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4,4′-二苯乙烯二甲酸合成工艺优化的研究
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作者 单玉才 何南峰 +1 位作者 徐昱玮 张万青 《化工文摘》 2007年第1期45-46,共2页
文章简要介绍了几种4,4′-二苯乙烯二甲酸合成工艺路线,重点叙述了对甲基苯甲酸用硫黄脱氢二聚生成4,4′-二苯乙烯二甲酸在原料配比、反应时间、溶剂的选择及碱溶与酸析几个方面工艺优化的内容。
关键词 4 4’-二苯乙烯二甲酸 对甲基苯甲酸 硫黄 工艺研完
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Preparation, Characterization and Biological Activity Studies of New Azo Compounds
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作者 Mouayad. N. Mohammed 《Journal of Chemistry and Chemical Engineering》 2012年第10期885-888,共4页
A new series of azo were derived from 2,5-di(p-amino phenyl)-3,6-diphenyl pyrazine in the presence of benzoic acid, salicylic acid, p-amino salicylic acid, p-methoxy phenol and pmethyl phenol. The structures of the ... A new series of azo were derived from 2,5-di(p-amino phenyl)-3,6-diphenyl pyrazine in the presence of benzoic acid, salicylic acid, p-amino salicylic acid, p-methoxy phenol and pmethyl phenol. The structures of the synthesized compounds were determined on the basis of their FTIR, UV (ultraviolet), elemental analysis and H-NMR (H-nuclear magnetic resonance) spectral date. The purity of synthesized compounds was checked by performing TLC (thin layer chromatography). The antibacterial activity was evaluated in DMSO (dimethyl sulfoxide). 展开更多
关键词 PYRAZINE benzoic acid salicylic acid p-amino salicylic acid p-methoxy phenol p-methyl phenol.
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