Research on properties of hollow glass microspheres/epoxy resin composites applied in deep rock in-situ temperature-preserved coring

Deep petroleum resources are in a high-temperature environment.However,the traditional deep rock coring method has no temperature preserved measures and ignores the effect of temperature on rock porosity and permeability,which will lead to the distortion of the petroleum resources reserves assessment.Therefore,the hollow glass microspheres/epoxy resin(HGM/EP)composites were innovatively proposed as temperature preserved materials for in-situ temperature-preserved coring(ITP-Coring),and the physical,mechanical,and temperature preserved properties were evaluated.The results indicated that:As the HGM content increased,the density and mechanical properties of the composites gradually decreased,while the water absorption was deficient without hydrostatic pressure.For composites with 50 vol%HGM,when the hydrostatic pressure reached 60 MPa,the water absorption was above 30.19%,and the physical and mechanical properties of composites were weakened.When the hydrostatic pressure was lower than 40 MPa,the mechanical properties and thermal conductivity of composites were almost unchanged.Therefore,the composites with 50 vol%HGM can be used for ITPCoring operations in deep environments with the highest hydrostatic pressure of 40 MPa.Finally,to further understand the temperature preserved performance of composites in practical applications,the temperature preserved properties were measured.An unsteady-state heat transfer model was established based on the test results,then the theoretical change of the core temperature during the coring process was obtained.The above tests results can provide a research basis for deep rock in-situ temperature preserved corer and support accurate assessment of deep petroleum reserves.

An automatic loading system for rock core testing with an industrial CT scanner

A new type of a loading and measuring system was developed for testing failure and deformation of rock core samples with an industrial CT （ICT） scanner.The loading and measuring system consisted of a loading system and a computer control system.The maximum servo-controlled force was 2 tonnes.The new system was a high-stiffness system with a small size.During ICT tests,rock core samples could be easily loaded in the axial direction.So the initiation,propagation,and coalescence of cracks in core samples were observed on ICT images.

Pore-based architecture and representative element volume evaluation in artificial sand packs and natural rock cores

The phenomenon of multiphase flow in porous media is confronted in various fields of science and industrial applications. Owing to the complicated porous structure, the flow mechanisms are still not completely resolved. A critical and fundamental question is the variation of pore structure and REV sizes among different types of porous media. In this study, a total of 22 porous samples were employed to systematically evaluate the pore-based architecture and REV sizes based on X-ray CT image analysis and pore network modelling. It is found that the irregular grain shapes give rise to large specific areas,narrow and thin throats in identical sand packs. The packs with more types of sands, or composited by the sands with larger difference in diameter, have larger specific area, smaller tortuosity and pore spaces.Based on the REV measurement through porosity solely, the REV sizes of sand packs are generally in the order of magnitude of 10^(-2) m L, while it is at least one order of magnitude smaller in rock cores. Our result indicates that the combination of porosity and Euler number is an effective indicator to get the REV sizes of porous samples.

Determination of mining-induced stresses using diametral rock core deformations

Knowledge of ground stresses is crucial for ground control activities such as the design of underground openings,selec-tion of support systems,and analysis for stability.However,it is a known fact that far field stresses experience changes in orientation and magnitude due to the presence of geological structures and due to the excavations created by mining activi-ties.As a result,in-situ stresses around drifts,ramps,and stopes in underground mines are quite different from far field or pre-mining stresses.The purpose of this research is to develop a simple and practical methodology for determining in-situ stresses.Stress relief occurs once the rock core is drilled off.Such relief is a function of the surrounding stress field.This study uses exploration rock cores that are drilled off for the purpose of orebody definition in the underground mine.The method measures and analyzes the diametral core deformations in laboratory.Two case studies from operating underground mines are presented for demonstration.In these case studies,rock core deformations are measured with a customized test apparatus and rock samples were prepared and tested for Young's modulus and Poisson's ratio.The differential stress,namely the difference between the local principal stresses in the plane perpendicular to the core rock axis is calculated.It is shown that this methodology is useful for determining the brittle shear ratio in the rock mass,which is of primary interest to ground control studies.

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