Interconnected microstructure and flexural behavior of Ti_(2)C-Ti composites with superior Young’s modulus

To enhance the Young’s modulus(E)and strength of titanium alloys,we designed titanium matrix composites with intercon-nected microstructure based on the Hashin-Shtrikman theory.According to the results,the in-situ reaction yielded an interconnected microstructure composed of Ti_(2)C particles when the Ti_(2)C content reached 50vol%.With widths of 10 and 230 nm,the intraparticle Ti lamellae in the prepared composite exhibited a bimodal size distribution due to precipitation and the unreacted Ti phase within the grown Ti_(2)C particles.The composites with interconnected microstructure attained superior properties,including E of 174.3 GPa and ultimate flexural strength of 1014 GPa.Compared with that of pure Ti,the E of the composite was increased by 55% due to the high Ti_(2)C content and interconnected microstructure.The outstanding strength resulted from the strong interfacial bonding,load-bearing capacity of interconnected Ti_(2)C particles,and bimodal intraparticle Ti lamellae,which minimized the average crack driving force.Interrupted flexural tests revealed preferential crack initiation along the{001}cleavage plane and grain boundary of Ti_(2)C in the region with the highest tensile stress.In addition,the propagation can be efficiently inhibited by interparticle Ti grains,which prevented the brittle fracture of the composites.

PSO algorithm for Young's modulus reconstruction

To get the quantitive value of abnormal biological tissues, an inverse algorithm about the Young＇s modulus based on the boundary extraction and the image registration technologies is proposed. With the known displacements of boundary tissues and the force distribution, the Young＇s modulus is calculated by constructing the unit system and the inverse finite element method （IFEM）. Then a tough range of the modulus for the whole tissue is estimated referring the value obtained before. The improved particle swarm optimizer （PSO） method is adopted to calculate the whole Yong＇s modulus distribution. The presented algorithm overcomes some limitations in other Young＇s modulus reconstruction methods and relaxes the displacements and force boundary condition requirements. The repetitious numerical simulation shows that errors in boundary displacement are not very sensitive to the estimation of next process; a final feasible solution is obtained by the improved PSO method which is close to the theoretical values obtained during searching in an extensive range.

Measurement of Young's Modulus and Poisson's Ratio of Thermal Barrier Coatings

In gas turbines, thermal barrier coatings （TBCs） applied by air plasma spraying are widely used to lower the temperature of hot components. To analyze the characteristics of TBCs such as residual stress, bond strength, fracture toughness, and crack propagation ratio, the Young＇s modulus and Poisson＇s ratio are important parameters. For TBC is a brittle and thin film, it is desirable to evaluate those properties while the coatings are bonded to a substrate. An atmospheric plasma spray MCrAIY bond coat and Yttria stabilized zirconia （YSZ） top coat are deposited onto a nickel-base superalloy GH150 substrate. The Young＇s modulus and Poisson＇s ratio are measured by cantilever beam bending with NDI. The method will be developed to test the Young＇ s modulus and Poisson ratio of other multilayer systems.

A method to determine Young's modulus of soft gels for cell adhesion

A convenient technique is reported in this note for measuring elastic modulus of extremely soft material for cellular adhesion. Specimens of bending cylinder under gravity are used to avoid contact problem between testing device and sample, and a beam model is presented for evaluating the curvatures of gel beams with large elastic deformation. A self-adaptive algorithm is also proposed to search for the best estimation of gels＇ elastic moduli by comparing the experimental bending curvatures with those computed from the beam model with preestimated moduli. Application to the measurement of the property of polyacrylamide gels indi- cates that the material compliance varies with the concentrations of bis-acrylamide, and the gels become softer after being immersed in a culture medium for a period of time, no matter to what extent they are polymerized.

Prediction and optimization of process variables to maximize the Young’s modulus of plasma sprayed alumina coatings on AZ31B magnesium alloy

Like other manufacturing techniques,plasma spraying has also a non-linear behavior because of the contribution of many coating variables.This characteristic results in finding optimal factor combination difficult.Subsequently,the issue can be solved through effective and strategic statistical procedures integrated with systematic experimental data.Plasma spray parameters such as power,stand-off distance and powder feed rate have significant influence on coating characteristics like Young’s modulus.This paper presents the use of statistical techniques in specifically response surface methodology(RSM),analysis of variance,and regression analysis to develop empirical relationship to predict Young’s modulus of plasma-sprayed alumina coatings.The developed empirical relationships can be effectively used to predict Young’s modulus of plasma-sprayed alumina coatings at 95%confidence level.Response graphs and contour plots were constructed to identify the optimum plasma spray parameters to attain maximum Young’s modulus in alumina coatings.A linear regression relationship was established between porosity and Young’s modulus of the alumina coatings.

Experimental Study on Young′s Modulus of Concrete

Young′s Modulus of concrete is studied on the basis of triaxial compressive experiments. The authors proposed two empirical equations to calculate its static Young′s modulus and dynamic Young′s modulus when dynamic Poisson ratio μ d varies nearby 0.20.P wave velocity and elastic modulus have the same varying tendency as letter N. μ,μ d decrease with the increase of loading rate and μ d has a great effect on the parameters E d and E D.

CALCULATION OF THE YOUNG'S MODULUS OF AN ADSORBED POLYMER LAYER

Polymer layers adsorbed to a surface or in a confined environment often change their mechanical properties. There is even the possibility of solidification of the confined layer. To judge the stiffness of such a layer, we used the Hertz model to calculate the Young＇s modulus of the polymer layer in the confinement of AFM experiments with silicon nitride tip with a radius of curvature ofR ≈ 50 nm and a glass sphere attached to the cantilever R =5 μm. Since there is no visible indentation of the layer in the AFM experiments, the layer is either penetrated very easily, or the indentation is too small to be seen in a force curve. The latter would be the case for a polymer layer with a Young＇s modulus above 4 × 10^8 Pa in case of an experiment with a silicon nitride tip and 4×10^5 Pa in case of a glass sphere.

Determination of reduced Young s modulus of thin films using indentation test

The flat cylindrical indentation tests with different sizes of punch radius were investigated using finite element method （FEM） aimed to reveal the effect of punch size on the indentation behavior of the film/substrate system. Based on the FEM results analysis, two methods was proposed to separate film＇s reduced Young＇s modulus from a film/substrate system. The first method was based on a new weight function that quantifies film＇s and substrate＇s contributions to the overall mechanical properties of the film/substrate system in the flat cylindrical indentation test. The second method, a numerical approach, including fitting and extrapolation procedures was put forward. Both of the results from the two methods showed a reasonable agreement with the one input FE model. At last, the effect of maximum indentation depth and the surface micro-roughness of the thin film on the reduced Young＇s modulus of the film/substrate system were discussed. The methods proposed in the present study provide some new conceptions on evaluating other properties of thin films, e.g. creep, for which a flat-ended punch is also employed.

Analysis of the elastic-plastic indentation properties of materials with varying ratio of hardness to Young’s modulus

The elastic-plastic indentation properties of materials with varying ratio of hardness to Young’s modulus(H/E) were analyzed with the finite element method. And the indentation stress fields of materials with varying ratio H/E on the surface were studied by the experiment. The results show that the penetration depth, contact radius, plastic pile-up and the degree of elastic recovery depend strongly on the ratio H/E. Moreover, graphs were established to describe the relationship between the elastic-plastic indentation parameters and H/E. The established graphs can be used to predict the H/E of materials when compared with experimental data.

Macroscopic Young’s Elastic Modulus Model of Particle Packing Rock Layers

Based on the Hertzian granular contact mechanics model, the paper built up a Macroscopic Young’s Elastic Modulus of particle/granular packing rock layers, and built up a ties to connecting Young’s Elastic Modulus of sand particle in Meso and the Macroscopic Young’s Modulus of granular packing rock layers. The Macroscopic Young’s Modulus of granular packing rock layers is far less than the Young’s Modulus of sand particle. The Macroscopic Young’s Modulus of granular packing rock layers is proportioned to the powers of 1/3 of the vertical contact force of sand particles. The Macroscopic Young’s Modulus is inversely proportional to particle diameter. The paper calculated the vertical contact force of five types aligning mode of the particles. When equal stress, the increased of the coordination number lead to the decrease of the contact force fn, this lead to the coordination number is an inverse proportion to Macroscopic Young’s Modulus. But the larger coordination number change only means very little Macroscopic Young’s Modulus change.

Probing the effect of Young's modulus on the plugging performance of micro-nano-scale dispersed particle gels

The effect of mechanical strength of the dispersed particle gel(DPG)on its macro plugging performance is significant,however,little study has been reported.In this paper,DPG particles with different mechanical strengths were obtained by mechanical shearing of bulk gels prepared with different formula.Young’s moduli of DPG particles on the micro and nano scales were measured by atomic force microscope for the first time.The mapping relationship among the formula of bulk gel,the Young’s moduli of the DPG particles and the final plugging performance were established.The results showed that when the Young’s moduli of the DPG particles increased from 82 to 328 Pa,the plugging rate increased significantly from 91.46%to 97.10%due to the distinctly enhanced stacking density and strength at this range.While when the Young’s moduli of the DPG particles surpassed 328 Pa,the further increase of plugging rate with the Young’s moduli of the DPG particles became insignificant.These results indicated that the improvement of plugging rate was more efficient by adjusting the Young’s moduli of the DPG particles within certain ranges,providing guidance for improving the macroscopic application properties of DPG systems in reservoir heterogeneity regulation.

The influence of defects on the effective Young's modulus of a defective solid

It is difficult to establish structure-property relationships in a defective solid because of its inhomogeneous-geometry microstructure caused by defects. In the present research, the effects of pores and cracks on the Young’s modulus of a defective solid are studied. Based on the law of the conservation of energy, mathematical formulations are proposed to indicate how the shape, size, and distribution of defects affect the effective Young’s modulus. In this approach, detailed equations are illustrated to represent the shape and size of defects on the effective Young’s modulus. Different from the results obtained from the traditional empirical analyses, mixture law or statistical method, for the first time, our results from the finite element method （FEM） and strict analytical calculation show that the influence of pore radius and crack length on the effective Young’s modulus can be quantified. It is found that the longest crack in a typical microstructure of ceramic coating dominates the contribution of the effective Young’s modulus in the vertical direction of the crack.

Influence of Temperature Conditions on Dynamic Young’s Modulus Testing

The Young’s modulus was measured at high temperatures by impulse excitation of vibration method,and the effects of heating rate,holding time and temperature cycle on the test results were analyzed.The results show that the heating rate has obvious effect on the high temperature Young’s modulus of the green body,but has no obvious effect on that of the sintered products;the holding time of the heating process has no regular effect on the Young’s modulus,and the effect varies with the different products at a certain temperature;the method can also be used to test the Young’s modulus during cooling process.

Biodegradation of Polymethylmethacrylate Bone Cement May Not Be a Serious Issue in Total Hip Arthroplasty—Retrieval Study for Knoop Hardness and Young’s Modulus

Introduction: To investigate a long-term in vivo deterioration of polymethylmethacrylate (PMMA) bone cement over time, we evaluated retrieved PMMA cement in terms of chemical elements presenting in the cement using energy dispersive analysis of X-rays;Knoop hardness;and the Young’s modulus using scanning acoustic microscopy. Materials and Methods: For mechanical evaluation, we could neglect the influences of entrapped air bubbles or blood by the use of small specimens. The study was based on thirteen cement samples (six used in the acetabulum and seven in the femur) derived from eight patients (age at revision surgery: mean 72.5, range 68 to 79). All of these samples were Simplex-P?cement. They were functioning well at least ten years after the previous surgery. Duration until revision surgery was ranged 12 to 25 years (average, 17.4 years). The reason for revision was aseptic mechanical loosening. Twenty samples of Simplex-Preg;cement were served by manually mixing as a control. Results: The average of the hardness of the cement was 17.0 ± 1.2 (range, 13.4-20.6). In the control, the hardness was 17.8 ± 1.5 (range, 14.0-24.6). There was no significant difference between these values. The mean of Young’s modulus of the cement was 5.61 ± 0.19 GPa (range, 5.09-6.10). In the control, the modulus was 6.04 ± 0.13 GPa (range, 5.68-6.45). Although the modulus was significantly less than that of the control, there was only 7% decrease in average between twelve and twenty-five years in vivo. Conclusions: Our results suggest that long-term implantation and functional loading in vivo may not be the limiting factor in the mechanical integrity of the bone cement.

Vibration of Gold Nano-Beam with Variable Young’s Modulus Due to Thermal Shock

In this paper, we will study the most important effects in the nano-scale resonator: the coupling effect of temperature and strain rate, and the non-Fourier effect in heat conduction. A solution for the generalized thermoelastic vibration of nano-resonator induced by thermal loading has been developed. The Young’s modulus is taken as a linear function of the reference temperature. The effects of the thermal loading and the reference temperature in all the studied fields have been studied and represented in graphs with some comparisons. The Young’s modulus makes significant effects on all the studied fields where the values of the temperature, the vibration of the deflection, stress, displacement, strain, stress-strain energy increase when the Young’s modulus has taken to be variable.

An improved model for predicting effective Young's modulus of the twisted structure under cyclic loading:taking into account the untwisting effect

Twist structures have diverse applications, ranging from dragline, electrical cable, and intelligent structure. Among these applications, tension deformation can＇t be avoided during the fabrication and working processes, which often leads to the twist structure rotation （called untwisting effect） and twist pitch increasing. As a consequence, this untwisting behavior has a large effect on the effective Young＇s modulus. In this paper, we present an improved model based on the classical Costello＇s theory to predict the effective Young＇s modulus of the basic structure, twisted by three same copper strands under cyclic loading. Series of experiments were carried out to verify the present model taking into account the untwisting effect. The experimental results have better agreements with the presented model than the common Costello＇s model.

剪切波弹性成像评估甲巯咪唑治疗初诊Graves病疗效的应用价值

目的 探讨超声剪切波弹性成像(shear wave elastography, SWE)技术评估甲巯咪唑治疗初诊Graves病疗效的临床应用价值。方法 收集60例经滨州医学院附属医院初诊确诊为Graves病的患者,给予服用甲巯咪唑进行治疗,检测治疗前及治疗2月后患者血清甲状腺功能指标包括血清促甲状腺激素(thyrotropin, TSH)、血清游离三碘甲状腺原氨酸(free triiodothyronine, FT3)和血清游离甲状腺素(free thyroxine, FT4),以及甲状腺自身免疫性炎症指标促甲状腺激素受体抗体(TRAb)。同时应用SWE技术分别测量患者治疗前及治疗2月后甲状腺组织的杨氏模量最大值、最小值和平均值,应用配对t检验对治疗前后的结果进行分析比较。结果 比较治疗前及治疗2月后结果显示,所测血清甲状腺功能指标(TSH、FT3、FT4)显著改善(P<0.01),TRAb显著好转(P<0.05);应用SWE技术测得患者甲状腺组织的各项杨氏模量值也有显著变化(P<0.01)。结论 SWE技术测得甲状腺组织杨氏模量值的变化与患者甲状腺功能指标变化的临床意义一致,说明SWE实时、定量且客观获取的患者甲状腺组织的硬度变化信息,可为临床医师准确评估Graves病治疗效果及调整用药剂量提供重要的量化参考依据,具有较高的临床应用价值。

经会阴三维超声联合SWE评估分娩方式对初产妇肛提肌的影响

目的探讨经会阴三维超声联合剪切波弹性成像技术(shear wave elastography,SWE)在评估分娩方式对初产妇肛提肌形态及功能影响中的应用价值,为早期诊断盆底功能障碍性疾病(pelvic floor disorders,PFD)提供新方法。方法选取在笔者医院分娩后6~8周复查的92例初产妇为产后组,根据其分娩方式分为经阴道分娩组(n=45)和剖宫产组(n=47),选取同期健康未育女性作为对照组(n=43)。采用经会阴三维超声联合SWE进行检查,比较各组间不同状态下肛提肌裂孔形态参数及弹性参数的差异。结果经阴道分娩组在静息、最大缩肛及最大Valsalva状态下肛提肌裂孔面积(levator ani hiatus area,LHA)均大于剖宫产组和对照组,剖宫产组大于对照组,差异有统计学意义(P<0.01);经阴道分娩组在静息及最大缩肛状态下弹性参数较对照组、剖宫产组均减小,差异有统计学意义(P<0.01);而剖宫产组与对照组弹性参数比较,差异无统计学意义(P>0.05);最大Valsalva状态与静息状态下LHA差值(ΔA′)与双侧PR杨氏模量值收缩前后的差值(ΔE)呈显著负相关(左侧r=-0.444,P=0.008;右侧r=-0.488,P=0.002)。结论经会阴三维超声联合SWE可定量评估肛提肌的形态及功能,为PFD的早期诊断提供依据。

Effects of reservoir fluids on sand packs consolidated by furan and epoxy resins:Static and dynamic states

One of the most effective methods for sand control is the chemical consolidation of sandstone structures.In this paper,the impacts of crude oil and brine in the static state and the impact of the flow rates of the fluids in the dynamic state have been assessed at the reservoir conditions.The analyses in this research were Young’s modulus,compressive strength,porosity,and permeability which were done on core samples after and before fluid contact.Samples made with two different resins showed good resistance to crude oil in both states.No considerable change was seen in the analyses even at high crude oil injection rates in the dynamic state.Conversely,brine caused a noticeable change in the analyses in both states.In the presence of brine at the static state,Young’s modulus and compressive strength respectively decreased by 37.5%and 34.5%for epoxy cores,whereas these parameters respectively reduced by 30%and 41%for furan cores.In brine presence at the dynamic state,compressive strength reduction was 10.28 MPa for furan and 6.28 MPa for epoxy samples and their compressive strength reached 16.75 MPa and 26.54 MPa respectively which are higher than the critical point to be known as weak sandstone core.Moreover,Young’s modulus decrease values for furan and epoxy samples were respectively 0.37 GPa and 0.44 GPa.Therefore,brine had a more destructive effect on the mechanical characteristics of samples in the static state than the dynamic one for two resins.In addition,brine injection increased permeability by about 13.6%for furan and 34.8%for epoxy.Also,porosity raised by about 21.8%for furan,and 19%for epoxy by brine injection.The results showed that the chemical sand consolidation weakens in the face of brine production along with crude oil which can lead to increasing cost of oil production and treating wellbore again.

Application of real-time shear wave elastography to Achilles tendon hardness evaluation in older adults

BACKGROUND Real-time shear wave elastography(SWE)is a non-invasive imaging technique used to measure tissue stiffness by generating and tracking shear waves in real time.This advanced ultrasound-based method provides quantitative information regarding tissue elasticity,offering valuable insights into the mechanical properties of biological tissues.However,the application of real-time SWE in the musculoskeletal system and sports medicine has not been extensively studied.AIM To explore the practical value of real-time SWE for assessing Achilles tendon hardness in older adults.METHODS A total of 60 participants were enrolled in the present study,and differences in the elastic moduli of the bilateral Achilles tendons were compared among the following categories:(1)Age:55-60,60-65,and 65-70-years-old;(2)Sex:Male and female;(3)Laterality:Left and right sides;(4)Tendon state:Relaxed and tense state;and(5)Tendon segment:Proximal,middle,and distal.RESULTS There were no significant differences in the elastic moduli of the bilateral Achilles tendons when comparing by age or sex(P>0.05).There were,however,significant differences when comparing by tendon side,state,or segment(P<0.05).CONCLUSION Real-time SWE plays a significant role compared to other examination methods in the evaluation of Achilles tendon hardness in older adults.