rather the important and prolonged global climatic changes and important vegetation changes on the northern hemisphere,including the opening up of the forest by humans. 展开更多
关键词 ancient demographic trend anthropological activity Bayesian Skyline plots early humans Eemian interglacial Eurasian common lizard mid-Brunhes event
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Assessment and Inventory of Forest Ecosystems Biodiversity: Case Study for Karelian Isthmus of Leningrad Region, Russia
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作者 Alexander S. Alekseev 《Open Journal of Ecology》 2018年第5期305-323,共19页
Regular grid of permanent sample plots (PSP) of ICP-Forests monitoring system was used for forest ecosystems biodiversity assessments and inventory. The supplementary features were added to the PSP structure to conduc... Regular grid of permanent sample plots (PSP) of ICP-Forests monitoring system was used for forest ecosystems biodiversity assessments and inventory. The supplementary features were added to the PSP structure to conduct biological diversity census: eight sample plots 1 × 1 m for geo-botanical description;two sample plots of 5 × 5 m each for description of the PSP’s undergrowth;one 25 × 25 m plot for coarse woody debris estimations;four soil inventory pits. The total number of PSP amounted to 248. Total data used are as following: 1) 1984 geo-botanical descriptions of vegetation belonging to ground cover layers made on 1 × 1 m sample plots;2) 496 descriptions of undergrowth on 5 × 5 m sample plots;3) 178 descriptions of woody debris on 25 × 25 m sample plots;4) 496 descriptions of soil inventory pits. General statistical indicators characterizing forest land cover diversity were calculated. Statistic indicators of α-diversity for the Karelian Isthmus forest vegetation cover have the following values: 1) m (mean number of species per PSP) = 26 species;2) σ (standard deviation) = 9.5 species;3) v (variation coefficient) = 36.5%;4) Р (deviation amplitude) = 60 – 7 = 53 species. β – diversity of forest ecosystems as well as γ – diversity also was studied on the base of information collected on the same regular grid of sample plots. It appears that sample plots distribution by species diversity gradation is well described by the standard curve of normal distribution for the entire Karelian Isthmus forest (determination coefficient of the curve being 95.2%) as well as for each type of forest. Hence, the criterion (standard) of biodiversity for forest ecosystems can be defined as the mean value of alpha diversity for each forest type group – m;and the standard deviation – σ, as a tool for assessing deviations from the standard. PSP locations are fixed using GPS technology, this allows biodiversity assessments at the same place in the next years for biodiversity trends estimations and consist the frame for systematic biodiversity inventory. 展开更多
关键词 Plant BIODIVERSITY ICP-Forests Program Forest ECOSYSTEMS α- β- γ-Diversity Regular Grid of Sample plotS BIODIVERSITY Standards.
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马克思小土地所有制思想对新时期土地改革的启示
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作者 王竹苗 魏人山 《玉林师范学院学报》 2015年第4期62-66,共5页
为了新一轮人口城镇化建设和社会主义新农村建设的健康发展,必须要进行相应农村土地制度的改革。在对农村土地制度如何改革的讨论中,一直有持土地私有化的主张。这种主张其实质就是坚持小土地所有制。马克思恩格斯曾对于小土地所有制进... 为了新一轮人口城镇化建设和社会主义新农村建设的健康发展,必须要进行相应农村土地制度的改革。在对农村土地制度如何改革的讨论中,一直有持土地私有化的主张。这种主张其实质就是坚持小土地所有制。马克思恩格斯曾对于小土地所有制进行了深入研究,认为它是一种落后的土地所有制形式,会随着时代的发展而逐渐消亡。认真学习马克思有关于小土地所有制的思想,有助于我们深刻认识土地制度发展规律,自觉抵制土地私有化主张,积极坚持党的土地政策。 展开更多
关键词 土地私有化思潮 小土地所有制 土地集体所有
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PEAK IDENTIFICATION FROM INTERACTION INDEX IN REVERSED-PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY
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作者 陈农 张玉奎 卢佩章 《Science China Chemistry》 SCIE EI CAS 1992年第12期1425-1433,共9页
The interaction index c which was derived from the fundamental retention equationlogk’ =a + cC_B in reversed--phase high--performancc liquid chromatography (RP-HPLC) quan-titatively describes the difference in the in... The interaction index c which was derived from the fundamental retention equationlogk’ =a + cC_B in reversed--phase high--performancc liquid chromatography (RP-HPLC) quan-titatively describes the difference in the interaction between solute--strong. solvent andsolute--weak solvent; it has shown to be a constant for a specific solute even when columnsystems with different C18 packings are used. The theoretical basis for peak identificationby using interaction index has been proposed, which was based on the a,c values on stan-dard C18 column by utilizing linear a-a plots on column pairs and the linear relationship be-tween parameters a and c for the structural related compounds. Through the establishmentof parameters a,c data based on the standard C18 column for a certain type of compounds,the retention of thesc compounds on various C18 columns can be predicted. Typical exam-ples have been given to verify the correctness of this method. 展开更多
关键词 peak identification REVERSED-PHASE high-performance liquid chromatography interaction INDEX c HYDROPHOBIC INDEX α LINEAR α-α plotS on column PAIRS LINEAR α-c relationship structural related compounds
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2015—2020年口服轮状病毒活疫苗的趋势分析和质量评价
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作者 张丽君 石岩 +2 位作者 刘东梅 刘晨鸣 刘晓凡 《国际生物制品学杂志》 CAS 2021年第5期259-262,共4页
目的统计分析我国2015—2020年口服轮状病毒活疫苗质量属性检测数据,评价其质量可控性和工艺稳定性。方法根据口服轮状病毒活疫苗注册标准和中国药典(2010、2015、2020年版)规定的方法对634批口服轮状病毒活疫苗的病毒滴度、热稳定性、... 目的统计分析我国2015—2020年口服轮状病毒活疫苗质量属性检测数据,评价其质量可控性和工艺稳定性。方法根据口服轮状病毒活疫苗注册标准和中国药典(2010、2015、2020年版)规定的方法对634批口服轮状病毒活疫苗的病毒滴度、热稳定性、抗生素残留量、渗透压以及pH进行检测,应用Minitab和GraphPad数据软件对检测结果进行单值移动极差控制图分析、方差分析和箱线图分析。结果2015—2020年634批口服轮状病毒活疫苗的病毒滴度均在每毫升5.5~7.0 lg半数细胞培养物感染量(50%cell culture infectious does,CCID_(50)),热稳定性试验病毒滴度均不低于5.5 lgCCID_(50)/ml、滴度下降不大于1.0 lg CCID_(50)/ml、抗生素残留量、渗透压以及pH均在国家标准范围及企业内控标准范围内。结论2015—2020年的口服轮状病毒活疫苗产品有较好的质量可控性,生产工艺稳定。 展开更多
关键词 轮状病毒疫苗 方差分析 箱线分析 趋势分析
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