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Effect of Multiple Coatings of One-step Self-etching Adhesive on Microtensile Bond Strength to Primary Dentin 被引量:5
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作者 Lin Ma Jian-feng Zhou +3 位作者 Jian-guo Tan Quan Jing Ji-zhi Zhao Kuo Wan 《Chinese Medical Sciences Journal》 CAS CSCD 2011年第3期146-151,共6页
Objective To investigate the effect of multiple coatings of the one-step self-etching adhesive on immediate microtensile bond strength to primary dentin.Methods Twelve caries-free human primary molars were randomly di... Objective To investigate the effect of multiple coatings of the one-step self-etching adhesive on immediate microtensile bond strength to primary dentin.Methods Twelve caries-free human primary molars were randomly divided into 2 groups with 6 teeth each.In group 1,each tooth was hemisected into two halves.One half was assigned to control subgroup 1,which was bonded with a single-step self-etching adhesive according to the manufacturer's instructions;the other half was assigned to experimental subgroup 1 in which the adhesive was applied three times before light curing.In group 2,the teeth were also hemisected into two halves.One half was assigned to control subgroup 2,which was bonded with the single-step self-etching adhesive according to the manufacturer's instructions;the other half was assigned to experimental subgroup 2 in which three layers of adhesive were applied with light curing each successive layer.Microtensile bond strength was immediately tested after specimen preparation.Results When the adhesive was applied three times before light curing,the bond strength of the experimental subgroup 1(n=33,57.49±11.61 MPa) was higher than that of the control subgroup 1(n=31,49.71±11.43 MPa,P<0.05).When using the technique of applying multiple layers of adhesive with light curing each successive layer,no difference of immediate bond strength was observed between the control subgroup 2 and the experimental subgroup 2(P>0.05).Conclusion Multiple coatings of one-step self-etching adhesive can increase the immediate bond strength to primary dentin when using the technique of light-curing after applying three layers of adhesive. 展开更多
关键词 self-etching adhesive microtensile bond test primary dentin multiple coatings
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Multiple Coatings can Improve the Bond Durability of One-step Self-etching Adhesive to Primary Dentin
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作者 Lin Ma Jian-feng Zhou +2 位作者 Quan Jing Ji-zhi Zhao Kuo Wan 《Chinese Medical Sciences Journal》 CAS CSCD 2012年第2期106-111,共6页
Objective To investigate whether multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin. Methods Twelve caries-free human primary molars were randomly divided into 2 gro... Objective To investigate whether multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin. Methods Twelve caries-free human primary molars were randomly divided into 2 groups. In group 1, each tooth was hemisected into 2 halves. One half was assigned to the control subgroup 1, which was bonded with a commercially available one-step self-etching adhesive according to the manufacturer's instruc- tions; the other half was assigned to experimental subgroup 1, in which the adhesive was applied three times before light curing. In group 2, one split half tooth was bonded with a commercially available one-step self-etching adhesive according to the manufacturer's instructions; for the other half, three layers of adhesive were applied with each successive layer of light curing. Specimens were stored in 0.9% NaC1 containing 0.02% sodium azide at 37℃ for 18 months and then were subjected to microtensile bond strength test and the fracture mode analysis. Results When the adhesive was applied three times before light curing, the bond strength of the ex- perimental subgroup 1 was significantly higher than that of the control subgroup 1 (47.46__+13.91 vs. 38.12+11.21 MPa, P〈O.05). When using the technique of applying multiple layers of adhesive with each successive layer of light curing, no difference was observed in bond strength between the control subgroup and the experimental subgroup (39.40+8.87 vs. 40.87-+9.33 MPa, P〉O.05). Conclusion Multiple coatings can improve the bond durability of one-step self-etching adhesive to primary dentin when using the technique of light-curing after applying 3 layers of adhesive. 展开更多
关键词 self-etching adhesive microtensile bond strength test primary dentin multiple coatings
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Effect of reagent films on coupling relationship between glass surface and particles 被引量:1
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作者 李明 吴超 +1 位作者 刘一静 闫晖 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第11期2799-2805,共7页
The experiments were conducted to investigate the behavior of airborne particles adhering to the glass slides which were coated by several reagent films. The results showed that the adhesion level could be significant... The experiments were conducted to investigate the behavior of airborne particles adhering to the glass slides which were coated by several reagent films. The results showed that the adhesion level could be significantly changed by the reagent films. There were no evident rules between the average size of particles and sampling time interval, the placing angle and reagent concentration. The average particle size on the surface coated by composite reagent (2-3 μm) was smaller than that on the single reagent coated surface, while the largest particle size (4-5 μm) was observed on the surface coated with the Tween 60. The experiment also demonstrated that the best adhesive performance was obtained on the surface which was coated with 0.5% SDBS and 0.5% fluorocarbon composite reagents. The experiment results indicated that each reagent had a certain optimum adhesive range to the particle. The composite reagents with different proportion of single reagents exhibited some particular physical and chemical properties, which could effectively change the adhesive performance between the solid surface and the particles. 展开更多
关键词 micro-particles adhesION glass surface reagent film size distribution
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Self-etching adhesives:possible new pulp capping agents to vital pulp therapy
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作者 Chun CUI Xiu-Neng ZHOU Wei-Min CHEN 《Frontiers of Medicine》 SCIE CSCD 2011年第1期77-79,共3页
Pulp capping is one of the solving for keeping vital pulp in the case of dentin caries,reversible pulpitis or traumatic pulp exposure.The presence of bacteria on the cavity walls or in the pulp was the major factor th... Pulp capping is one of the solving for keeping vital pulp in the case of dentin caries,reversible pulpitis or traumatic pulp exposure.The presence of bacteria on the cavity walls or in the pulp was the major factor that leads to the failure of pulp capping.Traditional pulp capping agent,calcium hydroxide,may not prevent microleakage.Selfetching system is a newly developed adhesive system,which could provide less microleakage and would not break down or dissolve,preventing the oral fluids and bacteria from the pulp along the cavity wall.This may reduce such clinical problems as postoperative sensitivity,secondary caries and marginal discoloration.Researches showed that some kinds of self-etching adhesives induced the mild to moderate inflammatory pulp response,with negative bacterial staining.Inclusion of antibacterial components into self-etching system,such as 12-methacryloyloxydodecylpyridinium bromide(MDPB)may inhibit bacteria and provide better clinical effects.It is speculated that using the self-etching adhesive system containing the antibacterial agent,such as MDPB,to the dental pulp directly or indirectly,may inhibit bacteria after the placement of restoration as well as residual bacteria in the cavity. 展开更多
关键词 dental pulp pulp capping self-etching adhesives antibacterial components
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Er:YAG激光联合3M ESPE Adper Easy-one粘结剂堵塞牙本质小管的体外研究 被引量:16
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作者 李鑫 陈新梅 +3 位作者 郭蓝 申思敏 王盼盼 郑黎薇 《牙体牙髓牙周病学杂志》 CAS 北大核心 2012年第2期92-95,共4页
目的:研究Er:YAG激光联合3M ESPE Adper Easy-one自酸蚀树脂粘结剂堵塞牙本质小管的效果,为其治疗牙本质敏感提供实验室依据。方法:选择因正畸需要拔除的牙体完整、无龋损的前磨牙8个,制备牙颈部牙本质小管暴露的牙本质样本32个,按处理... 目的:研究Er:YAG激光联合3M ESPE Adper Easy-one自酸蚀树脂粘结剂堵塞牙本质小管的效果,为其治疗牙本质敏感提供实验室依据。方法:选择因正畸需要拔除的牙体完整、无龋损的前磨牙8个,制备牙颈部牙本质小管暴露的牙本质样本32个,按处理方法不同随机分为4组:空白对照组、Er:YAG激光处理组、3M ESPE Adper Easy-one粘结剂处理组、Er:YAG激光、3M ESPE Adper Easy-one粘结剂联合处理组,扫描电镜下比较牙本质表面超微形态、纵断面的粘结剂牙本质界面的混合层、树脂突的微观表现,观察牙本质小管的堵塞效果。结果:Er:YAG激光联合3M ESPE Adper Easy-one粘结剂组与粘结剂组的堵塞牙本质小管的表面微观形态类似,牙本质小管被完全堵塞;激光处理组的牙本质小管基本完全堵塞;纵断面观察联合组粘结界面可见到清晰的混合层和树脂突,且树脂突深度较粘结剂组明显增加,激光组纵断面牙本质小管内无明显堵塞物。结论:Er:YAG激光与3M ESPE Adper Easy-one粘结剂联合处理能够有效的堵塞牙本质小管。 展开更多
关键词 牙本质敏感 ER:YAG激光 自酸蚀树脂粘结剂 扫描电镜 牙本质小管
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双增韧剂改性环氧树脂 被引量:7
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作者 姚兴芳 李玉男 +2 位作者 孙言乐 张海 罗俊会 《塑料》 CAS CSCD 北大核心 2012年第2期90-93,共4页
采用双增韧剂(端羧基液体丁腈橡胶(CTBN)与纳米SiO2(n-SiO2))对环氧树脂(ER)增韧,并用正交试验方法对其增韧条件进行了优化。通过对固化产物力学性能、热稳定性及微观形态的测定及表征,结果表明:优化的胶黏剂制备条件是双增韧剂(CTBN+n-... 采用双增韧剂(端羧基液体丁腈橡胶(CTBN)与纳米SiO2(n-SiO2))对环氧树脂(ER)增韧,并用正交试验方法对其增韧条件进行了优化。通过对固化产物力学性能、热稳定性及微观形态的测定及表征,结果表明:优化的胶黏剂制备条件是双增韧剂(CTBN+n-SiO2)占ER的1/8、CTBN与n-SiO2的比例为2∶1、反应温度为180℃、反应时间为2.5 h,胶黏剂冲击强度达到18.24 kJ/m2;红外表明(FTIR)双增韧剂均与ER发生作用,热重分析(TG)结果显示固化产物热稳定性良好,扫描电镜(SEM)对固化产物微观形态的观察结果显示双增韧剂对ER增韧作用明显。 展开更多
关键词 双增韧剂 改性 环氧树脂 冲击强度 胶黏剂
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焦粉成型技术 被引量:31
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作者 刘长林 雒和明 苟国俊 《环境污染治理技术与设备》 CSCD 北大核心 2002年第12期73-75,共3页
冶金、化工、电石生产企业 ,因生产工艺要求需要将大块的焦炭破碎成一定粒度的块焦 ,破碎过程要产生2 0 %— 2 5 %的焦粉。本文针对目前工业废弃焦粉再利用问题 ,通过深入调查 ,反复试验 ,取得了很好的效果。为冶金、化工。
关键词 焦粉成型技术 添加剂 黏结剂 润湿剂 烘干 化学活性 抗压强度 焦炭 工业废弃物 资源利用
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表面处理对锂离子电池胶粘剂性能的影响 被引量:2
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作者 周震涛 严燕 《电池》 CAS CSCD 北大核心 2000年第6期239-240,共2页
在锂离子电池的聚偏氟乙烯 (PVDF)胶粘剂中添加偶联剂和以铜氨液对集流体表面处理 ,可显著提高胶粘剂对集流体的粘接强度 ,对铝片粘结由 2 2 8MPa提高到 4 31MPa ,对铜片粘结由 5 17MPa提高到 11 10MPa ,并能改善胶层耐电解液性能。
关键词 聚偏氟乙烯 胶粘剂 偶联剂 铜氨溶液 表面处理
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Al(OH)_3胶体悬浮液对胶带粘性表面富脂潜指纹的显现研究 被引量:3
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作者 高峰 张斯儒 +4 位作者 马荣梁 李孝君 胡文锋 曲会英 赵越 《刑事技术》 2016年第5期383-386,共4页
目的使用Al(OH)_3胶体悬浮液为新型小颗粒(SPR)指纹显现试剂对胶带粘面上富脂潜指纹的显现效果进行研究。方法以Al(OH)_3、NaOH、H_2C_2O_4、C_(18)H_(29)NaO_3S为原料,制备Al(OH)_3胶体SPR指纹显现试剂,研究C_(18)H_(29)NaO_3S浓度及... 目的使用Al(OH)_3胶体悬浮液为新型小颗粒(SPR)指纹显现试剂对胶带粘面上富脂潜指纹的显现效果进行研究。方法以Al(OH)_3、NaOH、H_2C_2O_4、C_(18)H_(29)NaO_3S为原料,制备Al(OH)_3胶体SPR指纹显现试剂,研究C_(18)H_(29)NaO_3S浓度及指纹遗留时间对胶带粘面富脂潜指纹显现效果的影响,并与两种市售SPR试剂的指纹显现效果进行比较。结果当C_(18)H_(29)NaO_3S浓度为8.61 mmol/L时,所制Al(OH)_3胶体SPR指纹显现试剂对遗留时间为24 h以内的潜指纹显现效果良好,对1 h的新鲜潜指纹显现效果优于SPR1001 Dark试剂。结论胶带粘面富脂潜指纹可用Al(OH)_3胶体悬浮液SPR试剂很好地显现,纹路清晰、细节特征明显且与背景对比度高。 展开更多
关键词 指纹显现 胶带 富脂潜指纹 Al(OH)3胶体悬浮液 小颗粒悬浮液试剂
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炼焦配煤中添加剂对焦炭质量的影响 被引量:7
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作者 商铁成 《洁净煤技术》 CAS 2012年第6期39-43,48,共6页
以华北地区某焦化厂炼焦用煤为研究对象,通过对基础煤样和添加剂性质分析,说明各煤样及添加剂的优势和不足,并提出了具体的配煤方案,得到了配合煤及焦炭的性质。依据煤岩学观点和共炭化炼焦理论,以焦油沥青、石油沥青替代部分强黏结煤,... 以华北地区某焦化厂炼焦用煤为研究对象,通过对基础煤样和添加剂性质分析,说明各煤样及添加剂的优势和不足,并提出了具体的配煤方案,得到了配合煤及焦炭的性质。依据煤岩学观点和共炭化炼焦理论,以焦油沥青、石油沥青替代部分强黏结煤,或以焦粉、石油焦作为瘦化剂炼焦,通过与基础炼焦煤配合后进行炼焦试验,对添加剂在炼焦配煤中的作用进行分析。结果表明:沥青是较为理想的黏结剂,配入量以3%~5%为宜;无烟煤最佳配入量为5%;无烟煤、焦粉、石油焦是常用的瘦化剂,其中无烟煤提高焦炭耐磨强度作用显著,焦粉降低配合煤挥发分作用突出,石油焦在降灰及提高焦炭块度等方面作用更为明显。 展开更多
关键词 炼焦配煤 黏结剂 瘦化剂 改质沥青 无烟煤 焦粉 石油焦
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偶联剂对聚硫密封剂性能的影响 被引量:1
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作者 王磊 刘彩召 +2 位作者 孙明明 张绪刚 张斌 《黑龙江科学》 2016年第12期20-23,共4页
通过在聚硫密封剂体系中引入偶联剂,研究了其种类对密封剂与各种界面老化前后的黏结效果,同时考察了偶联剂对聚硫密封剂耐介质、工艺性能及贮存稳定性的影响。结果表明:单一的偶联剂并不能满足密封剂对多种界面都达到可靠稳定黏结的要... 通过在聚硫密封剂体系中引入偶联剂,研究了其种类对密封剂与各种界面老化前后的黏结效果,同时考察了偶联剂对聚硫密封剂耐介质、工艺性能及贮存稳定性的影响。结果表明:单一的偶联剂并不能满足密封剂对多种界面都达到可靠稳定黏结的要求。使用550与401共混偶联剂,聚硫密封剂的综合性能较好。 展开更多
关键词 聚硫密封剂 偶联剂 耐油 耐盐水 黏结性能
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鞋用聚氨酯胶粘剂的改性研究 被引量:1
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作者 冯炎龙 吕健全 《绍兴文理学院学报(自然科学版)》 2002年第3期63-65,共3页
本文以二甘醇代替其它多元醇与已二酸反应合成聚酯多元醇,再以合适的OH/NCO比与二异氰酸酯TDI生产聚氨酯胶粘剂。成本低,各项粘接性能达到超过同类产品,同时利用了制备乙二醇时的副产品二甘醇,一举数得。
关键词 聚氨酯胶粘剂 鞋用胶粘剂 改性 粘接性能 二甘醇 已二酸
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脉冲Nd:YAG激光联合3M ESPE粘结剂对牙本质小管封闭作用的体外研究 被引量:6
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作者 杨宾 王彬娉 +4 位作者 吴卓骏 陈奕苗 王秀丽 陆丽英 郁豆 《牙体牙髓牙周病学杂志》 CAS 2015年第9期538-540,共3页
目的:探讨脉冲Nd:YAG激光与3M ESPE粘结剂联合应用对牙本质小管的封闭作用。方法:选择因重度牙周炎而拔除的牙体完整、无龋损的第二磨牙30个,制备成30个牙本质小管口暴露的牙本质样本后,随机分为3组(n=10):空白对照组、单纯Nd:YAG激光... 目的:探讨脉冲Nd:YAG激光与3M ESPE粘结剂联合应用对牙本质小管的封闭作用。方法:选择因重度牙周炎而拔除的牙体完整、无龋损的第二磨牙30个,制备成30个牙本质小管口暴露的牙本质样本后,随机分为3组(n=10):空白对照组、单纯Nd:YAG激光照射组、Nd:YAG激光照射联合3M ESPE粘结剂处理组;按分组进行相应处理后,扫描电镜下观察各组牙本质表面的形态变化,并分别测量各组牙本质小管口的直径。结果:与单纯激光照射组相比,激光联合粘结剂组的牙本质小管封闭更完全;对照组、激光组、联合组的牙本质小管管径(μm)分别为:1.793368±0.284225、1.401832±0.539471、1.009611±0.503342,组间两两相比差异均有统计学意义(P<0.05)。结论:Nd:YAG激光与3M ESPE粘结剂联合应用具有良好的牙本质小管封闭作用。 展开更多
关键词 牙本质过敏 脉冲ND:YAG激光 3M ESPE粘结剂 牙本质小管
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双相陶瓷材料——羟基磷灰石与细胞黏附剂协同促进成骨细胞增殖的研究
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作者 黄力 赵劲民 《右江民族医学院学报》 2016年第2期132-135,共4页
目的观察在体外涂刷细胞黏附剂(cell adherent reagent,CAR)对羟基磷灰石(biphasic calcium phosphate,BCP)生物学活性的影响。方法成骨细胞被种植入经过CAR涂刷的BCP材料(实验组,即BCP-CAR组)和用生理盐水处理过的BCP材料(空白组,即BCP... 目的观察在体外涂刷细胞黏附剂(cell adherent reagent,CAR)对羟基磷灰石(biphasic calcium phosphate,BCP)生物学活性的影响。方法成骨细胞被种植入经过CAR涂刷的BCP材料(实验组,即BCP-CAR组)和用生理盐水处理过的BCP材料(空白组,即BCP组)中,在培养2d、5d、8d后,分别测定细胞增殖、细胞生存活力、碱性磷酸酶(ALP)活性,RT-PCR用于检测成骨细胞runt转录相关因子2(RUNX2)、ALP、骨唾液蛋白(BSP)和Ⅰ型胶原酶(COLⅠ)的基因表达。结果与空白组对比,涂刷了CAR的BCP材料,其成骨细胞的细胞增殖和ALP活力上调,RUNX2、BSP、ALP及COLⅠ基因表达上调,差异均有统计学意义(P<0.05)。结论经过CAR涂刷能增强BCP材料的生物活性,这为其临床应用提供了重要的依据。 展开更多
关键词 细胞黏附剂 羟基磷灰石 吸附能力 成骨细胞
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化学交联在牙本质粘接修复中的应用及展望 被引量:6
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作者 古丽莎 吴倩 《中华口腔医学研究杂志(电子版)》 CAS 2019年第3期129-135,共7页
牙本质混合层裸露胶原水解变性是导致树脂粘接修复失败的主要原因。化学交联作用可增加混合层胶原纤维间或纤维内的分子键或氢键结合,提高胶原的机械性能及抗酶解能力,从而改善树脂牙本质粘接修复的耐久性。因此,本文针对化学交联改善... 牙本质混合层裸露胶原水解变性是导致树脂粘接修复失败的主要原因。化学交联作用可增加混合层胶原纤维间或纤维内的分子键或氢键结合,提高胶原的机械性能及抗酶解能力,从而改善树脂牙本质粘接修复的耐久性。因此,本文针对化学交联改善树脂牙本质粘接耐久性的机制及其应用效果作一分析探讨。 展开更多
关键词 胶原 牙本质 粘着剂 交联试剂
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化学预处理对微型钻头沉积类金刚石薄膜附着力的影响 被引量:6
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作者 李衍飞 《硬质合金》 CAS 北大核心 2011年第5期300-304,共5页
在刀具上沉积类金刚石(DLC)薄膜的关键技术问题是如何提高DLC薄膜的附着力,以发挥DLC薄膜在刀具涂层领域的优势。本文通过对微型钻头表面进行不同的化学预处理后利用射频等离子体化学气相沉法沉积DLC薄膜,对影响膜基附着力的内在规律进... 在刀具上沉积类金刚石(DLC)薄膜的关键技术问题是如何提高DLC薄膜的附着力,以发挥DLC薄膜在刀具涂层领域的优势。本文通过对微型钻头表面进行不同的化学预处理后利用射频等离子体化学气相沉法沉积DLC薄膜,对影响膜基附着力的内在规律进行了探讨。结果表明:采用简单酸碱腐蚀(先后使用NaOH溶液和HNO3溶液进行腐蚀)对DLC薄膜附着力的提高有一定作用,而综合腐蚀(首先使用酸碱腐蚀,然后使用Murakami试剂腐蚀)的效果更佳;此外,使用Murakami试剂腐蚀时间过长(超过6 min)会影响钻头本体的机械强度。实验结果对于DLC薄膜作为微型钻头涂层的应用具有很好的指导意义。 展开更多
关键词 类金刚石(DLC)薄膜 表面腐蚀 Murakami试剂 附着力
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