The protective chromium coating was prepared on P110 steel by employing pack cementation.The corrosion behaviors of P110 steel and the obtained coating in CO2-saturated simulated oilfield brine were studied by static ...The protective chromium coating was prepared on P110 steel by employing pack cementation.The corrosion behaviors of P110 steel and the obtained coating in CO2-saturated simulated oilfield brine were studied by static complete immersion tests and electrochemical measurements.The corrosion attacks of the samples were determined by mass loss,corroded surface morphologies,corrosion products,and results of electrochemical measurements.The experimental results showed that the coating was uniform,continuous and compact.The chromium coating was slightly corroded,and the mass loss and corrosion rate of the coating were far lower than those of P110 steel.Chromium coating has higher self-corroding potential and lower corrosion current density than P110 steel in accordance with the electrochemical tests results.Taken as a whole,chromizing treatment has significantly improved the corrosion resistance of P110 steel.展开更多
In order to improve the surface performance and increase the lifetime of P 110 oil casing tube steel during operation, electroless plating was conducted to form Ni-P coating onto its surface. The surface morphology/el...In order to improve the surface performance and increase the lifetime of P 110 oil casing tube steel during operation, electroless plating was conducted to form Ni-P coating onto its surface. The surface morphology/element distribution and phase constitution of the Ni-P coating were analyzed using scanning electron microscope (SEM) equipped with energy dispersive spectrometry (EDS) and X-ray diffraction (XRD). Tribological and electrochemical measurement tests were applied to investigate the wear and corrosion resistance of P110 steel and the Ni-P coating. The results showed that a uniform and compact, high phosphorous Ni-P coating was formed. The obtained Ni-P coating indicated certain friction-reduction effect and lower mass loss during friction-wear tests. The Ni-P coating also exhibited higher corrosion resistance in comparison with bared P 110 steel. The obtained N i-P coating has significantly improved the surface performance of P110 steel.展开更多
In order to obtain a high-performance surface on P110 steel that can meet the requirements in oil/gas field environment, the chromium coatings were fabricated by pack cementation. The chromium coatings differed in wit...In order to obtain a high-performance surface on P110 steel that can meet the requirements in oil/gas field environment, the chromium coatings were fabricated by pack cementation. The chromium coatings differed in with/without the addition of La2O3. Scanning electron microscope (SEM), energy dispersive X-ray spectrometer (EDS), X-ray diffractometer (XRD) and microhardness tester were employed to investigate the surface morphologies, surface element distributions, microstructures, phase constitutions and microhardness of the coatings. Friction-wear tests of the P110 steel substrate and the coatings were conducted in air at ambient temperature and humidity. The results show that 'uniform and continuous coatings are formed on P110 steel regardless of adding La2O3 or not. The chromium coatings consist of Cr23C6, Cr7C3, and (Cr, Fe)7C3. The La2O3-added chromium coating is more beneficial in terms of surface morphology, microstructure, thickness and microharduess as compared with the coating without adding La2O3. Chromizing treatment significantly improves the surface hardness and wear resistance of the P110 steel. The wear resistance of the tested samples can be sorted in the following sequence: La2O3-coating 〉 no RE-coating 〉bare P110 steel.展开更多
A series of rare earth (RE) dispersed chromizing coatings were produced on P 110 steel by pack cementation. The orthogonal array design (OAD)was applied to set the experiments. An artificial neural network (ANN)...A series of rare earth (RE) dispersed chromizing coatings were produced on P 110 steel by pack cementation. The orthogonal array design (OAD)was applied to set the experiments. An artificial neural network (ANN) approach is employed to predict the thickness values of the obtained chromizing coatings based on the OAD tests results. The results revealed that the built model was reliable, the thickness values of chromizing coatings were well predicted at selected process parameters, and the predicted error lied in rational range.展开更多
基金Funded by the Science and Technology Programs for Research and Development of Shaanxi Province (No.2008K01-31)
文摘The protective chromium coating was prepared on P110 steel by employing pack cementation.The corrosion behaviors of P110 steel and the obtained coating in CO2-saturated simulated oilfield brine were studied by static complete immersion tests and electrochemical measurements.The corrosion attacks of the samples were determined by mass loss,corroded surface morphologies,corrosion products,and results of electrochemical measurements.The experimental results showed that the coating was uniform,continuous and compact.The chromium coating was slightly corroded,and the mass loss and corrosion rate of the coating were far lower than those of P110 steel.Chromium coating has higher self-corroding potential and lower corrosion current density than P110 steel in accordance with the electrochemical tests results.Taken as a whole,chromizing treatment has significantly improved the corrosion resistance of P110 steel.
基金Funded by the China Postdoctoral Science Foundation(No.2012M520604)the Natural Science Foundation for Young Scientists of Shanxi Province(No.2013021013-2)
文摘In order to improve the surface performance and increase the lifetime of P 110 oil casing tube steel during operation, electroless plating was conducted to form Ni-P coating onto its surface. The surface morphology/element distribution and phase constitution of the Ni-P coating were analyzed using scanning electron microscope (SEM) equipped with energy dispersive spectrometry (EDS) and X-ray diffraction (XRD). Tribological and electrochemical measurement tests were applied to investigate the wear and corrosion resistance of P110 steel and the Ni-P coating. The results showed that a uniform and compact, high phosphorous Ni-P coating was formed. The obtained Ni-P coating indicated certain friction-reduction effect and lower mass loss during friction-wear tests. The Ni-P coating also exhibited higher corrosion resistance in comparison with bared P 110 steel. The obtained N i-P coating has significantly improved the surface performance of P110 steel.
基金Project(2007CB607603) supported by the National Basic Research Program of China
文摘In order to obtain a high-performance surface on P110 steel that can meet the requirements in oil/gas field environment, the chromium coatings were fabricated by pack cementation. The chromium coatings differed in with/without the addition of La2O3. Scanning electron microscope (SEM), energy dispersive X-ray spectrometer (EDS), X-ray diffractometer (XRD) and microhardness tester were employed to investigate the surface morphologies, surface element distributions, microstructures, phase constitutions and microhardness of the coatings. Friction-wear tests of the P110 steel substrate and the coatings were conducted in air at ambient temperature and humidity. The results show that 'uniform and continuous coatings are formed on P110 steel regardless of adding La2O3 or not. The chromium coatings consist of Cr23C6, Cr7C3, and (Cr, Fe)7C3. The La2O3-added chromium coating is more beneficial in terms of surface morphology, microstructure, thickness and microharduess as compared with the coating without adding La2O3. Chromizing treatment significantly improves the surface hardness and wear resistance of the P110 steel. The wear resistance of the tested samples can be sorted in the following sequence: La2O3-coating 〉 no RE-coating 〉bare P110 steel.
基金Funded by the National Natural Science Foundation of China(No.51171125)the China Postdoctoral Science Foundation (No.2012M520604)+1 种基金the Youth Foundation of Taiyuan University of Technology (No.2012L050)the Foundation for Talents Introduction of Taiyuan University of Technology
文摘A series of rare earth (RE) dispersed chromizing coatings were produced on P 110 steel by pack cementation. The orthogonal array design (OAD)was applied to set the experiments. An artificial neural network (ANN) approach is employed to predict the thickness values of the obtained chromizing coatings based on the OAD tests results. The results revealed that the built model was reliable, the thickness values of chromizing coatings were well predicted at selected process parameters, and the predicted error lied in rational range.