Structure and effects of electroless Ni-Sn-P transition layer during acid electroless plating on magnesium alloys

An electroless ternary Ni-Sn-P transition layer with high corrosion resistance was applied for acid electroless nickel plating on magnesium alloys. The surface morphologies and microstructure of the traditional alkaline electroless Ni-P and novel Ni-Sn-P transition layers were compared by SEM and XRD, and the bonding strengths between the transition layers and AZ31 magnesium alloys were tested. The corrosion resistance of the samples was analyzed by porosity test, potentiodynamic polarization, electrochemical impedance spectroscopy（EIS） in acid electroless solution at p H 4.5 and immersion test in 10% HCl. The results indicate that the transition layer is essential for acid electroless plating Ni-P coatings on magnesium alloys. Under the same thin thickness（-6 μm）, the electroless Ni-Sn-P transition layer possesses superior properties to the traditional Ni-P transition layer, including high amorphization, smooth and dense surface without pores, enhanced bonding strength and corrosion resistance. Most importantly, acid electroless Ni-P coatings can be successfully deposited on magnesium alloys by using Ni-Sn-P transition layer.

MICROSTRUCTURE AND MECHANISM OF A NEW TYPE OF Ni－Fe－W－P－S WEAR－RESISTANT BRUSH PLATING LAYER

A new type of Ni-Fe-W-P-S wear-resistant brush plating layer isdeveloped, and its microstructure is investigated at different temperatures by usingX-ray diffractometer, transmission electron microscope and surface analytical appa-ratus. The results revealed that the plating layer is composed of amorphous and mi-crocrystalline matrix and intermetallic compounds. Such a microstructure is verybeneficial to improving its wear-resistance.This new type of plating layer can replacethe chromium plating technique which is very poisonous for human health and harm-ful to the agricultural production.

Formation mechanism of bimetal composite layer between LCS and HCCI

A low carbon steel （LCS）/high chromium white cast iron （HCCI） bimetal wear plate about 20 mm in thickness was prepared by liquid-liquid bimetal composite casting technology to substitute for the welding wear plate. A clear and distinguishable composite layer between the LCS and the HCCI was detected with SEM, and the composition and phase were analyzed through EDS and XRD. The composite layer was composed of three sublayers from the LCS to the HCCI： pearlite transition layer, composite layer, and HCCI transition layer. The Vickers hardness from the pearlite transition layer to the HCCl transition layer was 360 HV to 855 HV. The austenite grows as dendrites between the composite layer and the HCCI transition layer under constitutional undercooling. A large amount of C and Cr, and a small amount of Si and Mn dissolve in the matrix. Granular Cr7C3 is uniformly distributed. Due to the solute redistribution at the solid-liquid interface, the primary austenite grows from planar to cellular and finally to the distinct dendrite crystals. The dendrite crystals have an obvious growth direction perpendicular to the composite layer.

Determination of isolation layer thickness for undersea mine based on differential cubature solution to irregular Mindlin plate

The differential cubature solution to the problem of a Mindlin plate lying on the Winkler foundation with two simply supported edges and two clamped edges was derived.Discrete numerical technology and shape functions were used to ensure that the solution is suitable to irregular shaped plates.Then,the mechanical model and the solution were employed to model the protection layer that isolates the mining stopes from sea water in Sanshandao gold mine,which is the first subsea mine of China.Furthermore,thickness optimizations for the protection layers above each stope were conducted based on the maximum principle stress criterion,and the linear relations between the best protection layer thickness and the stope area under different safety factors were regressed to guide the isolation design.The method presented in this work provides a practical way to quickly design the isolation layer thickness in subsea mining.

Electroless Nickel Plating and Electroplating on FBG Temperature Sensor

Metal-coated fiber Bragg grating（FBG）temperature sensors were prepared via electroless nickel（EN）plating and tin electroplating methods on the surface of normal bare FBG.The surface morphologies of the metal-coated layers were observed under a metallographic microscope.The effects of pretreatment sequence,pH value of EN plating solution and current density of electroplating on the performance of the metal-coated layers were analyzed.Meanwhile, the Bragg wavelength shift induced by temperature was monitored by an optical spectrum analyzer.Sensitivity of the metal-coated FBG（MFBG）sensor was almost two times that of normal bare FBG sensor.The measuring temperature of the MFBG sensor could be up to 280℃,which was much better than that of conventional FBG sensor.

MODIFIED LAYER REMOVAL METHOD FOR MEASUREMENT OF RESIDUAL STRESS DISTRIBUTION IN THICK PRE-STRETCHED ALUMINUM PLATE

The integrated structure parts are widely used in aircraft. The distortion caused by residual stresses in thick pre-stretched aluminum plates during machining integrated parts is a common and serious problem. To predict and control the machining distortion, the residual stress distribution in the thick plate must be measured firstly. The modified removal method for measuring residual stress in thick pre-stretched aluminum plates is proposed and the stress-strain relation matrix is deduced by elasticity theory. The residual stress distribution in specimen of 7050T7451 plate is measured by using the method, and measurement results are analyzed and compared with data obtained by other methods. The method is effective to measure the residual stress.

Breakdown voltage model and structure realization of a thin silicon layer with linear variable doping on a silicon on insulator high voltage device with multiple step field plates

Based on the theoretical and experimental investigation of a thin silicon layer（TSL） with linear variable doping（LVD） and further research on the TSL LVD with a multiple step field plate（MSFP）,a breakdown voltage（BV） model is proposed and experimentally verified in this paper.With the two-dimensional Poisson equation of the silicon on insulator（SOI） device,the lateral electric field in drift region of the thin silicon layer is assumed to be constant.For the SOI device with LVD in the thin silicon layer,the dependence of the BV on impurity concentration under the drain is investigated by an enhanced dielectric layer field（ENDIF）,from which the reduced surface field（RESURF） condition is deduced.The drain in the centre of the device has a good self-isolation effect,but the problem of the high voltage interconnection（HVI） line will become serious.The two step field plates including the source field plate and gate field plate can be adopted to shield the HVI adverse effect on the device.Based on this model,the TSL LVD SOI n-channel lateral double-diffused MOSFET（nLDMOS） with MSFP is realized.The experimental breakdown voltage（BV） and specific on-resistance（R on,sp） of the TSL LVD SOI device are 694 V and 21.3 ·mm 2 with a drift region length of 60 μm,buried oxide layer of 3 μm,and silicon layer of 0.15 μm,respectively.

Cumulative second-harmonic generation of Lamb waves propagating in a two-layered solid plate

The physical process of cumulative second-harmonic generation of Lamb waves propagating in a two-layered solid plate is presented by using the second-order perturbation and the technique of nonlinear reflection of acoustic waves at an interface. In general, the cumulative second-harmonic generation of a dispersive guided wave propagation does not occur. However, the present paper shows that the second-harmonic of Lamb wave propagation arising from the nonlinear interaction of the partial bulk acoustic waves and the restriction of the three boundaries of the solid plates does have a cumulative growth effect if some conditions are satisfied. Through boundary condition and initial condition of excitation, the analytical expression of cumulative second-harmonic of Lamb waves propagation is determined. Numerical results show the cumulative effect of Lamb waves on second-harmonic field patterns.

Influence of active constrained layer damping on the coupled vibration response of functionally graded magneto-electro-elastic plates with skewed edges

This article makes the first attempt in assessing the influence of active constrained layer damping(ACLD)treatment towards precise control of frequency responses of functionally graded skew-magneto-electroelastic(FGSMEE)plates by employing finite element methods.The materials are functionally graded across the thickness of the plate in terms of modest power-law distributions.The principal equations of motion of FGSMEE are derived via Hamilton’s principle and solved using condensation technique.The effect of ACLD patches are modelled by following the complex modulus approach(CMA).Additionally,distinctive emphasis is laid to evaluate the influence of geometrical skewness on the attenuation capabilities of the plate.The accuracy of the current analysis is corroborated with comparison of previous researches of similar kind.Additionally,a complete parametric study is directed to understand the combined impacts of various factors like coupling fields,patch location,fiber orientation of piezoelectric patch in association with skew angle and power-law index.

Non-axisymmetrical vibration of elastic circular plate on layered transversely isotropic saturated ground

The non-axisymmetrical vibration of elastic circular plate resting on a layered transversely isotropic saturated ground was studied. First, the 3-d dynamic equations in cylindrical coordinate for transversely isotropic saturated soils were transformed into a group of governing differential equations with 1-order by the technique of Fourier expanding with respect to azimuth, and the state equation is established by Hankel integral transform method, furthermore the transfer matrixes within layered media are derived based on the solutions of the state equation. Secondly, by the transfer matrixes, the general solutions of dynamic response for layered transversely isotropic saturated ground excited by an arbitrary harmonic force were established under the boundary conditions, drainage conditions on the surface of ground as well as the contact conditions. Thirdly, the problem was led to a pair of dual integral equations describing the mixed boundaryvalue problem which can be reduced to the Fredholm integral equations of the second kind solved by numerical procedure easily. At the end of this paper, a numerical result concerning vertical and radical displacements both the surface of saturated ground and plate is evaluated.

Boundary Layer Distributions and Cooling Rate of Cooling Sloping Plate Process

According to the principle of grain refining and slurry preparation by cooling sloping plate process, the distributions of boundary layers during melt treatment by cooling sloping plate were studied, and mathematic model of cooling rate was established. The calculation value approximately agrees with the experimental result. Laminar flow and turbulent flow exist on sloping plate surface commonly. The thickness of velocity boundary layer and the critical transfer distance from laminar flow to turbulent flow increase with the decrease of initial flow velocity. The thickness of temperature boundary layer increases with the increment of flow distance and the decrease of initial flow velocity. The melt cooling rate and melt thickness have an inverse proportion relationship. The melt cooling rate increases along the plate direction gradually when the initial flow velocity is lower than 1 m/s, the melt cooling rate keeps nearly a constant when the initial flow velocity is 1 m/ s, when the initial flow velocity is higher than 1 m/s, the melt cooling rate decreases gradually. The melt cooling rate of cooling sloping plate process can reach 102-103 K/s and belongs to meta-rapid solidification scope.

Transient electro-osmotic and pressure driven flows of two-layer fluids through a slit microchannel

By method of the Laplace transform, this arti- cle presents semi-analytical solutions for transient electro- osmotic and pressure-driven flows （EOF/PDF） of two-layer fluids between microparallel plates. The linearized Poisson- Boltzmann equation and the Cauchy momentum equation have been solved in this article. At the interface, the Maxwell stress is included as the boundary condition. By numerical computations of the inverse Laplace transform, the effects of dielectric constant ratio e, density ratio p, pressure ratio p, viscosity ratioμ of layer II to layer I, interface zeta potential difference △ψ, interface charge density jump Q, the ratios of maximum electro-osmotic velocity to pressure velocity , and the normalized pressure gradient B on transient veloc- ity amplitude are presented.We find the velocity amplitude becomes large with the interface zeta potential difference and becomes small with the increase of the viscosity. The ve- locity will be large with the increases of dielectric constant ratio; the density ratio almost does not influence the EOF ve- locity. Larger interface charge density jump leads to a strong jump of velocity at the interface. Additionally, the effects of the thickness of fluid layers （hi and h2） and pressure gradient on the velocity are also investigated.

Correlation between plate age and layer separation of double seismic zones

Global seismicity catalogs are sufficient for characterizing double seismic zones （DSZs） in subducting slab and facilitate to estimate layer separation without inconsistent uncertainties as local catalogs. Previous studies have shown the correlation between DSZs layer separation and plate age while correlation for those younger than -60 Ma is suspicious. The lacking of DSZs with layer separation less than 10 km further makes it difficult to precisely estimate such correlation. Thus, we incorporate eight DSZs data determined through local seismicity into globally-determined dataset and reexamine such correlation. The best fitting results show that both a linear model and a square root of plate age can mathematically fit the layer separation well. However, it is difficult to distinguish these two models when plate age is greater than -20 Ma since their difference is less than 2 km. However, if extrapolation is possible, both models should provide physical information that DSZs will not form if there is no subducting lithosphere. As a result, the DSZs cannot be produced until the oceanic lithospheric age becomes greater than 0.9 Ma in the square root model while the linear model gives a misleading result. As such the square root model demonstrates the relationship physically better than the linear one, it still needs further test in the future with more available data, nevertheless, our study might also provide evidence for the suggestion that the plate age is a primary control factor of the DSZs geometry as well as the subducting process which disregards any local tectonic stresses.

Layer-block tectonics of Cenozoic basements and formation of intra-plate basins in Nansha micro-plate, southern South China Sea

Layer-block tectonics （LBT） concept, with the core of pluralistic geodynamic outlook and multilayer-sliding tectonic outlook, is one of new keys to study 3-dimensional solid and its 4-dimensional evolution history of global tectonic system controlled by global geodynamics system. The LBT concept is applied to study the lithospheric tectonics of the southern South China Sea （SCS）. Based on the analysis of about 30 000 km of geophysical and geological data, some layer-blocks in the Nansha micro-plate can be divided as Nansha ultra-crustal layer-block, Zengmu crustal layer-block, Nanwei （Rifleman bank）-Andu （Ardasier bank） and Liyue （Reed bank） North Palawan crustal layer-blocks, Andu-Bisheng and Liyue-Banyue basemental layer-blocks. The basic characteristics of the basemental layer-blocks have been dicussed, and three intra-plate basin groups are identified. The intra-plate basins within Nansha micro-plate can be divided into three basin groups of Nanwei- Andu, Feixin-Nanhua, and Liyue-North Palawan based on the different geodynamics. In the light of pluralistic geodynamic concept, the upheaving force induced by the mid-crust plastic layer is proposed as the main dynamical force which causes the formation of the intra-plate basins within the Nansha micro-plate. Finally, models of a face-to-face dip-slip detachment of basemental layerblock and a unilateral dip-slip-detachment of basemental layer-block are put forward for the forming mechanisms of the Nanwei Andu and Liyue-North Palawan intra-plate basin groups, respectively.

Non-equilibrium turbulent phenomena in transitional flat plate boundary-layer flows

Many recent laboratory experiments and numerical simulations support a non-equilibrium dissipation scaling in decaying turbulence before it reaches an equilibrium state.By analyzing a direct numerical simulation(DNS)database of a transitional boundary-layer flow,we show that the transition region and the non-equilibrium turbulence region,which are located in different streamwise zones,present different non-equilibrium scalings.Moreover,in the wall-normal direction,the viscous sublayer,log layer,and outer layer show different non-equilibrium phenomena which differ from those in grid-generated turbulence and transitional channel flows.These findings are expected to shed light on the modelling of various types of non-equilibrium turbulent flows.

Hydroelastic Response of A Circular Plate in Waves on A Two-Layer Fluid of Finite Depth

The hydroelastic response of a circular, very large floating structure(VLFS), idealized as a floating circular elastic thin plate, is investigated for the case of time-harmonic incident waves of the surface and interfacial wave modes, of a given wave frequency, on a two-layer fluid of finite and constant depth. In linear potential-flow theory, with the aid of angular eigenfunction expansions, the diffraction potentials can be expressed by the Bessel functions. A system of simultaneous equations is derived by matching the velocity and the pressure between the open-water and the platecovered regions, while incorporating the edge conditions of the plate. Then the complex nested series are simplified by utilizing the orthogonality of the vertical eigenfunctions in the open-water region. Numerical computations are presented to investigate the effects of different physical quantities, such as the thickness of the plate, Young’s modulus, the ratios of the densities and of the layer depths, on the dispersion relations of the flexural-gravity waves for the two-layer fluid. Rapid convergence of the method is observed, but is slower at higher wave frequency. At high frequency, it is found that there is some energy transferred from the interfacial mode to the surface mode.

General series expression of eddy-current impedance for coil placed above multi-layer plate conductor

This paper presents a closed expression of the layered-plate factor used to calculate the coil eddy-current impedance over the multi-layer plate conductor. By using this expression, the general series of eddy-current impedance can be written directly without solving the undetermined constant equations. The series expression is easy to use for theoretical analysis and programming. Experimental results show that calculated values and measured values are in agreement. As an application, when the bottom layer of the layered plate is a non-ferromagnetic thin layer conductor and the product of the thickness and conductivity of the layer remains unchanged, using the layered-plate factor expression proposed in this paper, it can be theoretically predicted that the eddy-current impedance curves corresponding to different thin layer thickness values will coincide.

Modified Layer-Removal Method for Measurement of Residual Stress in Pre-stretched Aluminium Alloy Plate

Residual stress is one of the factors affecting the machining deformation of monolithic structure parts in the aviation industry. Thus, the studies on machining deformation rules induced by residual stresses largely depend on correctly and efficiently measuring the residual stresses of workpieccs. A modified layer-removal method is proposed to measure residual stress by analysing the characteristics of a traditional, layer-removal method. The coefficients of strain release are then deduced according to the simulation results using the finite element method （FEM）. Moreover, the residual stress in a 7075T651 aluminium alloy plate is measured using the proposed method, and the results are then analyzed and compared with the data obtained by the traditional methods. The analysis indicates that the modified layer-removal method is effective and practical for measuring the residual stress distribution in pre-stretched aluminium alloy plates.

XTEM STUDY ON ION PLATED STAINLESS STEEL MULTI-LAYER FILMS

In this paper, the cross sectional microstructure and crystal structure of ion plated multi layer films of stainless steel (1Cr18Ni9Ti ) were studied by cross sectional transmission electron microscopy (XTEM). The results show that ion plated stainless steel multi layer films are fine grained double phase steel films of austenites and ferrites.Cross section film growing microstructures can be divided into three zones: fine equiaxed crystals, fine columnar crystals and coarse columnar crystals. Interfaces in multi layer films can promote fine grained growing and interrupt columnar grained growing,and improve properties of film materials.

CONTINUAL CONDITIONS BETWEEN LAYERS FOR LAMINATED PLATES

In this paper, various forms of functional on blending energy principles of composite laminated plates are gir en, which guarantee satisfied continual conditions of displacements and stress between layers, and then the reliability of the functional are proved by the computing example.