The effects of glass flit on the sintering and electric properties of PMN-PT textured ceramics were investigated. The glass frits, including PbO, Bi2O3 and ZnO, were selected since liquid phase sintering lowered the P...The effects of glass flit on the sintering and electric properties of PMN-PT textured ceramics were investigated. The glass frits, including PbO, Bi2O3 and ZnO, were selected since liquid phase sintering lowered the PMN-PT sintering temperature. The piezoelectric properties of PMN-PT ceramics with glass frit addition are strongly dependent on the densification. The addition of glass frits into PMN-PT matrix reduced the sintering temperature to 1 100℃ instead of 1 150 ℃ for samples without glass. The piezoelectric coefficients (d33) of PMN-PT textured ceramics achieved 568 pc/N with 1 wt% excess PbO.展开更多
Transparent Al_(2)O_(3) ceramics with grains aligned to the c-axis were prepared by adding platelets with a low aspect ratio into fine equiaxed particles.The mixed powders were formed into green bodies using spontaneo...Transparent Al_(2)O_(3) ceramics with grains aligned to the c-axis were prepared by adding platelets with a low aspect ratio into fine equiaxed particles.The mixed powders were formed into green bodies using spontaneous coagulation casting and sintered by pressureless sintering and hot-isostatic pressure sintering.Zeta potentials and rheological behavior of the slurries,relative densities of green bodies,and orientation and optical properties of sintered bodies were investigated and discussed.The platelet with a high aspect ratio suppressed densification more seriously during sintering than the one with a low aspect ratio.An excellent oriented structure was obtained when 5 wt%platelets with a low aspect ratio were added,and transparent Al_(2)O_(3) ceramics with grains aligned to c-axis were successfully prepared;the in-line transmittance was 78.4%at 600 nm,which is the highest one in the currently reported literature.展开更多
基金Supported by the National Natural Science Foundation of China (No.50502027)the 973 Project (No. 2002CB613303)
文摘The effects of glass flit on the sintering and electric properties of PMN-PT textured ceramics were investigated. The glass frits, including PbO, Bi2O3 and ZnO, were selected since liquid phase sintering lowered the PMN-PT sintering temperature. The piezoelectric properties of PMN-PT ceramics with glass frit addition are strongly dependent on the densification. The addition of glass frits into PMN-PT matrix reduced the sintering temperature to 1 100℃ instead of 1 150 ℃ for samples without glass. The piezoelectric coefficients (d33) of PMN-PT textured ceramics achieved 568 pc/N with 1 wt% excess PbO.
基金This work was supported by the National Natural Science Foundation of China(Nos.51772309 and 52130207).The authors thank Prof.Jing WANG(Dalian University of Technology)for the synthesis of Al2O3 platelets.
文摘Transparent Al_(2)O_(3) ceramics with grains aligned to the c-axis were prepared by adding platelets with a low aspect ratio into fine equiaxed particles.The mixed powders were formed into green bodies using spontaneous coagulation casting and sintered by pressureless sintering and hot-isostatic pressure sintering.Zeta potentials and rheological behavior of the slurries,relative densities of green bodies,and orientation and optical properties of sintered bodies were investigated and discussed.The platelet with a high aspect ratio suppressed densification more seriously during sintering than the one with a low aspect ratio.An excellent oriented structure was obtained when 5 wt%platelets with a low aspect ratio were added,and transparent Al_(2)O_(3) ceramics with grains aligned to c-axis were successfully prepared;the in-line transmittance was 78.4%at 600 nm,which is the highest one in the currently reported literature.