The pulse-control operation technique which alternates between total reflux operation and total efflux operation in batch distillation was studied along with the minimum amount of slop cut. Total reflux time was confi...The pulse-control operation technique which alternates between total reflux operation and total efflux operation in batch distillation was studied along with the minimum amount of slop cut. Total reflux time was confirmed by dynamic simulation, and total efflux time was adopted by statistic method. For the mixture of hexane and cyclohexane and the traditional constant reflux ratio operation strategy, the amount of slop cut is 1.8-2.1 times of the minimum amount of slop cut; whereas for the pulse-control operation strategy, it is 1. 2 -1.4 times of the minimum amount of slop cut. So compared with the traditional constant reflux ratio operation, the pulse-control operation can decrease the amount of slop cut and operation time, and meanwhile, enhance separation efficiency and yield.展开更多
The new mode of operation for slop cut withdrawal in batch distillation, i.e., draining Column liquid holdup at the end of slop cut period, was proposed. And the stopping criterion for the operation was investigated, ...The new mode of operation for slop cut withdrawal in batch distillation, i.e., draining Column liquid holdup at the end of slop cut period, was proposed. And the stopping criterion for the operation was investigated, Experiments were carded out with isopropanol-n-propanol binary system and isopropanol-n-propanol-n-butanol ternary system in a distillation column with a liquid collector installed between the reboiler and the column section, Experimental results in a Ф 45mm batch column show that the proposed policy can overcome the flywheel effect caused by column liquid holdup and thus cut down operation time and energy consumption 31%-61%.展开更多
The new mode of operation for slop cut withdrawal in batch distillation, i.e., draining column liquid holdup at the end of slop cut period, was proposed. And the stopping criterion for the operation was investigated. ...The new mode of operation for slop cut withdrawal in batch distillation, i.e., draining column liquid holdup at the end of slop cut period, was proposed. And the stopping criterion for the operation was investigated. Experiments were carried out with isopropanol-n-propanol binary system and isopropanol-n-propanol-n-butanol ternary system in a distillation column with a liquid collector installed between the reboiler and the column section. Experimental results in a 45mm batch column show that the proposed policy can overcome the flywheel effect caused by column liquid holdup and thus cut down operation time and energy consumption 31%—61%.展开更多
The paper analysesthe treatment measurementsof railway roadbed main diseases in permafrost regions. Taking lessonsfrom the diseases finallythe mature experiences of treatments are offered.
文摘The pulse-control operation technique which alternates between total reflux operation and total efflux operation in batch distillation was studied along with the minimum amount of slop cut. Total reflux time was confirmed by dynamic simulation, and total efflux time was adopted by statistic method. For the mixture of hexane and cyclohexane and the traditional constant reflux ratio operation strategy, the amount of slop cut is 1.8-2.1 times of the minimum amount of slop cut; whereas for the pulse-control operation strategy, it is 1. 2 -1.4 times of the minimum amount of slop cut. So compared with the traditional constant reflux ratio operation, the pulse-control operation can decrease the amount of slop cut and operation time, and meanwhile, enhance separation efficiency and yield.
文摘The new mode of operation for slop cut withdrawal in batch distillation, i.e., draining Column liquid holdup at the end of slop cut period, was proposed. And the stopping criterion for the operation was investigated, Experiments were carded out with isopropanol-n-propanol binary system and isopropanol-n-propanol-n-butanol ternary system in a distillation column with a liquid collector installed between the reboiler and the column section, Experimental results in a Ф 45mm batch column show that the proposed policy can overcome the flywheel effect caused by column liquid holdup and thus cut down operation time and energy consumption 31%-61%.
文摘The new mode of operation for slop cut withdrawal in batch distillation, i.e., draining column liquid holdup at the end of slop cut period, was proposed. And the stopping criterion for the operation was investigated. Experiments were carried out with isopropanol-n-propanol binary system and isopropanol-n-propanol-n-butanol ternary system in a distillation column with a liquid collector installed between the reboiler and the column section. Experimental results in a 45mm batch column show that the proposed policy can overcome the flywheel effect caused by column liquid holdup and thus cut down operation time and energy consumption 31%—61%.
文摘The paper analysesthe treatment measurementsof railway roadbed main diseases in permafrost regions. Taking lessonsfrom the diseases finallythe mature experiences of treatments are offered.