Pre-dispersed solvent extraction (PDSE) was used to extract quercentin from its diluted solution. The influences of temperature, phase volume ratio (PVR), concentration of sodium Dodecyl benzene sulphonate and pH valu...Pre-dispersed solvent extraction (PDSE) was used to extract quercentin from its diluted solution. The influences of temperature, phase volume ratio (PVR), concentration of sodium Dodecyl benzene sulphonate and pH value etc. on the extraction efficiency were examined. It is found that, compared with traditional extraction techniques under the same condition, a higher extraction productivity can be obtained by PDSE. The stability of colloidal liquid aphrons plays an important role in this process. In a certain scope, the extraction efficiency increases with PVR. Excessive amount of solvent is not much helpful. A new analytical method by using ultraviolet spectrometer to determine the concentration of quercentin is established.展开更多
A novel method was developed to fabricate carbon nanotubes (CNTs)-reinforced Mg matrix composites. The method consists of two steps: CNTs pre-dispersion by ball-milling and the ultrasonic melt processing. Mechanica...A novel method was developed to fabricate carbon nanotubes (CNTs)-reinforced Mg matrix composites. The method consists of two steps: CNTs pre-dispersion by ball-milling and the ultrasonic melt processing. Mechanical ball- milling effectively pre-dispersed CNTs on Zn flakes with suitable rotational speed and ball-milling time. Serious CNT entanglements were dispersed by the ball-milling. However, ball-milling for a long time at high speed would damage the morphology of CNTs. The ultrasonic overcame the poor wettability between Mg melt and CNTs and then dispersed pre-dispersed CNTs in the Mg melt. CNTs were distributed well in the composites and maintained integrated structure. CNTs significantly improved the mechanical properties of the matrix. The strengthening efficiency reached to 37.1, which proves the superiority of this novel method. Besides grain refinement, load transfer may make a great contribution to the improvement of the strength for the composites.展开更多
Carbon nanotubes(CNTs) reinforced Mg matrix composites were fabricated by a novel melt processing.The novel processing consisted of two courses:CNTs pre-dispersion and ultrasonic melt processing.Mechanical ball-mil...Carbon nanotubes(CNTs) reinforced Mg matrix composites were fabricated by a novel melt processing.The novel processing consisted of two courses:CNTs pre-dispersion and ultrasonic melt processing.Mechanical ball-milling was employed to pre-disperse CNTs on Zinc(Zn) flakes.Serious CNT entanglements were well dispersed to single CNT or tiny clusters on Zn flakes.The ultrasonic melt processing further dispersed CNTs in the Mg melt,especially tiny CNT clusters.Thus,a uniform dispersion of CNTs was achieved in the as-cast composites.Hot extrusion further improved the distribution of CNTs.CNTs increased both the strength and elongation of the matrix alloy.Notably,the elongation of the matrix alloy was enhanced by 40%.Grain refinement and the pulling-out of CNTs resulted in the evident improvement of ductility for the composites.展开更多
Aims Theory suggests that species perform best at intermediate densities,where density-dependent facilitation and antagonism are balanced,but empirical evidence is scarce,particularly in plants.In a selfincompatible p...Aims Theory suggests that species perform best at intermediate densities,where density-dependent facilitation and antagonism are balanced,but empirical evidence is scarce,particularly in plants.In a selfincompatible perennial herb(Saussurea nigrescens),whose recruitment heavily relies on seed output,we test whether both intraspecific facilitation and antagonism significantly affect seed production,resulting in highest seed yield at an intermediate capitulum density.Methods Plots with different S.nigrescens densities were sampled in an Eastern Tibetan meadow during the growing season of 2012 to investigate the relationships between capitulum density and pollinator visitation rate,seed set ratio,parasite ratio,seed damage ratio,and capitulum size.Both simple linear and quadratic models were employed to determine the shape of relationships.Important Findings In line with general theory,hump-shaped relationships of capitulum density versus seed set ratio and number of florets per capitulum indicate intraspecific facilitation in sparse populations,which can be attributed to positive density-dependent pollinator visitation and the amelioration of detrimental physical factors.However,the proportion of seeds damaged by pre-dispersal predators increased monotonically with capitulum density,which may have—in combination with increased intraspecific competition for light and soil nutrients—resulted in density-dependent antagonism.Both positive and negative density-dependent agents acted simultaneously throughout the density range investigated and led to the highest seed yield at intermediate density levels in the Tibetan lotus.More efforts concurrently exploring the two effects are needed to facilitate understanding species abundance and community structure.展开更多
基金Supported by the National Natural Science Foundation of China (No.29736170)
文摘Pre-dispersed solvent extraction (PDSE) was used to extract quercentin from its diluted solution. The influences of temperature, phase volume ratio (PVR), concentration of sodium Dodecyl benzene sulphonate and pH value etc. on the extraction efficiency were examined. It is found that, compared with traditional extraction techniques under the same condition, a higher extraction productivity can be obtained by PDSE. The stability of colloidal liquid aphrons plays an important role in this process. In a certain scope, the extraction efficiency increases with PVR. Excessive amount of solvent is not much helpful. A new analytical method by using ultraviolet spectrometer to determine the concentration of quercentin is established.
基金financially supported by the National Natural Science Foundation of China (No.51101043 and 51471059)Key Project of Science and Technology Department of Heilongjiang Province of China (No.GC12A109)the China Postdoctoral Science Foundation (No.2013M531035 and 2014T70328)
文摘A novel method was developed to fabricate carbon nanotubes (CNTs)-reinforced Mg matrix composites. The method consists of two steps: CNTs pre-dispersion by ball-milling and the ultrasonic melt processing. Mechanical ball- milling effectively pre-dispersed CNTs on Zn flakes with suitable rotational speed and ball-milling time. Serious CNT entanglements were dispersed by the ball-milling. However, ball-milling for a long time at high speed would damage the morphology of CNTs. The ultrasonic overcame the poor wettability between Mg melt and CNTs and then dispersed pre-dispersed CNTs in the Mg melt. CNTs were distributed well in the composites and maintained integrated structure. CNTs significantly improved the mechanical properties of the matrix. The strengthening efficiency reached to 37.1, which proves the superiority of this novel method. Besides grain refinement, load transfer may make a great contribution to the improvement of the strength for the composites.
基金supported by the National Natural Science Foundation of China(Grant No.51471059 and 51671066)the China Postdoctoral Science Foundation(Grant No.2014T70328)
文摘Carbon nanotubes(CNTs) reinforced Mg matrix composites were fabricated by a novel melt processing.The novel processing consisted of two courses:CNTs pre-dispersion and ultrasonic melt processing.Mechanical ball-milling was employed to pre-disperse CNTs on Zinc(Zn) flakes.Serious CNT entanglements were well dispersed to single CNT or tiny clusters on Zn flakes.The ultrasonic melt processing further dispersed CNTs in the Mg melt,especially tiny CNT clusters.Thus,a uniform dispersion of CNTs was achieved in the as-cast composites.Hot extrusion further improved the distribution of CNTs.CNTs increased both the strength and elongation of the matrix alloy.Notably,the elongation of the matrix alloy was enhanced by 40%.Grain refinement and the pulling-out of CNTs resulted in the evident improvement of ductility for the composites.
基金973 program(2013CB956300)National Science Foundation of China(31100397 and 3250004)‘Program for Changjiang Scholars and Innovative Research Team in University’(IRT_14R27).
文摘Aims Theory suggests that species perform best at intermediate densities,where density-dependent facilitation and antagonism are balanced,but empirical evidence is scarce,particularly in plants.In a selfincompatible perennial herb(Saussurea nigrescens),whose recruitment heavily relies on seed output,we test whether both intraspecific facilitation and antagonism significantly affect seed production,resulting in highest seed yield at an intermediate capitulum density.Methods Plots with different S.nigrescens densities were sampled in an Eastern Tibetan meadow during the growing season of 2012 to investigate the relationships between capitulum density and pollinator visitation rate,seed set ratio,parasite ratio,seed damage ratio,and capitulum size.Both simple linear and quadratic models were employed to determine the shape of relationships.Important Findings In line with general theory,hump-shaped relationships of capitulum density versus seed set ratio and number of florets per capitulum indicate intraspecific facilitation in sparse populations,which can be attributed to positive density-dependent pollinator visitation and the amelioration of detrimental physical factors.However,the proportion of seeds damaged by pre-dispersal predators increased monotonically with capitulum density,which may have—in combination with increased intraspecific competition for light and soil nutrients—resulted in density-dependent antagonism.Both positive and negative density-dependent agents acted simultaneously throughout the density range investigated and led to the highest seed yield at intermediate density levels in the Tibetan lotus.More efforts concurrently exploring the two effects are needed to facilitate understanding species abundance and community structure.