Effects of the flow pattern of intertubular liquid film on mass and heat transfer synergies in a falling-film dehumidification system with horizontal pipes are studied.A flow model of the dehumidifying solution betwee...Effects of the flow pattern of intertubular liquid film on mass and heat transfer synergies in a falling-film dehumidification system with horizontal pipes are studied.A flow model of the dehumidifying solution between horizontal pipes is established using Fluent software,the rule of transitions of the flow pattern between pipes is studied,critical Reynolds numbers of flow pattern transitions are obtained,and the accuracy of the model is verified by experiments.The mass transfer synergy angle and heat transfer synergy angle are respectively used as evaluation criteria for the mass transfer synergy and heat transfer synergy,and distribution laws of the synergy angles for droplet,droplet columnar and curtain flow patterns are obtained.Simulation results show that the mass transfer synergy angles corresponding to droplet,droplet columnar and curtain flow patterns all rise to a plateau with time.The mean mass-transfer synergy angle is 98°for the droplet flow pattern,higher than 96.5°for the droplet columnar flow pattern and 95°for the curtain flow pattern.The results show that the mass transfer synergy of the droplet flow pattern is better than that of the droplet columnar flow pattern and that of the curtain flow pattern.展开更多
In this paper a systematic ferromagnetic resonance study shows that an in-plane magnetic anisotropy in the patterned micron octagon permalloy (Ni80Fe20) elements is mainly determined by the element geometry. The eas...In this paper a systematic ferromagnetic resonance study shows that an in-plane magnetic anisotropy in the patterned micron octagon permalloy (Ni80Fe20) elements is mainly determined by the element geometry. The easy-axis is along the edge of the elements, and the hard-axis is along the diagonal. The shape anisotropy of the octagon elements is determined by square and equilateral octagon, and the theoretical calculation was studied on the shape anisotropy. The shape anisotropy of rectangular was calculated by using the same theory.展开更多
CoNiFe patterned films with rectangular elements, all 600-nm wide but of different lengths, were fabricated and inves- tigated by ferromagnetic resonance experiment and micromagnetic simulation. An in-plane magnetic u...CoNiFe patterned films with rectangular elements, all 600-nm wide but of different lengths, were fabricated and inves- tigated by ferromagnetic resonance experiment and micromagnetic simulation. An in-plane magnetic uniaxial anisotropy was exhibited, and its value increases with the increase of the aspect ratio of the elements, which was fitted by the model, including a quasi-ellipsoid demagnetizing field and a non-uniform demagnetizing field. The relative importance of the non- uniform demagnetizing field decreased from 0.26 to 0.16 with the increase of the length-width aspect ratio of the patterned element from 1.5 to 10. The demagnetizing factors in the three principal axes were determined from the experimental data of ferromagnetic resonance, which agreed reasonably well with the values calculated by micromagnetic simulation. The calculation also indicated that the interaction between elements could be neglected when the edge-to-edge spacing between neighboring elements was larger than 3 μm in our patterned films.展开更多
A nearly free sustained copper (Cu) film system has been successfully fabricated by thermal evaporation deposition of Cu atoms on silicone oil surfaces, and a characteristic ordered pattern has been systematically s...A nearly free sustained copper (Cu) film system has been successfully fabricated by thermal evaporation deposition of Cu atoms on silicone oil surfaces, and a characteristic ordered pattern has been systematically studied. The ordered pattern, namely, band, is composed of a large number of parallel key-formed domains with different width w but nearly uniform length L; its characteristic values of w and L are very susceptible to the growth period, deposition rate and nominal film thickness. The formation mechanism of the ordered patterns is well explained in terms of the relaxation of the internal stress in the films, which is related to the nearly zero adhesion of the solid-liquid interface. By using a two-time deposition method, it is confirmed that the ordered patterns really form in the vacuum chamber.展开更多
The deformation measurement of electrosynthesized polythiophene(Pth) thin films is difficult because of the small thickness and highflexibility of the specimen. An electronic speckle patterninterferom- etry (ESPI) met...The deformation measurement of electrosynthesized polythiophene(Pth) thin films is difficult because of the small thickness and highflexibility of the specimen. An electronic speckle patterninterferom- etry (ESPI) method is used to measure the deformation ofPth films of thicknesses in the range of 4-65 μm . Theirstress-strain curves are obtained. It is found that the mechanicalproperties of Pth films are sensitive to the specimen thickness. Thetensile strength increases with decreasing thickness of thin filmfrom 10 μm. The influence of the electrochemical synthesisconditions on the mechanical properties of Pth films is also dis-Cussed.展开更多
Preparation and photo-patterning characteristics of organic-inorganic hybrid thin film containing latent pigment by using photo-acid-generator (PAG) and microwave irradiation have been investigated. The acrylic thin f...Preparation and photo-patterning characteristics of organic-inorganic hybrid thin film containing latent pigment by using photo-acid-generator (PAG) and microwave irradiation have been investigated. The acrylic thin film modified with methoxysilane containing PAG was formed on a glass substrate and irradiated with ultraviolet rays to promote sol-gel reaction by catalytic action of acid which was generated from PAG. And then the film was hardened with microwave irradiation, yielding organic-inorganic hybrid polymer film having hardness, highly transparency and strong adhesion with a glass substrate. Since this reaction only occurred in the optically (UV) irradiated regions, by exploiting the difference between the adhesivenesses of these regions photo-irradiated through photomask with a glass substrate, it was possible to form a patterned film with pitch of 100 to 50 μm by a simple lift-off method. A pigment-containing film using latent pigments (with subtractive three primary colors of coloring materials) and a patterned film were prepared, and it was possible to make these films multi-colored by varying the mixing ratio of the pigments. This multi-colored film-preparation method is effective for simply and efficiently forming a color-filter film by applying optical and microwave irradiation.展开更多
Furrow irrigation with film-mulched agricultural beds is being promoted in the arid region of northwest China because it improves water utilization. Two-dimensional infiltration patterns under film-mulched furrows can...Furrow irrigation with film-mulched agricultural beds is being promoted in the arid region of northwest China because it improves water utilization. Two-dimensional infiltration patterns under film-mulched furrows can provide guidelines and criteria for irrigation design and operation. Our objective was to investigate soil water dynamics during ponding irrigation infiltration of mulched furrows in a cross-sectional ridge-furrow configuration, using laboratory experiments and mathematical simulations. Six experimental treatments, with two soil types (silt loam and sandy loam), were investigated to monitor the wetting patterns and soil water distribution in a cuboid soil chamber. Irrigation of mulched furrows clearly increased water lateral infiltration on ridge shoulders and ridges, due to enhancement of capillary driving force. Increases to both initial soil water content (SWC) and irrigation water level resulted in increased wetted soil volume. Empirical regression equations accurately estimated the wetted lateral distance (Rl) and downward distance (Rd) with elapsed time in a variably wetted soil medium. Optimization of model parameters followed by the Inverse approach resulted in satisfactory agreement between observed and predicted cumulative infiltration and SWC. On the basis of model calibration, HYDRUS-2D model can accurately simulate two-dimensional soil water dynamics under irrigation of mulched furrows. There were significant differences in wetting patterns between unmulched and mulched furrow irrigation using HYDRUS-2D simulation. The Rd under the mulched furrows was 32.14% less than the unmulched furrows. Therefore, film-mulched furrows are recommended in a furrow irrigation system.展开更多
The development of stationary patterns on a thin polymer surface subject to an electric field is studied by means of the hexagonal-planform weakly nonlinear stability analysis and numerical simulations. The time evolu...The development of stationary patterns on a thin polymer surface subject to an electric field is studied by means of the hexagonal-planform weakly nonlinear stability analysis and numerical simulations. The time evolution of the interface between the air and the polymer film on the unbounded spatial domain is described by a thin film equation, incorporating the electric driving force and the surface diffusion.The nonlinear interfacial growth includes the amplitude equations and superposition of one-dimensional structures at regular orientations. The pattern selection is driven by the subcritical instability mechanism in which the relative thickness of the polymer film plays a critical role.展开更多
A kinetics approach is developed for the geometrically nonlinear analysis of photo-induced wrinkling of glassy twist nematic films on soft elastic substrates.In this way,the problem is reduced to finding the steady st...A kinetics approach is developed for the geometrically nonlinear analysis of photo-induced wrinkling of glassy twist nematic films on soft elastic substrates.In this way,the problem is reduced to finding the steady state of an overdamped evolution system according to a kinetic law,rather than directly solving the coupled nonlinear equations.This enables one to account for the complicated director distribution and obtain the precise wrinkling morphology of the film.Though the approach proposed here is for a twist nematic film,it can be extended to study glassy nematic films with other director distributions.展开更多
Formation of copper wiring on a polyimide film by laser irradiation to a stable copper-complex film consisting of glyoxylic acid copper complex and methylamine copper complex in air has been investigated. A stable met...Formation of copper wiring on a polyimide film by laser irradiation to a stable copper-complex film consisting of glyoxylic acid copper complex and methylamine copper complex in air has been investigated. A stable metallic copper on the polyimide film was precipitated even in air. Since this copper was generated only in the laser-irradiated parts, direct patterning of copper wiring was possible. It was also found that copper was precipitated by electroless copper plating on the laser-deposited copper wiring and it was possible to thicken the copper wiring by this precipitation. The resistivity of the copper wiring was almost the same as that of the bulk of metallic copper. The developed method—combining laser irradiation to a copper-complex-coated film and electroless copper plating—enables the high-speed deposition of fine copper wiring on a polyimide film in air by a printing process, indicating an inexpensive and useful process for fabricating copper wiring without high vacuum facility and heat-treatment under inert gas.展开更多
The BLU (back light unit) is the core component of the LCD for notebook, mobile-phone, navigation, as well as large sized TV, PID (public information display), etc. In order to enhance optical efficiency of LCD, optic...The BLU (back light unit) is the core component of the LCD for notebook, mobile-phone, navigation, as well as large sized TV, PID (public information display), etc. In order to enhance optical efficiency of LCD, optical films with the uniform prism patterns have been used for BLU by stacking two films up orthogonally. In this case, light interference-phenomenon occurred such as Morie, wet-out, u-turning, etc. It caused several problems such as low brightness, spots and stripes in LCD. Recently, the high-luminance micro complex prism patterns are actively studied to avoid the light interference-phenomenon and enhance the optical efficiency. In this study, the roll master to manufacture complex micro prism pattern film was machined by using the high precision lathe. The machined patterns on the roll master were 50, 45, 40, 35, 30, 25, 20, 15, 10 and 5 μm in the pitch with 25.0, 22.5, 20.0, 17.5, 15.0, 12.5, 10.0, 7.5, 5.0 and 2.5 μm in the peak height, respectively. The roll was 2 000 mm in length and 320 mm in diameter. The electroplated roll by copper and the natural single crystal diamond tool was used for machining the patterns. The cutting force was measured and analyzed for each cutting condition by using the dynamometer. The chips and the surfaces after being machined were analyzed by SEM and microscope.展开更多
Patterning technology of ferrite and insulating material in multilayer ceramic devices is proposed. In the conventional technology, the different ceramic materials such as the ferrite and the insulating material have ...Patterning technology of ferrite and insulating material in multilayer ceramic devices is proposed. In the conventional technology, the different ceramic materials such as the ferrite and the insulating material have been prepared in the form of the each different green sheet, and then they have been stacked each other. Otherwise the different material has filled cavities that were formed by a mechanical punching in advanced. In our proposing technology, arbitrary patterning of the different ceramic material inside the same green sheet is possible. In this process, the arbitrary shape of the through pattern is formed in the green sheet of the base material by making use of photo resist films as sacrifice patterns, and then the base material is masked by the patterned photo resist film. After filling the slurry of the different material into the through pattern of the base material passing the resist mask, the pattern of the different ceramic material in the green sheet is achieved. In the present paper, the ferrite magnetic material and the alumina-glass composite material are used. The patterned structure inside the green sheet is obtained. The slurry preparation, the thickness of the mask resist film, and the obtained structure of the green sheet are discussed.展开更多
基金Project(2016YFC0700100)supported by the National Key R&D Program of ChinaProject(JDJQ20160103)supported by the Promotion of the Connotation Development Quota Project of Colleges and Universities-Outstanding Youth of Architectural University,China。
文摘Effects of the flow pattern of intertubular liquid film on mass and heat transfer synergies in a falling-film dehumidification system with horizontal pipes are studied.A flow model of the dehumidifying solution between horizontal pipes is established using Fluent software,the rule of transitions of the flow pattern between pipes is studied,critical Reynolds numbers of flow pattern transitions are obtained,and the accuracy of the model is verified by experiments.The mass transfer synergy angle and heat transfer synergy angle are respectively used as evaluation criteria for the mass transfer synergy and heat transfer synergy,and distribution laws of the synergy angles for droplet,droplet columnar and curtain flow patterns are obtained.Simulation results show that the mass transfer synergy angles corresponding to droplet,droplet columnar and curtain flow patterns all rise to a plateau with time.The mean mass-transfer synergy angle is 98°for the droplet flow pattern,higher than 96.5°for the droplet columnar flow pattern and 95°for the curtain flow pattern.The results show that the mass transfer synergy of the droplet flow pattern is better than that of the droplet columnar flow pattern and that of the curtain flow pattern.
基金Project supported by the National Natural Science Foundation of China (Grant No 50171020) and the Foundation for youth of Liaocheng University (Grant No X051050).
文摘In this paper a systematic ferromagnetic resonance study shows that an in-plane magnetic anisotropy in the patterned micron octagon permalloy (Ni80Fe20) elements is mainly determined by the element geometry. The easy-axis is along the edge of the elements, and the hard-axis is along the diagonal. The shape anisotropy of the octagon elements is determined by square and equilateral octagon, and the theoretical calculation was studied on the shape anisotropy. The shape anisotropy of rectangular was calculated by using the same theory.
基金Project supported by the Postgraduates Innovation Program of Jiangsu Province, China (Grant No. CXZZ12-0086)the National Natural Science Foundation of China (Grant No. 11074034)+1 种基金the National Basic Research Program of China (Grant No. 2010CB923404)the National Laboratory of Solid State Microstructures at Nanjing University and Southeast University, China
文摘CoNiFe patterned films with rectangular elements, all 600-nm wide but of different lengths, were fabricated and inves- tigated by ferromagnetic resonance experiment and micromagnetic simulation. An in-plane magnetic uniaxial anisotropy was exhibited, and its value increases with the increase of the aspect ratio of the elements, which was fitted by the model, including a quasi-ellipsoid demagnetizing field and a non-uniform demagnetizing field. The relative importance of the non- uniform demagnetizing field decreased from 0.26 to 0.16 with the increase of the length-width aspect ratio of the patterned element from 1.5 to 10. The demagnetizing factors in the three principal axes were determined from the experimental data of ferromagnetic resonance, which agreed reasonably well with the values calculated by micromagnetic simulation. The calculation also indicated that the interaction between elements could be neglected when the edge-to-edge spacing between neighboring elements was larger than 3 μm in our patterned films.
基金Project supported by the National Natural Science Foundation of China (Grant No 10574109)the Zhejiang Provincial Science and Technology Department (Grant No 2005C24008)the Zhejiang Provincial Natural Science Foundation (Grant No.Y604064)
文摘A nearly free sustained copper (Cu) film system has been successfully fabricated by thermal evaporation deposition of Cu atoms on silicone oil surfaces, and a characteristic ordered pattern has been systematically studied. The ordered pattern, namely, band, is composed of a large number of parallel key-formed domains with different width w but nearly uniform length L; its characteristic values of w and L are very susceptible to the growth period, deposition rate and nominal film thickness. The formation mechanism of the ordered patterns is well explained in terms of the relaxation of the internal stress in the films, which is related to the nearly zero adhesion of the solid-liquid interface. By using a two-time deposition method, it is confirmed that the ordered patterns really form in the vacuum chamber.
基金the Basic-Research Foundation of Tsinghua University(JC2000057)the Visiting Scholar Foundation of Solid Mechanical Key Lab in Tongji University of the Ministry of Education of China
文摘The deformation measurement of electrosynthesized polythiophene(Pth) thin films is difficult because of the small thickness and highflexibility of the specimen. An electronic speckle patterninterferom- etry (ESPI) method is used to measure the deformation ofPth films of thicknesses in the range of 4-65 μm . Theirstress-strain curves are obtained. It is found that the mechanicalproperties of Pth films are sensitive to the specimen thickness. Thetensile strength increases with decreasing thickness of thin filmfrom 10 μm. The influence of the electrochemical synthesisconditions on the mechanical properties of Pth films is also dis-Cussed.
文摘Preparation and photo-patterning characteristics of organic-inorganic hybrid thin film containing latent pigment by using photo-acid-generator (PAG) and microwave irradiation have been investigated. The acrylic thin film modified with methoxysilane containing PAG was formed on a glass substrate and irradiated with ultraviolet rays to promote sol-gel reaction by catalytic action of acid which was generated from PAG. And then the film was hardened with microwave irradiation, yielding organic-inorganic hybrid polymer film having hardness, highly transparency and strong adhesion with a glass substrate. Since this reaction only occurred in the optically (UV) irradiated regions, by exploiting the difference between the adhesivenesses of these regions photo-irradiated through photomask with a glass substrate, it was possible to form a patterned film with pitch of 100 to 50 μm by a simple lift-off method. A pigment-containing film using latent pigments (with subtractive three primary colors of coloring materials) and a patterned film were prepared, and it was possible to make these films multi-colored by varying the mixing ratio of the pigments. This multi-colored film-preparation method is effective for simply and efficiently forming a color-filter film by applying optical and microwave irradiation.
基金supported by National Natural Science Foundation of China (NO. 41401036)China Postdoctoral Science Foundation (NO. 2015T81070, 2014M560818)West Light Foundation of the Chinese Academy of Sciences
文摘Furrow irrigation with film-mulched agricultural beds is being promoted in the arid region of northwest China because it improves water utilization. Two-dimensional infiltration patterns under film-mulched furrows can provide guidelines and criteria for irrigation design and operation. Our objective was to investigate soil water dynamics during ponding irrigation infiltration of mulched furrows in a cross-sectional ridge-furrow configuration, using laboratory experiments and mathematical simulations. Six experimental treatments, with two soil types (silt loam and sandy loam), were investigated to monitor the wetting patterns and soil water distribution in a cuboid soil chamber. Irrigation of mulched furrows clearly increased water lateral infiltration on ridge shoulders and ridges, due to enhancement of capillary driving force. Increases to both initial soil water content (SWC) and irrigation water level resulted in increased wetted soil volume. Empirical regression equations accurately estimated the wetted lateral distance (Rl) and downward distance (Rd) with elapsed time in a variably wetted soil medium. Optimization of model parameters followed by the Inverse approach resulted in satisfactory agreement between observed and predicted cumulative infiltration and SWC. On the basis of model calibration, HYDRUS-2D model can accurately simulate two-dimensional soil water dynamics under irrigation of mulched furrows. There were significant differences in wetting patterns between unmulched and mulched furrow irrigation using HYDRUS-2D simulation. The Rd under the mulched furrows was 32.14% less than the unmulched furrows. Therefore, film-mulched furrows are recommended in a furrow irrigation system.
文摘The development of stationary patterns on a thin polymer surface subject to an electric field is studied by means of the hexagonal-planform weakly nonlinear stability analysis and numerical simulations. The time evolution of the interface between the air and the polymer film on the unbounded spatial domain is described by a thin film equation, incorporating the electric driving force and the surface diffusion.The nonlinear interfacial growth includes the amplitude equations and superposition of one-dimensional structures at regular orientations. The pattern selection is driven by the subcritical instability mechanism in which the relative thickness of the polymer film plays a critical role.
基金supported by the National Natural Science Foundation of China(Grant 11072231)Collaborative Innovation Center of Suzhou Nano Science and Technology
文摘A kinetics approach is developed for the geometrically nonlinear analysis of photo-induced wrinkling of glassy twist nematic films on soft elastic substrates.In this way,the problem is reduced to finding the steady state of an overdamped evolution system according to a kinetic law,rather than directly solving the coupled nonlinear equations.This enables one to account for the complicated director distribution and obtain the precise wrinkling morphology of the film.Though the approach proposed here is for a twist nematic film,it can be extended to study glassy nematic films with other director distributions.
文摘Formation of copper wiring on a polyimide film by laser irradiation to a stable copper-complex film consisting of glyoxylic acid copper complex and methylamine copper complex in air has been investigated. A stable metallic copper on the polyimide film was precipitated even in air. Since this copper was generated only in the laser-irradiated parts, direct patterning of copper wiring was possible. It was also found that copper was precipitated by electroless copper plating on the laser-deposited copper wiring and it was possible to thicken the copper wiring by this precipitation. The resistivity of the copper wiring was almost the same as that of the bulk of metallic copper. The developed method—combining laser irradiation to a copper-complex-coated film and electroless copper plating—enables the high-speed deposition of fine copper wiring on a polyimide film in air by a printing process, indicating an inexpensive and useful process for fabricating copper wiring without high vacuum facility and heat-treatment under inert gas.
基金Project(R15-2006-022-01001-0) supported by the National Core Research Center Program from MOST and KOSEF
文摘The BLU (back light unit) is the core component of the LCD for notebook, mobile-phone, navigation, as well as large sized TV, PID (public information display), etc. In order to enhance optical efficiency of LCD, optical films with the uniform prism patterns have been used for BLU by stacking two films up orthogonally. In this case, light interference-phenomenon occurred such as Morie, wet-out, u-turning, etc. It caused several problems such as low brightness, spots and stripes in LCD. Recently, the high-luminance micro complex prism patterns are actively studied to avoid the light interference-phenomenon and enhance the optical efficiency. In this study, the roll master to manufacture complex micro prism pattern film was machined by using the high precision lathe. The machined patterns on the roll master were 50, 45, 40, 35, 30, 25, 20, 15, 10 and 5 μm in the pitch with 25.0, 22.5, 20.0, 17.5, 15.0, 12.5, 10.0, 7.5, 5.0 and 2.5 μm in the peak height, respectively. The roll was 2 000 mm in length and 320 mm in diameter. The electroplated roll by copper and the natural single crystal diamond tool was used for machining the patterns. The cutting force was measured and analyzed for each cutting condition by using the dynamometer. The chips and the surfaces after being machined were analyzed by SEM and microscope.
文摘Patterning technology of ferrite and insulating material in multilayer ceramic devices is proposed. In the conventional technology, the different ceramic materials such as the ferrite and the insulating material have been prepared in the form of the each different green sheet, and then they have been stacked each other. Otherwise the different material has filled cavities that were formed by a mechanical punching in advanced. In our proposing technology, arbitrary patterning of the different ceramic material inside the same green sheet is possible. In this process, the arbitrary shape of the through pattern is formed in the green sheet of the base material by making use of photo resist films as sacrifice patterns, and then the base material is masked by the patterned photo resist film. After filling the slurry of the different material into the through pattern of the base material passing the resist mask, the pattern of the different ceramic material in the green sheet is achieved. In the present paper, the ferrite magnetic material and the alumina-glass composite material are used. The patterned structure inside the green sheet is obtained. The slurry preparation, the thickness of the mask resist film, and the obtained structure of the green sheet are discussed.