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Highly efficient solution-processed CZTSSe solar cells based on a convenient sodium-incorporated post-treatment method 被引量:9
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作者 Biwen Duan Linbao Guo +7 位作者 Qing Yu Jiangjian Shi Huijue Wu Yanhong Luo Dongmei Li Sixin Wu Zhi Zheng Qingbo Meng 《Journal of Energy Chemistry》 SCIE EI CAS CSCD 2020年第1期196-203,I0007,共9页
In CZTSSe solar cells,a simple sodium-incorporation post-treatment method toward solution-processed Cu2Zn Sn S4precursor films is presented in this work.An ultrathin NaCl film is deposited on Cu2Zn Sn S4precursor film... In CZTSSe solar cells,a simple sodium-incorporation post-treatment method toward solution-processed Cu2Zn Sn S4precursor films is presented in this work.An ultrathin NaCl film is deposited on Cu2Zn Sn S4precursor films by spin-coating NaCl solution.In subsequent selenization process,the introduction of Na Cl is found to be benefacial for the formation of Cu2-xSe,which can further facilitate the element transportation,leading to dense and smooth CZTSSe films with large grains and less impurity Cu2Sn(S,Se)3phase.SIMS depth profiles confirm the gradient distribution of the sodium element in Na-doped absorbers.Photoluminescence spectra show that the introduction of appropriate sodium into the absorber can inhibit the band tail states.As high as 11.18% of power conversion efficiency(PCE)is achieved for the device treated with 5 mg mL^-1 NaCl solution,and an average efficiency of Na-doped devices is 10.71%,13%higher than that of the control groups(9.45%).Besides,the depletion width and the charge recombination lifetime can also have regular variation with sodium treatment.This work offers an easy modification method for high-quality Na-doped CZTSSe films and high-performance devices,in the meantime,it can also help to further understand the effects of sodium in CZTSSe solar cells. 展开更多
关键词 Thin film solar cell CZTSSe sodium doping POST-treatment Spin-coating method
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Preliminary Findings on the Use of Targeted Therapy with Pazopanib and Other Agents in Combination with Sodium Phenylbutyrate in the Treatment of Glioblastoma Multiforme 被引量:1
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作者 Stanislaw R. Burzynski Tomasz J. Janicki +1 位作者 Gregory S. Burzynski Sheldon Brookman 《Journal of Cancer Therapy》 2014年第14期1423-1437,共15页
The most common and aggressive type of brain tumor is glioblastoma multiforme (GBM). The prognosis for GBM remains poor with a five-year survival rate between 1% and 2%. The prospects for patients with recurrent GBM (... The most common and aggressive type of brain tumor is glioblastoma multiforme (GBM). The prognosis for GBM remains poor with a five-year survival rate between 1% and 2%. The prospects for patients with recurrent GBM (RGBM) are much worse, with the majority dying within 6 months. This publication provides a brief description of the treatment of 11 GBM patients treated with sodium phenylbutyrate (PB) in combination with pazopanib, m-TOR inhibitors, and other agents. The treatment was associated with tolerable side effects and resulted in objective responses in 54.5% of cases (complete response 18.2%, partial response 36.3%) and 27.3% cases of stable disease. The preferable treatment regimen consisted of PB, pazopanib, dasatinib, everolimus, and bevacizumab (BVZ). For various reasons not all patients were compliant with the treatment regimen. In patients who strictly complied with the treatment plan, all responded as CR or PR. Based on preliminary findings, the authors propose further phase I/II clinical trials with PB in combination with pazopanib, dasatinib, everolimus, and BVZ in patients with RGBM who failed standard surgery, radiation therapy and chemotherapy. With proper dose reductions, the treatment appears to be well-tolerated. Molecular profiling of patient subgroups with favorable genomic signatures may help to select patients for future studies. 展开更多
关键词 Gliobastoma MULTIFORME Personalized Targeted AGENTS sodium PHENYLBUTYRATE treatment of GLIOBLASTOMA MULTIFORME
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Preparation of Spherical Silica-supported Biosorbent for Copper Ions Removal in Wastewater Based on Sol-gel Reaction and Simple Treatment with Sodium Hydroxide 被引量:1
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作者 ZHENG Li JIANG Feng-hua +2 位作者 DONG Ping-jun ZHUANG Qian-fen LI Feng 2 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2010年第3期355-359,共5页
A new and effective strategy was proposed for preparing new organic-inorganic composite biosorbent with spherical silica as supporting core and chitosan(CS)-based hybrid layer as shell based on sol-gel reaction and ... A new and effective strategy was proposed for preparing new organic-inorganic composite biosorbent with spherical silica as supporting core and chitosan(CS)-based hybrid layer as shell based on sol-gel reaction and simple treatment with sodium hydroxide(NaOH). The coating layer was covalently bound on the supporting silica through polysaccharide incorporated sol-gel process starting from CS and inorganic precursor γ-glycidoxypropyltrimethoxysiloxane(GPTMS). GPTMS had epoxide groups and cross-linked amine groups of CS to avoid its acidic solubilization. The composite biosorbent had coarse surface due to the wet phase-inversion by treating in NaOH solution. The prepared biosorbent could be used in treating electric plating wastewater. 展开更多
关键词 CHITOSAN sodium hydroxide BIOSORPTION Waste treatment
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Synthesis of Sodium Beta Alumina Films by Heat Treatment of Sodium Aluminum Oxides
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作者 池晨 Hirokazu KATSUI Takashi GOTO 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2016年第1期6-10,共5页
Sodium beta alumina(Na-β-alumina) films were synthesized by heat treatment of NaAl6O(9.5)and γ-NaA1O2 films at temperatures of 1 373-1 573 K.Single-phase γ-NaA1O2 and NaAl6O(9.5) films were prepared by laser ... Sodium beta alumina(Na-β-alumina) films were synthesized by heat treatment of NaAl6O(9.5)and γ-NaA1O2 films at temperatures of 1 373-1 573 K.Single-phase γ-NaA1O2 and NaAl6O(9.5) films were prepared by laser chemical vapor deposition at the deposition temperatures of 976 and 1 100 K,respectively.Subsequent heat treatment of the films resulted in the formation of Na-β-alumina with α-Al2O3 at temperatures above 1 373 K for NaAl6O(9.5) and 1 473 K for γ-NaA1O2.On heat treatment at temperatures of 1 473-1 573 K,the faceted morphology with terraces of the as-deposited(110)-oriented γ-NaAlO2 films transformed to a porous morphology with platelet grains comprising Na-β-alumina and α-Al2O3.On heat treatment at temperatures of1 373-1 473 K,the pyramidal,faceted grains of as-deposited NaAl6O(9.5) films transformed to planer,shapeanisotropic morphology in the film of mixed Na-β-alumina and α-Al2O3.A dense morphology was observed in both the as-deposited and heat-treated NaAl6O(9.5) films. 展开更多
关键词 sodium beta alumina heat treatment chemical vapor deposition morphology
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Segregation Treatment and Resource Recycling of Enteric Coating and Heparin Sodium Manufacturing Wastewater
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作者 Jiang Chunhua Zhai Jian +3 位作者 Cao Guoqing Lu Xiuguo Ling Shulei Zhang Jing 《Meteorological and Environmental Research》 CAS 2014年第4期51-53,共3页
Firstly, the water-quality characteristics of intestinal lavage wastewater and enzymolysis wastewater from the typical heparin sodium pro- ductive process were analyzed, and then the segregation treatment was applied ... Firstly, the water-quality characteristics of intestinal lavage wastewater and enzymolysis wastewater from the typical heparin sodium pro- ductive process were analyzed, and then the segregation treatment was applied in the treatment of enteric coating and heparin sodium manufacturing wastewater. Finally, the treatment of the two kinds of wastewater by different methods were discussed. The results showed that, COD of enzymolysis wastewater treated by centrifugation-coagulation-Fenton reagent oxidation-adsorption process was lower than 100 mg/L, while intestinal lavage wastewater treated by coagulation-ASBR-SBR process could meet the first standard of Comprehensive Discharge Standard of Sewage (GB8978-1996) after one month of continuous operation. 展开更多
关键词 Enteric coating and heparin sodium manufacturing wastewater Segregation treatment Resource recovery technology ASBR-SBR Fenton reagent China
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Pre-desilication and digestion of gibbsitic bauxite with lime in sodium aluminate liquor 被引量:13
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作者 Xiao-lin Pan Hai-yan Yu +2 位作者 Kai-wei Dong Gan-feng Tu Shi-wen Bi 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2012年第11期973-977,共5页
The effect of lime on the pre-desilication and digestion of gibbsitic bauxite in synthetic sodium aluminate liquor at different tem- peratures was investigated. The bauxite is comprised of gibbsite, aluminogoethite, h... The effect of lime on the pre-desilication and digestion of gibbsitic bauxite in synthetic sodium aluminate liquor at different tem- peratures was investigated. The bauxite is comprised of gibbsite, aluminogoethite, hematite, kaolin, quartz, and minor boehmite. Lime in- creases the desilication efficiency of the bauxite during the pre-desilication process by promoting the conversion of sodalite and cancrinite to hydrogamet. Desilication reactions during the digestion process promoted by lime result in the loss of A1203 entering the red mud, but the amount of aluminogoethite-to-hematite conversion promoted by lime leads to the increase of aluminogoethific A1203 entering the digested liquor. The alumina digestion rate at 245~C is higher than that at 145 C due to the more pronounced conversion of aluminogoethite to hema- tite. The soda consumption during the digestion process decreases due to lime addition, especially at higher temperatures. 展开更多
关键词 bauxite ore treatment LIME sodium aluminate DESILICATION alumina Bayer process
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Alkaline pretreatment for chlorine removal from high-chlorine rhodochrosite 被引量:1
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作者 Xing-ran Zhang Zuo-hua Liu +3 位作者 Wen-sheng Li Ya-ya Cheng Jun Du Chang-yuan Tao 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2016年第11期1252-1257,共6页
Chloride in manganese ore adversely affects mineral extraction. The mechanisms and the factors that influence an alkali pretreatment to removal chlorine from manganese ore were explored to eliminate hazards posed by c... Chloride in manganese ore adversely affects mineral extraction. The mechanisms and the factors that influence an alkali pretreatment to removal chlorine from manganese ore were explored to eliminate hazards posed by chlorine during the electrolysis of manganese. The results showed that sodium carbonate, when used as an alkaline additive, promoted the dissolution of insoluble chloride, enhanced the migration of chloride ions, and effectively stabilized Mn^(2+). The optimal conditions were a sodium carbonate concentration of 0.45 mol·L^(-1), a liquid-solid ratio of 5:1 mL ·g^(-1), a reaction time of 1 h, and a temperature of 25°C. The chlorine removal efficiency was greater than 95%, and the ore grade(Mn) was increased by 2.7%. 展开更多
关键词 manganese ore treatment rhodochrosite sodium carbonation pretreatment dechlorination
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Effect of Thermal Treatment and Acid Leaching Process on Pore Characteristics of Nanometer Porous Glass 被引量:2
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作者 韩建军 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2007年第1期129-131,共3页
Porous glass was prepared by thermally treating sodium borosilicate glass for different time, the effect of thermal treatment on pore size distribution was discussed and the pore size of the prepared porous glass was ... Porous glass was prepared by thermally treating sodium borosilicate glass for different time, the effect of thermal treatment on pore size distribution was discussed and the pore size of the prepared porous glass was measured by scanning electron microscopy (SEM) and differential thermal analysis (DTA). The results show that the optimum porous glass with an average diameter of 80 nm can be prepared by thermal treatment at 600℃ for 12 h and then acid treatment for 12 h in 2 mol·L^-1 hydrochloric acid solution. 展开更多
关键词 porous glass: thermal treatment sodium borosilicate glass phase-separate
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Comparison between the Quality Traits of Phosphate and Bicarbonate-Marinated Chicken Breast Fillets Cooked under Different Heat Treatments 被引量:1
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作者 Samer Mudalal Massimiliano Petracci +2 位作者 Silvia Tappi Pietro Rocculi Claudio Cavani 《Food and Nutrition Sciences》 2014年第1期35-44,共10页
Because the use of phosphates has being recently diminished in meat industry due to the nutritional drawbacks of phosphates, some researchers started to evaluate sodium bicarbonate as phosphate replacer in meat produc... Because the use of phosphates has being recently diminished in meat industry due to the nutritional drawbacks of phosphates, some researchers started to evaluate sodium bicarbonate as phosphate replacer in meat products. The aim of this study was to evaluate the effect of different temperature combinations of dry air-cooking treatments (Air and Core temperatures: 160 - 76, 160 - 80, 200 - 76 and 200℃ - 80℃, respectively) on chemical composition, texture properties, water activity, freezable water and bound water, color, pH, and water binding capacity of phosphate and bicarbonate-marinated chicken breast. A batch of 24 h post-mortem broiler breast meat of 80 fillets was divided into two groups of marination treatments (0.3% sodium bicarbonate n = 40, 0.3% sodium tripolyphosphate n = 40) and was vacuum tumbled (45 min, ?0.95 mbar, 20 rpm). Different temperature-combinations cooking treatments significantly modified the chemical composition. Bicarbonate marinated fillets showed higher ability to retain water (67.3% vs. 65.7%, P 0.05) during severe heat treatment and lower cook losses (30.7% vs. 33.4%, P 0.05) when compared with phosphate-marinated fillets. The effect of changing the cooking temperatures on Texture Profile Analysis (hardness, cohesiveness, gumminess, springiness, and chewiness) was more tangible in phosphate marinated fillets than bicarbonate. Bicarbonate-marinated fillets showed significant differences in the percentage of bound water, latent heat, and water activity after cooking in comparison to phosphate-marinated fillets. The results of this study revealed that phosphate-marinated fillets interacted with heat treatments in different patterns in comparison with bicarbonate-marinated fillets. 展开更多
关键词 Chicken MEAT MARINATION sodium BICARBONATE Heat treatment Quality TRAITS
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Effects of Chemical Treatment on the Physical Properties of Typha
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作者 Ibrahima Diaw Mactar Faye +1 位作者 Seckou Bodian Vincent Sambou 《Fluid Dynamics & Materials Processing》 EI 2022年第5期1409-1418,共10页
Plant-based concretes are produced from plant aggregates and a binder.Plant fibers are mainly composed of saccharides(sugars)and these sugars can decrease the concentration of Ca2+ions in the cement pore solution and ... Plant-based concretes are produced from plant aggregates and a binder.Plant fibers are mainly composed of saccharides(sugars)and these sugars can decrease the concentration of Ca2+ions in the cement pore solution and delay the formation of hydration products.To improve the interfacial bond between fibers and matrix a chemical treatment is widely used.This study investigates the effect of sodium hydroxide treatment on physical and hygroscopic properties of Typha aggregates.In particular,a 5%sodium hydroxide solution is used to treat these aggregates and their bulk and absolute densities,porosity,water content and water absorption are evaluated accordingly.Results indicate that bulk and absolute densities increase after treatment from 56.44 kg/m^(3) to 122.57 kg/m^(3) and 541.93 kg/m^(3) to 555.17 kg/m^(3),respectively.NaOH treatment reduces porosity of Typha from 89.58%to 77.92%and decreases water content from 1.4%to 1%.The treatment with sodium hydroxide reduces substantially the water absorption of the aggregates. 展开更多
关键词 sodium hydroxide treatment typha aggregates hygroscopic properties physical properties
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Recycling water glass from wet reclamation sewage of waste sodium silicate-bonded sand 被引量:2
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作者 Li-chi Wang Wen-ming Jiang +2 位作者 Xiao-long Gong Fu-chu Liu Zi-tian Fan 《China Foundry》 SCIE 2019年第3期198-203,共6页
Wet reclamation of waste sodium silicate-bonded sand produces much alkaline sewage and causes pollution. Recycling water glass from wet reclamation sewage of the waste sodium silicate-bonded sand can solve pollution i... Wet reclamation of waste sodium silicate-bonded sand produces much alkaline sewage and causes pollution. Recycling water glass from wet reclamation sewage of the waste sodium silicate-bonded sand can solve pollution issues and generate economic benefits. In this work, the wet reclamation sewage was filtered, and the filtrate was causticized with a quicklime powder to produce a lye. The effects of causticization temperature, causticization time, and the amount of quicklime powder on the causticization rate were studied. The lye was used to dissolve the silica in the filtration residue to prepare a sodium silicate solution. The effects of the mass of filtration residue, dissolution temperature, and dissolution time on sodium silicate modulus were studied. Finally, the recycled water glass was obtained by concentrating the sodium silicate solution, and the bonding strength of the recycled water glass was tested. The results showed that the causticization rate could be improved by increasing the amount of quicklime powder, causticization temperature, and causticization time, and the highest causticization rate was above 92%. Amorphous silica in the filtration residue dissolved in the lye. Increasing the amount of the filtration residue, dissolution temperature, and dissolution time could improve the sodium silicate modulus. The bonding strength of the recycled water glass was close to that of commercial water glass. The recycled water glass could be used as a substitute for the commercial water glass. 展开更多
关键词 WASTE sodium silicate-bonded SAND wet reclamation SEWAGE treatment CAUSTICIZATION RECYCLING water glass
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Bacterial Deterioration in the Limestone Minaret of Prince Muhammad and Suggested Treatment Methods, Akhmim, Egypt
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作者 Elashmawy Abd-Elkareem Ahmed Rehab Mustafa Mohamed 《Geomaterials》 CAS 2022年第3期37-58,共22页
El-Amir Muhammad’s minaret in Akhmim, Sohag, Egypt, is constructed of limestone and has been exposed to many factors of damage as a result of the high levels of ground water. Limestone is strongly affected by ground ... El-Amir Muhammad’s minaret in Akhmim, Sohag, Egypt, is constructed of limestone and has been exposed to many factors of damage as a result of the high levels of ground water. Limestone is strongly affected by ground water, especially when being impure. The current work discusses the results of analytical techniques including chemical testing to determine the types of soluble salts through optical microscopy, electronic scanning electron microscope with an X-ray energy dispersion system (ESEM) to study and determine the causes of rapid degradation. Microbial weathering phenomena toward limestone were also studied. Different bacteria and fungi were isolated from outdoors and indoors of air and limestone of the building of which Bacillus cereus OK447647, B. subtilis OK447648, Serratia marcescens OK447650, Pseudomonasoryzihabitans OK447649, Aspergillus flavus, A. niger, Penicillium chrysogenum and Cladosporium cladosporoids were the most representative. B. cereus OK447647 and B. subtilis OK447648 have shown ability for calcium carbonate dissolving. The minimal inhibitory concentrations (MICs) of sodium azide were investigated against the growth of microbial isolates. Sodium azide at 100 ppm was found to be the best treatment for bacterial isolates although it had no significant effect against fungi. 展开更多
关键词 El-Amir Muhammad’s Minaret LIMESTONE XRD Microbial Deterioration treatment sodium Azide
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Miramistinum and metronidazole in the local treatment of the experimental purulent wounds
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作者 Alexandr I.Bezhin Boris S.Sukovatykh +5 位作者 Tatyana A.Pankrusheva Arsen Y.Grigoryan Lyudmila V.Zhilyaeva Elena V.Kobzareva Ekaterina S.Mishina Mariya A.Zatolokina 《哈尔滨医科大学学报》 CAS 2017年第3期285-288,F0003,共5页
Objective To study the wound-healting ability of immobilized forms of miramistinum and metronidazole,based on a sodium salt of carboxymethylcellulose.Methods The research was made on an experimental model of a purulen... Objective To study the wound-healting ability of immobilized forms of miramistinum and metronidazole,based on a sodium salt of carboxymethylcellulose.Methods The research was made on an experimental model of a purulent wound and levomecol was used for comparison.Results During the experiment antimicrobial activity of made drugs was evaluated and the planimetric assessment of the process of epithelialization of the wound’s surface,bacterial load,morphometric examination of histological drugs for wounds and were made.ConclusionThe benefits of combination miramistinum and metronidazole,immobilized on a sodium salt of carboxymethylcellulose,compared with the drug levomecol. 展开更多
关键词 眼科病房 眼病患者 智能型药品集纳盒 可行性研究
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SA-PQ-11/CF阳极提高MFC废水处理效果与发电性能
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作者 樊立萍 温越霄 《精细化工》 EI CAS CSCD 北大核心 2024年第5期1101-1107,共7页
为提高微生物燃料电池(MFC)的废水处理效果和发电性能,制备了一种海藻酸钠(SA)-聚季铵盐-11(PQ-11)/碳毡(CF)阳极(SA-PQ-11/CF),分别以制药废水和糖蜜废水为阳极液,以CF为阴极,构建了MFC系统,采用SEM对阳极表面形貌进行了表征,通过循环... 为提高微生物燃料电池(MFC)的废水处理效果和发电性能,制备了一种海藻酸钠(SA)-聚季铵盐-11(PQ-11)/碳毡(CF)阳极(SA-PQ-11/CF),分别以制药废水和糖蜜废水为阳极液,以CF为阴极,构建了MFC系统,采用SEM对阳极表面形貌进行了表征,通过循环伏安(CV)特性和电化学阻抗(EIS)特性、化学需氧量(COD)去除率对其性能进行了考察。结果表明,SA-PQ-11/CF阳极具有较大的比表面积,MFC的溶液电阻和电荷转移电阻得到明显降低。阳极液为制药废水时,采用SA-PQ-11/CF阳极的MFC的稳态输出电压和COD去除率分别约为0.22 V和62%,较常规CF阳极的MFC分别提高了100%和130%;阳极液为糖蜜废水时,采用SA-PQ-11/CF阳极的MFC的稳态输出电压和COD去除率分别为0.15 V和43%,分别较采用常规CF阳极的MFC提高了275%和95%。 展开更多
关键词 微生物燃料电池 废水处理 阳极改性 海藻酸钠 聚季铵盐-11 发电性能
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左西孟旦联合沙库巴曲缬沙坦钠治疗扩张型心肌病并心力衰竭的临床疗效 被引量:1
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作者 杨志超 王琦 +2 位作者 曹俊达 张文强 邹家旺 《临床合理用药杂志》 2024年第3期1-4,共4页
目的观察左西孟旦联合沙库巴曲缬沙坦钠治疗扩张型心肌病(DCM)并心力衰竭的临床疗效。方法回顾性选取2020年1月—2022年6月于九江市第一人民医院心血管内科住院的71例DCM并心力衰竭患者为研究对象,根据治疗方法分为A组23例、B组23例和C... 目的观察左西孟旦联合沙库巴曲缬沙坦钠治疗扩张型心肌病(DCM)并心力衰竭的临床疗效。方法回顾性选取2020年1月—2022年6月于九江市第一人民医院心血管内科住院的71例DCM并心力衰竭患者为研究对象,根据治疗方法分为A组23例、B组23例和C组25例。A组患者予以常规治疗,B组患者在A组基础上加用沙库巴曲缬沙坦钠片,C组患者在B组基础上联用左西孟旦注射液。3组疗程均为1个月。比较3组临床疗效,治疗前及治疗1个月后6 min步行距离、心功能指标(每搏输出量、左心室舒张末期内径、左心室射血分数)、N末端脑钠肽前体(NT-proBNP)水平。结果治疗1月后,A、B、C组治疗总有效率分别为60.87%、56.52%、92.00%,C组总有效率高于A、B组(χ2/P=6.572/0.010、8.042/0.005)。治疗1个月后,3组6 min步行距离均较治疗前延长,且C组长于A、B组,B组长于A组(P<0.05);3组每搏输出量、左心室射血分数高于治疗前,左心室舒张末期内径小于治疗前,且C组优于A、B组,B组优于A组(P<0.05);3组血清NT-proBNP水平低于治疗前,且C组低于A、B组,B组低于A组(P<0.05)。结论左西孟旦联合沙库巴曲缬沙坦钠治疗DCM并心力衰竭可增强疗效,明显降低血清NT-proBNP水平,减轻心肌损伤,极大程度地提高心功能,增强运动耐量。 展开更多
关键词 扩张型心肌病 心力衰竭 左西孟旦 沙库巴曲缬沙坦钠 治疗结果
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组成对钠铝硅玻璃中钇锆酸盐纳米晶析晶性能的影响
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作者 田英良 韩金龙 +4 位作者 徐博 温玉琳 李培浩 何峰 赵志永 《硅酸盐通报》 CAS 北大核心 2024年第2期710-718,共9页
基于含Y2O_(3)和ZrO_(2)的钠铝硅玻璃体系,研究了玻璃组分中Al_(2)O_(3)/Na2O摩尔比值(MAN)与SiO_(2)/Al_(2)O_(3)摩尔比值(MSA)对玻璃析晶性能的影响。研究结果表明,当MAN<1时,玻璃经热处理后表面析出钠霞石晶体;当MAN≥1时,玻璃热... 基于含Y2O_(3)和ZrO_(2)的钠铝硅玻璃体系,研究了玻璃组分中Al_(2)O_(3)/Na2O摩尔比值(MAN)与SiO_(2)/Al_(2)O_(3)摩尔比值(MSA)对玻璃析晶性能的影响。研究结果表明,当MAN<1时,玻璃经热处理后表面析出钠霞石晶体;当MAN≥1时,玻璃热处理后析出钇锆酸盐纳米晶体,且此时微晶玻璃仍然具有不小于90%的高可见光透过率。对于固定MAN的玻璃,调整其MSA也能实现钇锆酸盐纳米晶的析出,且析出晶体尺寸随MSA增加而减小。随着热处理温度升高微晶玻璃样品中纳米晶体尺寸增大,维氏硬度也增大。 展开更多
关键词 钠铝硅玻璃 析晶行为 热处理 钇锆酸盐纳米晶 透明微晶玻璃 维氏硬度
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封闭处理对超声波辅助制备的锌系磷化膜耐蚀性的影响
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作者 贾春燕 刘海涛 《电镀与精饰》 CAS 北大核心 2024年第9期48-55,共8页
在Q345钢磷化过程中引入超声波以改善锌系磷化膜表面平整度和致密性,为进一步提高超声波辅助制备的锌系磷化膜耐蚀性,分别采用油性封闭剂、硝酸铈溶液、硅酸钠溶液进行封闭处理。结果表明:硅酸钠溶液的封闭效果好于油性封闭剂和硝酸铈溶... 在Q345钢磷化过程中引入超声波以改善锌系磷化膜表面平整度和致密性,为进一步提高超声波辅助制备的锌系磷化膜耐蚀性,分别采用油性封闭剂、硝酸铈溶液、硅酸钠溶液进行封闭处理。结果表明:硅酸钠溶液的封闭效果好于油性封闭剂和硝酸铈溶液,封闭后超声锌系磷化膜的物相组成为Zn_(3)(PO_(4))_(2)·4H_(2)O、Zn_(2)Fe(PO_(4))_(2)·4H_(2)O、ZnSiO_(3)和Na_(2)Si O_(3),并且呈现良好的致密性和耐蚀性,其耐硫酸铜点滴时间超过150 s,腐蚀电流密度低至3.20×10^(-6)A/cm^(2),较未封闭超声锌系磷化膜的腐蚀电流密度降低幅度接近一个数量级。在硅酸钠溶液封闭过程中发生腐蚀整平现象,同时生成ZnSiO_(3)并析出Na_(2)Si O_(3)起到填补孔隙的作用,使超声锌系磷化膜的致密性得到更大程度改善,从而显著增强抗腐蚀能力。 展开更多
关键词 锌系磷化膜 超声波 封闭处理 耐蚀性 硝酸铈溶液 硅酸钠溶液
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左甲状腺素钠治疗老年甲状腺功能减退症患者的临床研究 被引量:2
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作者 张方方 厉艳萍 《临床医学工程》 2024年第2期199-200,共2页
目的探讨左甲状腺素钠治疗老年甲状腺功能减退症(甲减)患者的临床效果及对其甲状腺激素水平、脂代谢的影响。方法60例老年甲减患者随机分为两组,对照组给予甲状腺片治疗,观察组给予左甲状腺素钠片治疗,比较两组的治疗效果以及甲状腺激... 目的探讨左甲状腺素钠治疗老年甲状腺功能减退症(甲减)患者的临床效果及对其甲状腺激素水平、脂代谢的影响。方法60例老年甲减患者随机分为两组,对照组给予甲状腺片治疗,观察组给予左甲状腺素钠片治疗,比较两组的治疗效果以及甲状腺激素、脂代谢指标水平。结果观察组的治疗总有效率为93.33%,显著高于对照组的70.00%(P<0.05)。治疗6周后,观察组的TSH水平显著低于对照组,FT_(3)、FT_(4)水平均显著高于对照组,CHO、TG水平均显著低于对照组(P<0.05)。结论左甲状腺素钠治疗老年甲减患者的效果显著,可明显改善患者的甲状腺功能,调节患者的脂代谢水平。 展开更多
关键词 左甲状腺素钠 甲状腺功能减退症 治疗效果 甲状腺激素 脂代谢
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根管治疗中次氯酸钠意外事件1例
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作者 路瑶 卢志山 +3 位作者 刘程 郭佳欣 吕晨炜 姚丽萍 《实用口腔医学杂志》 CAS CSCD 北大核心 2024年第5期723-725,共3页
次氯酸钠(NaClO)在根管治疗过程中通过根尖孔或破损根管壁溢出,进入软组织的情况比较罕见。文章报道1例根管治疗中出现的NaClO溢出事件。通过文献回顾,对这类病例症状、治疗方法、预防措施进行分析讨论,为临床诊疗提供依据。
关键词 根管治疗 次氯酸钠意外事件 瘀斑
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磷酸肌酸钠联合处理用于腔镜下心内直视手术心肌保护的临床研究
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作者 吴丽灵 张武 +6 位作者 李贻霞 杨凯 梁结连 杜楚川 文先杰 胡旭东 钟执文 《国际医药卫生导报》 2024年第10期1652-1658,共7页
目的探讨磷酸肌酸钠(CP)联合处理对腔镜下心内直视手术患者的心肌缺血再灌注(I/R)损伤的影响。方法选择2022年1月至2023年4月在佛山市第二人民医院和暨南大学附属华侨医院就诊并计划在体外循环下行腔镜二尖瓣置换术或整形术的患者36例,... 目的探讨磷酸肌酸钠(CP)联合处理对腔镜下心内直视手术患者的心肌缺血再灌注(I/R)损伤的影响。方法选择2022年1月至2023年4月在佛山市第二人民医院和暨南大学附属华侨医院就诊并计划在体外循环下行腔镜二尖瓣置换术或整形术的患者36例,采用随机数字表法,将患者分为预处理组、后处理组和联合处理组,每组12例。预处理组男8例,女4例;年龄(58.33±12.35)岁;心功能分级:Ⅲ级8例,Ⅳ级4例。后处理组男5例,女7例;年龄(59.67±13.77)岁;心功能分级:Ⅲ级7例,Ⅳ级5例。联合处理组男7例,女5例;年龄(59.92±11.29)岁;心功能分级:Ⅲ级9例,Ⅳ级3例。患者在全身麻醉和体外循环下行腔镜二尖瓣整形术或置换术。预处理组:体外循环开始前静脉注射CP 2.0 g,停搏液中加入CP 2.0 g;后处理组:主动脉开放后5 min体外循环机内注入CP 2.0 g,体外循环停止前体外循环机内注入CP 2.0 g;联合处理组:体外循环开始前静脉注射CP 1.0 g,停搏液中加入CP 1.0 g,主动脉开放后5 min体外循环机内注入CP 1.0 g,体外循环停止前体外循环机内注入CP 1.0 g。比较3组患者体外循环时间、主动脉阻断时间、体外循环辅助时间、心脏自动复跳情况以及术后多巴胺和肾上腺素的使用情况;比较3组患者术前、术毕、术后1 d和术后2 d的血肌酸激酶同工酶(CK-MB)、心肌肌钙蛋白I(cTnI)以及脑利钠肽(BNP)水平。采用F检验、LSD检验、χ^(2)检验、Fisher确切概率法、秩和检验。结果联合处理组术后48 h肾上腺素的使用比例(1/12)少于预处理组(6/12)和后处理组(5/12),差异有统计学意义(P<0.05)。联合处理组术毕的CK-MB水平[(12.14±4.98)U/L]低于预处理组[(17.51±5.14)U/L],差异有统计学意义(P<0.05);联合处理组术后1 d、术后2 d的CK-MB水平[(27.17±11.25)U/L、(17.10±8.27)U/L]均低于预处理组[(37.58±11.15)U/L、(26.46±8.98)U/L]和后处理组[(39.54±14.27)U/L、(24.28±7.07)U/L],差异均有统计学意义(均P<0.05)。联合处理组术毕的cTnI水平[(4.65±1.07)μg/L]低于预处理组[(5.86±0.99)μg/L],差异有统计学意义(P<0.05);联合处理组术后1 d、术后2 d的cTnI水平[(6.54±0.86)μg/L、(6.24±1.10)μg/L]均低于预处理组[(8.02±1.04)μg/L、(7.22±1.07)μg/L]和后处理组[(9.01±0.87)μg/L、(7.45±1.08)μg/L],差异均有统计学意义(均P<0.05)。联合处理组术后1 d的BNP水平[(168.64±20.19)ng/L]低于预处理组[(185.65±25.13)ng/L],差异有统计学意义(P<0.05);联合处理组术后2 d的BNP水平[(134.77±22.14)ng/L]均低于预处理组[(169.33±26.07)ng/L]和后处理组[(157.10±28.16)ng/L],差异均有统计学意义(均P<0.05)。结论与CP预处理或后处理比较,CP联合处理更能有效地减轻腔镜下心内直视手术心肌I/R损伤,改善心功能。 展开更多
关键词 心肌缺血再灌注损伤 磷酸肌酸钠 预处理 后处理 联合处理 腔镜心脏手术
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