The interfacial status of the steel-aluminum solid to liquid bonding plates (their steel plate surfaces were or were not immersed in flux aqueous solution) were measured by using SEM (Scanning Electron Microscope) and...The interfacial status of the steel-aluminum solid to liquid bonding plates (their steel plate surfaces were or were not immersed in flux aqueous solution) were measured by using SEM (Scanning Electron Microscope) and X-ray diffraction . The results showed that the layer of flux (the minimum thickness was 15 μm on the steel plate surface) could protect the steel plate surface from oxidizing effectively at high temperature in solid to liquid bonding. The melt temperatUre of the flux should be lower than 580 ℃ so that it could be melted and removed completely. No. 1 flux (patent product made by the author) made up of halogeindes could also force liquid aluminum to infiltrate into steel plate surface and thus the interfacial shear strength of the bonding plate was rather large.展开更多
Soil dissolved organic matter (DOM) consists of many organic compounds and plays an important role in contaminant transport in the ecosystem. However, the effects of different extraction conditions on contents of di...Soil dissolved organic matter (DOM) consists of many organic compounds and plays an important role in contaminant transport in the ecosystem. However, the effects of different extraction conditions on contents of different DOM components are poorly understood. We extracted DOM from three soils using different extraction times, solid to liquid ratios (SLR), and extraction solution (KC1) concentrations, and evaluated the extractions using three-dimensional excitation-emission matrix (EEM) fluorescence spectroscopy. The sum of the contents of the main DOM components (protein-, fulvic-, and humic-like compounds) increased by 0.6-3.5, 2.5-3.9, and 0.11 0.37 times (P 〈 0.05) when SLR decreased from 1:2 to 1:10, the extraction solution concentration increased from 0.01 to 1.5 mol L-1, and extraction time increased from 10 to 300 rain, respectively. The three-dimensional EEM fluorescence spectroscopy is a useful tool to characterize the components of DOM and evaluate DOM extraction in soils.展开更多
文摘The interfacial status of the steel-aluminum solid to liquid bonding plates (their steel plate surfaces were or were not immersed in flux aqueous solution) were measured by using SEM (Scanning Electron Microscope) and X-ray diffraction . The results showed that the layer of flux (the minimum thickness was 15 μm on the steel plate surface) could protect the steel plate surface from oxidizing effectively at high temperature in solid to liquid bonding. The melt temperatUre of the flux should be lower than 580 ℃ so that it could be melted and removed completely. No. 1 flux (patent product made by the author) made up of halogeindes could also force liquid aluminum to infiltrate into steel plate surface and thus the interfacial shear strength of the bonding plate was rather large.
基金the financial support of the Special Environmental Research Fund for Public Welfare of the State Environmental Protection Administration of China (No.201309035)the Natural Science Foundation of China (No.51408587)
文摘Soil dissolved organic matter (DOM) consists of many organic compounds and plays an important role in contaminant transport in the ecosystem. However, the effects of different extraction conditions on contents of different DOM components are poorly understood. We extracted DOM from three soils using different extraction times, solid to liquid ratios (SLR), and extraction solution (KC1) concentrations, and evaluated the extractions using three-dimensional excitation-emission matrix (EEM) fluorescence spectroscopy. The sum of the contents of the main DOM components (protein-, fulvic-, and humic-like compounds) increased by 0.6-3.5, 2.5-3.9, and 0.11 0.37 times (P 〈 0.05) when SLR decreased from 1:2 to 1:10, the extraction solution concentration increased from 0.01 to 1.5 mol L-1, and extraction time increased from 10 to 300 rain, respectively. The three-dimensional EEM fluorescence spectroscopy is a useful tool to characterize the components of DOM and evaluate DOM extraction in soils.