The nanosecond(ns) pulsed nitrogen dielectric barrier discharge(DBD) is employed to enhance the hydrophilicity of polypropylene(PP) surface and improve its application effect.The discharge characteristics of the ns pu...The nanosecond(ns) pulsed nitrogen dielectric barrier discharge(DBD) is employed to enhance the hydrophilicity of polypropylene(PP) surface and improve its application effect.The discharge characteristics of the ns pulsed nitrogen DBD with different pulse rise times(from 50to 500 ns) are investigated by electrical and optical diagnostic methods and the discharge uniformity is quantitatively analyzed by image processing method.To characterize the surface hydrophilicity,the water contact angle(WCA) is measured,and the physical morphology and chemical composition of PP before and after modification are analyzed to explore the effect of plasma on PP surface.It is found that with increasing pulse rise time from 50 to 500 ns,DBD uniformity becomes worse,energy efficiency decreases from 20% to 10.8%,and electron density decrease from 6.6 × 10^(11)to 5.5 × 10^(11)cm^(-3).The tendency of electron temperature is characterized with the intensity ratio of N_(2)/N_(2)^(+)emission spectrum,which decreases from 17.4 to15.9 indicating the decreasing of T_(e) with increasing pulse rise time from 50 to 500 ns.The PP surface treated with 50 ns pulse rise time DBD has a lower WCA(~47°),while the WCA of PP treated with 100 to 500 ns pulse rise time DBD expands gradually(~50°–57°).According to the study of the fixed-point WCA values,the DBD-treated PP surface has superior uniformity under50 ns pulse rise time(3° variation) than under 300 ns pulse rise time(8° variation).After DBD treatment,the increased surface roughness from 2.0 to 9.8 nm and hydrophilic oxygencontaining groups on the surface,i.e.hydroxyl(-OH) and carbonyl(C=O) have played the significant role to improve the sample’s surface hydrophilicity.The short pulse voltage rise time enhances the reduced electric field strength(E/n) in the discharge space and improves the discharge uniformity,which makes relatively sufficient physical and chemical reactions have taken place on the PP surface,resulting in better treatment uniformity.展开更多
In order to increase the usefulness of pulsed current source in engineering practice, research and study was carried out on how to increase the pulse current amplitude, reduce the rise /fall time of output pulse and M...In order to increase the usefulness of pulsed current source in engineering practice, research and study was carried out on how to increase the pulse current amplitude, reduce the rise /fall time of output pulse and MOSFET switching losses, etc. Through the analysis of the pulsed current source works theory and the mathematical derivation of the circuit model, the deduction and calculation of the pulse edge compression control methods, and improve the overall circuit structure and optimize the manufacturing process according to the theory. The following indicators was realized: the output pulse current amplitude can be up to 100 A, the shortest pulse rise / fall time was 18.8 ns and 16.1 ns respectively when the maximum amplitude output, the pulse width could be narrowest to 40 ns, repetition frequency could achieve 10 Hz to 10 k Hz, MOSFET switching losses decreased by 30.9 %. This pulsed current source can be used, not only as the power supply for the ordinary high speed narrow pulse width laser diode, but also as an ideal drive power for the high energy, narrow width pulse laser diode.展开更多
基金supported by National Natural Science Foundation of China (Nos. 52037004, 51777091 and52250410350)Postgraduate Research&Practice Innovation Program of Jiangsu Province (No.KYCX22_1314)。
文摘The nanosecond(ns) pulsed nitrogen dielectric barrier discharge(DBD) is employed to enhance the hydrophilicity of polypropylene(PP) surface and improve its application effect.The discharge characteristics of the ns pulsed nitrogen DBD with different pulse rise times(from 50to 500 ns) are investigated by electrical and optical diagnostic methods and the discharge uniformity is quantitatively analyzed by image processing method.To characterize the surface hydrophilicity,the water contact angle(WCA) is measured,and the physical morphology and chemical composition of PP before and after modification are analyzed to explore the effect of plasma on PP surface.It is found that with increasing pulse rise time from 50 to 500 ns,DBD uniformity becomes worse,energy efficiency decreases from 20% to 10.8%,and electron density decrease from 6.6 × 10^(11)to 5.5 × 10^(11)cm^(-3).The tendency of electron temperature is characterized with the intensity ratio of N_(2)/N_(2)^(+)emission spectrum,which decreases from 17.4 to15.9 indicating the decreasing of T_(e) with increasing pulse rise time from 50 to 500 ns.The PP surface treated with 50 ns pulse rise time DBD has a lower WCA(~47°),while the WCA of PP treated with 100 to 500 ns pulse rise time DBD expands gradually(~50°–57°).According to the study of the fixed-point WCA values,the DBD-treated PP surface has superior uniformity under50 ns pulse rise time(3° variation) than under 300 ns pulse rise time(8° variation).After DBD treatment,the increased surface roughness from 2.0 to 9.8 nm and hydrophilic oxygencontaining groups on the surface,i.e.hydroxyl(-OH) and carbonyl(C=O) have played the significant role to improve the sample’s surface hydrophilicity.The short pulse voltage rise time enhances the reduced electric field strength(E/n) in the discharge space and improves the discharge uniformity,which makes relatively sufficient physical and chemical reactions have taken place on the PP surface,resulting in better treatment uniformity.
基金supported by the Changchun Science and Technology Project (13KG28)the Jilin Province Science and Technology Development Plan (20120320)
文摘In order to increase the usefulness of pulsed current source in engineering practice, research and study was carried out on how to increase the pulse current amplitude, reduce the rise /fall time of output pulse and MOSFET switching losses, etc. Through the analysis of the pulsed current source works theory and the mathematical derivation of the circuit model, the deduction and calculation of the pulse edge compression control methods, and improve the overall circuit structure and optimize the manufacturing process according to the theory. The following indicators was realized: the output pulse current amplitude can be up to 100 A, the shortest pulse rise / fall time was 18.8 ns and 16.1 ns respectively when the maximum amplitude output, the pulse width could be narrowest to 40 ns, repetition frequency could achieve 10 Hz to 10 k Hz, MOSFET switching losses decreased by 30.9 %. This pulsed current source can be used, not only as the power supply for the ordinary high speed narrow pulse width laser diode, but also as an ideal drive power for the high energy, narrow width pulse laser diode.