The thiono-thiolo allylic rearrangement of O-allyl-O-aryl-O-ethyl thionophosphates(1a-j) adsorbed on SiO2 afforded the corresponding O-aryl-O-ethyl-S-allyl thiolophosphates (2a-j) in good yields.
A sample enrichment method focusing on the minor targeted components was established to help them to be successfully separated by pH-zone refining CCC.Seven minor indole alkaloids in Uncaria rhynchophylla(Miq.)Miq.ex ...A sample enrichment method focusing on the minor targeted components was established to help them to be successfully separated by pH-zone refining CCC.Seven minor indole alkaloids in Uncaria rhynchophylla(Miq.)Miq.ex Havil(UR)were chosen to show the advantage of this method.The sample enrichment and separation were展开更多
文摘The thiono-thiolo allylic rearrangement of O-allyl-O-aryl-O-ethyl thionophosphates(1a-j) adsorbed on SiO2 afforded the corresponding O-aryl-O-ethyl-S-allyl thiolophosphates (2a-j) in good yields.
基金supported by the National Science and Technology Major Project for Major Drug Development(No.2013ZX09508104)the Traditional Chinese Medicine Industry Research Special Project(No.201307002)the National Science&Technology Major Project Key New Drug Creation and Manufacturing program(No.2011ZX09307002-03)of the People's Republic of China
文摘A sample enrichment method focusing on the minor targeted components was established to help them to be successfully separated by pH-zone refining CCC.Seven minor indole alkaloids in Uncaria rhynchophylla(Miq.)Miq.ex Havil(UR)were chosen to show the advantage of this method.The sample enrichment and separation were
