Influence of strain rate on grain refinement and texture evolution under complex shear stress conditions

The effects of different complex shear stress conditions on grain refinement and texture evolution of Mg-13Gd-4Y-2Zn-0.5Zr alloy were investigated.With increasing strain rate,the average grain size of compression-shear(CS)and compression-torsion(CT)samples are decreased,and the grain size of dynamic recrystallization(DRX)grains is also decreased.This is because that the precipitation number ofβphases is increased,and the hindering effect on grain growth can be significantly enhanced.The DRX fractions of CS and CT samples are decreased with increased strain rate.The low DRX fraction at high strain rate is related to the insufficient time for grains to nucleate.The DRX process can be promoted by the PSN mechanism of second phases,and the grain growth can be restricted by the pinning effect.At the same time,the texture strength is enhanced as the strain rate increased.Besides,the kinking degree of lamellar long-period stacking ordered(LPSO)phases is increased.Under complex shear stress conditions,non-basal slip,especially pyramidal slip,is easily activated and the texture is deflected greatly.Compared with the CS samples,CT samples have smaller average grain size,higher DRX fraction,and lower texture strength for a certain strain rate.This is because that the equivalent stress of the CT sample is larger,the stress triaxiality is smaller,so more serious dislocations are piled up near grain boundaries and second phases.At the same time,since CT sample was sheared with torsion,the dislocation movement path can be called“rotational dislocation accumulation”,and the longer distribution path of the CT sample is generated,so more sub-grains and low-angle grain boundaries(LAGBs)are formed.Compared with the CS sample,more huge-angle grain boundaries(HAGBs)and DRX grains are formed from grain boundary to grain interior,so better grain refinement effect is achieved.

Deformation mechanism of cold ring rolling in view of texture evolution predicted by a newly proposed polycrystal plasticity model

An explicit polycrystal plasticity model was proposed to investigate the deformation mechanism of cold ring rolling in view of texture evolution. The model was created by deducing a set of linear incremental controlling equations within the framework of crystal plasticity theory. It was directly solved by a linear algorithm within a two-level procedure so that its efficiency and stability were guaranteed. A subroutine VUMAT for ABAQUS/Explicit was developed to combine this model with the 3D FE model of cold ring rolling. Results indicate that the model is reliable in predictions of stress-strain response and texture evolution in the dynamic complicated forming process; the shear strain in RD of the ring is the critical deformation mode according to the sharp Goss component （{110}？100？） of deformed ring; texture and crystallographic structure of the ring blank do not affect texture type of the deformed ring;texture evolves rapidly at the later stage of rolling, which results in a dramatically increasing deformation of the ring.

Texture evolution and recrystallization behaviors of Cu-Ag alloys subjected to cryogenic rolling

The texture evolution and mechanical properties of Cu-Ag alloys subjected to severe plastic deformation at cryogenic temperature（CT） were investigated and the sequent annealing behaviors were also studied.Compared with the sheets rolled at room temperature（RT） showing copper texture,the CT-rolled sheets exhibited brass texture which indicated that cross-slip was suppressed at CT,and both the ultimate tensile strength and yield strength of the sheets were increased.Due to the in-situ recrystallization mechanism,recrystallization textures in as-annealed CT-rolled sheets were randomly distributed,while the as-annealed RT-rolled sheets mainly contained cube texture.Microstructures of the rolled and annealed sheets were observed using optical microscopy and electronic back-scatter diffraction.The results show that the dynamic recovery was suppressed during CT-rolling and resulted in higher deformation energy storage.Therefore,the recrystallization of CT-rolled sheets could start at a lower temperature than that of RT-rolled sheet at the same reduction.

Microstructure and texture evolution of AZ31 magnesium alloy during large strain hot rolling

Commercial AZ31 magnesium alloy sheets were rolled by nearly 70% thickness reduction in one rolling pass at 823 K. The results show that ultrafine grains are distributed in both shear bands and surfaces of the rolled sheets. The grain size of the refined grain in the shear bands is 0.4-1 μm. The outstanding grain refinement is attained by dynamic recrystallization due to flow localization. The texture in middle layer of the sheet is basal texture with little change in intensity throughout the rolling process, while the texture on surface becomes a double-peak texture with basal poles splitting in the transverse direction（TD）. The relative intensity of the double-peak texture is 26.6, which is quite higher than that of the texture in the middle layer. The inhomogeneous strain distribution is responsible for the exceptional grain refinement and texture evolution.

Effect of Cu on microstructure,mechanical properties,and texture evolution of ZK60 alloy fabricated by hot extrusion−shearing process

As-cast Mg-6Zn-xCu-0.6Zr(x=0,0.5,1.0,wt.%)alloys were fabricated by permanent mold casting;then,the alloys were subjected to homogenization heat treatment and extrusion-shearing(ES)process.The microstructure and mechanical properties of the alloys were evaluated by OM,SEM/EDS,XRD,TEM,EBSD and tensile tests.The results show that the hard MgZnCu phase in Cu-added alloy can strengthen particle-stimulated nucleation(PSN)effect and hinder the migration of dynamic recrystallization(DRX)grain boundary at an elevated temperature during ES.The ZK60+0.5Cu alloy shows an optimal tensile strength–ductility combination(UTS of 396 MPa,YS of 313 MPa,andδ=20.3%)owing to strong grain boundary strengthening and improvement of Schmid factor for{0001}■basal slip.The aggregation of microvoids around the MgZnCu phase mainly accounts for the lower tensile elongation of ZK60+1.0Cu alloy compared with ZK60 alloy.

Quasi-in-situ investigation into the microstructure and texture evolution of pure magnesium during friction stir welding

The quasi-in-situ microstructure and texture evolution along the real flow path of pure magnesium during friction stir welding were investigated.Five representative stages were involved from the base metal to the formation of the final stir zone.The material experienced compression,preheating,acceleration,deceleration,and subsequent annealing over the course of the welding process.A highly concentrated(0001)texture,denoted as''orientation convergence^,was initiated at the beginning of the acceleration stage(shearing deformation zone)in front of the tool.Both continuous and discontinuous dynamic recrystallization occurred simultaneously in the stir zone,and continuous dynamic recrystallization was determined to be the primary recrystallization mechanism.The marker material morphology and EBSD data were used to elucidate the in-situ evolution of the shear direction and shear plane along with the real flow path.

Phase-field study of the second phase particle effect on texture evolution of polycrystalline material

The second phase particle effect on texture evolution of polycrystalline material is studied through phase-field method. A unique field variable is introduced into the phase-field model to represent the second phase particles. Elastic interaction between particles and grains is also considered. Results indicate that in the presence of second phase particles the average particle diameter turns smaller than in the absence of these particles and retards texture formation by pinning effect. The second phase particles change the strain energy profile, which tremendously influences the pinning effect.

Texture evolution during semicontinuous equal-channel angular extrusion process of interstitial-free steel

Semicontinuous equal-channel angular extrusion（ SC-ECAE） is a novel severe plastic deformation technique that has been developed to produce ultrafine-grain steels. Instead of external forces being exerted on specimens in the conventional ECAE,driving forces are applied to dies in SC-EACE. The deformation of interstitial-free（ IF） steel w as performed at room temperature,and individual specimens w ere repeatedly processed at various passes. An overall grain size of 0. 55 μm w as achieved after 10 passes. During SC-ECAE,the main textures of IF steel included { 111} ,{ 110} ,{ 112} ,{ 110} ,and { 110} At an early stage,increasing dislocations induce new textures and increase intensity. When the deformation continues,low-angle boundaries are formed betw een dislocation cell bands,w hich cause some dislocation cell bands to change their orientation,and therefore,the intensity of the textures begins to decrease. After more passes,the intensity of textures continues to decrease w ith high-angle boundaries,and the sub-grains in dislocation cell bands continuously increase. The present study reports the evolution of textures during deformation; these w ere examined and characterized using high-resolution electron backscattered diffraction（ EBSD） in a field emission scanning electron microscope. The mechanisms of texture evolution are discussed.

Texture evolution behavior and anisotropy of 2A97 Al-Li alloy during recrystallization at elevated temperature

2A97 Al-Li alloy was cold-rolled to 2 mm and then thermally exposed at different temperatures for 1 h and at 723 K for different time,respectively.The texture evolution behavior and the anisotropy of 2A97 Al-Li alloy were investigated.The result shows that the{001}<120>and{011}<233>textures are the dominant recrystallization texture.The{124}<211>texture is the final recrystallization texture.In case of low-temperature thermal exposure(473,573 K),the{011}<211>texture is aggregated to the{112}<111>and{123}<634>textures.During the recrystallization at 723 K,the{001}<110>,{111}<112>and{011}<100>textures are the intermediate transition grain orientations.The concurrent precipitation of Al_(20)Cu_(2)Mn_(3)and Al_(3)Zr results in the occurrence of unusually sharp{011}<233>and{001}<120>texture components during recrystallization.The alloy with both recrystallization and deformation texture possesses the smallest anisotropic,and the texture is the direct reason that results in the anisotropy.

Texture evolution prediction of 2219 aluminum alloy sheet under hydro-bulging using cross-scale numerical modeling

A simultaneous prediction of macroscopic deformation and microstructure evolution is critical for un-derstanding the deformation mechanism of components.In this work,the hydro-bulging process of 2219 aluminum alloy sheet was investigated using cross-scale numerical modeling,in which the macroscopic finite element method(FEM)and crystal plasticity finite element method(CPFEM)were combined.The calculated texture evolution exhibits good agreement with the experimental results,and the stress er-ror between the two scales is generally small.The effects of different strain states on texture evolution and slip mode are further discussed.As the strain ratioηincreases,the volume fractions of the initial Rotated Copper texture component andγ-Fiber texture component decrease significantly,which tend to be stabilized at P texture component.The initial Rotated Cube texture component is inclined to rotate towards the Cube texture component,while the volume fraction of this orientation is relatively stable.The lower strain ratio can considerably enhance the activity of more equivalent slip systems,promoting a more uniform strain distribution over grains.The difficulty of grain deformation changes as the lat-tice rotates.The grain with easy-to-deform orientation can gradually rotate to a stable orientation during plastic deformation,which has a lower Schmid factor.

Influence of Hot-Rolling Deformation on Microstructure,Crystalline Orientation,and Texture Evolution of the Ti6Al4V-5Cu Alloy

The influence of hot-deformation on the microstructure,crystalline orientation,and texture evolution of Ti6Al4V-5Cu,an antibacterial(α+β)titanium alloy,was investigated.The alloy was deformed using a hot rolling process in 15%,58%,and 73%thickness reduction ratios.It was found that the basal<α→>and pyramidal<c→+α→>type slip planes could be activated in theαphase,which dominated the deformation behavior of Ti6Al4V-5Cu alloy.Under various deformation conditions,the alloy revealed different microstructure features.On the 15%hot rolled alloy,the deformation was performed by the breakdown of priorβgrain boundaries(GBβ),which was attributed to the formation of coarseαgrains,rotated nearly 45°with respect to the transversal and rolling directions.The presence of different sub-structure geometries made the interior grain size distribution heterogeneous.On the 58%hot rolled alloy,Ti2Cu intermetallic compound was found at theα/βinterface.High-resolution transmission electron microscopy investigation showed the occurrence of grain rotation in different crystallographic directions.At room temperature,the percentage elongation(El)of the alloy reached 23.15%on the 58%hot rolled sample.On the 73%deformed alloy,refined and randomly oriented characteristics of grains were obtained due to higher thickness reduction,which resulted from the segregation of very fine granules.The influence of grain rotation during a hot rolling process revealed that theα/βtexture fiber separation angle to maintain the Burger orientation relationship of{0001}α//{110}βplanes decreased with increase of the thickness reduction ratio when Ti6Al4V-5Cu alloy was deformed by a hot rolling mechanism.Activation of tensile{1012}<1011>and compressive{1122}<1123>twins on the deformation of the alloy was also studied.

Microstructure,texture evolution and mechanical properties of cold rolled Ti-32.5Nb-6.8Zr-2.7Sn biomedical beta titanium alloy

Ti-32.5 Nb-6.8 Zr-2.7 Sn（TNZS,wt%） alloy was produced by using vacuum arc melting method,followed by solution treatment and cold rolling with the area reductions of 50% and 90%.The effects of cold rolling on the microstructure,texture evolution and mechanical properties of the experimental alloy were investigated by optical microscopy,X-ray diffraction,transmission electron microscopy and universal material testing machine.The results showed that the grains of the alloy were elongated along rolling direction and stress-induced α＇＇ martensite was not detected in the deformed samples.The plastic deformation mechanisms of the alloy were related to {112} 111 type deformation twinning and dislocation slipping.Meanwhile,the transition from γ-fiber texture to α-fiber texture took place during cold rolling and a dominant {001} 110α-fiber texture was obtained after 90% cold deformation.With the increase of cold deformation degree,the strength increased owing to the increase of microstrain,dislocation density and grain refinement,and the elastic modulus decreased owing to the increase of dislocation density as well as an enhanced intensity of {001} 110α-fiber texture and a weakened intensity of {111} 112γ-fiber texture.The 90% cold rolled alloy exhibited a great potential to become a new candidate for biomedical applications,since it possesses low elastic modulus（47.1 GPa）,moderate strength（883 MPa） and high elastic admissible strain（1.87%）,which are superior than those of Ti-6 Al-4 V alloy.

Microstructure and texture evolution of TB8 titanium alloys during hot compression

In this study, microstructure and texture evolution of TB8 titanium alloys during hot deformation were investigated by using electron back-scattered diffraction(EBSD) analysis. The results showed that dynamic recrystallization(DRX) behavior of TB8 titanium alloys was drastically sensitive to the strain. As the true strain raised from 0.2 to 0.8, the degree of DRX gradually increased. The nucleation mechanism of recrystallization was observed, including discontinuous dynamic recrystallization(DDRX) resulting from the bulging of original boundaries. Furthermore, continuous dynamic recrystallization(CDRX) occurred because of the transformation of low-angle grain boundaries(LAGBs) to high-angle grain boundaries(HAGBs) in the interior of the original deformed grains. The texture evolution of TB8 titanium alloy during hot deformation process was analyzed in detail, and five texture components were observed,including{001}h100 i,{011}h100 i,{112}h110 i,{111}h110 i, and {111}h112 i. As the true strain increased,deformation textures were gradually weakened due to an increase in the volume fraction of DRX grains. When the true strain was 0.8, the main texture components consisted of the recrystallization texture components of the{001}h100 i and {011}h100 i textures.

Effect of normalization on texture evolution of 0.2-mm-thick thingauge non-oriented electrical steels with strong η-fiber textures

Thin-gauge non-oriented electrical steel sheets of 0.2 mm in thickness with high magnetic induction and low core loss were produced by a two-stage cold-rolling method with and without normalization annealing.The through-process texture evolutions of the two processes were compared and studied by means of X-ray diffractometer and electron backscattered diffraction.Results showed that excellent magnetic properties were attributed to strong η-fiber recrystallization texture in the final sheet.Coarse γ-fiber-oriented grains after intermediate annealing and medium cold-rolling reduction were considered key factors to obtain a strong γ-fiber texture given that a large number of shear bands within the γ-fiber deformed matrix provided dominant nucleation sites for η-fiber-oriented grains.The normalization annealing after hot rolling was favorable for the retention of cube texture,thereby decreasing the magnetic anisotropy of thin-gauge non-oriented electrical steels.

Microstructure and texture evolution of the β-Mg17A12 phase in a Mg alloy with an ultra-high Al content

In the present study,the effects of equal channel angular pressing(ECAP)on the microstructure and mechanical property of the Mg-20Al alloy were systematically investigated.For the first time,the texture of Mg17Al12 phase and its evolution with ECAP conditions were reported.The results show that increasing the processing temperature and passes generates more uniform distribution and finer size ofβ-Mg17Al12 phases.The large pieces ofβ-Mg17A12 phases are composed of many fine grains with different crystallographic orientations.For theβ-Mg17A12 phase,a preferred distribution of(001)appears at 523 K and 573 K,and hardly varies with temperature.Nevertheless,a random texture is observed at 623 K.The(0002)poles exhibit a preferred distribution at 473 K,but this preferred distribution varies with temperature.A random distribution of(0002)poles is observed when processed at 623 K.Many types of crystallographic planar relationship betweenβ-Mg17A12 phase andα-Mg matrix are observed and the relationships of{11-23}//{100}or{110}or{111}and{1-211}//{100}or//{110}or{111}have a relatively higher frequency than others.The texture ofα-Mg matrix is much different from that of the ECAPed Mg alloys with a relative low Al content,in which a texture with basal poles inclining approximately 45°away from the extrusion direction often develops.The mechanical properties of Mg-20Al alloy are closely related to the temperature and passes of ECAP.A higher temperature often decreases the yield strength,but hardly alters the maximum strength.There is a low plasticity for all the samples and increasing processing temperature slightly enhances the plasticity.The corresponding mechanisms were deeply discussed.

Effect of cooling rate followingβforging on texture evolution and variant selection duringβ→αtransformation in Ti-55511 alloy

The control of the post-forging cooling rate has been a key issue in the industrial production process of titanium alloys. We investigated texture evolution and variant selection(VS) during β → α transformation through high-temperature compression experiments followed by quantitative control of varying cooling rates. Results show that post-forging cooling rates affect β grains, α variants, and α/β textures. The αprecipitation inhibits motions of β static recrystallization(β_(SRX)) grain boundaries and thus leads to grain refining from 0.1 ℃/s to 0.05 ℃/s. Further analysis reveals that lamellae grain boundary widmanstattenα(α_(WGB)) keeps growing rapidly within β-grain in an interface instability manner at 0.1–0.05 ℃/s. Most of α-phase with 50°–60°/<-12–10> is preferentially precipitated at β-medium angle GBs between 30°and 45° and strictly follows BOR with the side of of adjacent β-grain with the same or similar {110} or{111}. Moreover, the texture type transforms gradually from RGoss {110} <1–10> to Brass {110} <1–12>from 25 ℃/s to 1 ℃/s. βgrains exhibit(102) [-201] texture, while the corresponding α has textures of<0001>//Z and <11–20>//Y from 1 ℃/s to 0.05 ℃/s. Our findings lay a profound theoretical foundation in microstructure evolution of near-β titanium alloy for industrial production.

Texture evolution and slip mode of a Ti-5.5Mo-7.2Al-4.5Zr-2.6Sn-2.1Cr dual-phase alloy during cold rolling based on multiscale crystal plasticity finite element model

The complex micromechanical response among grains remains a persistent challenge to understand the deformation mechanism of titanium alloys during cold rolling.Therefore,in this work,a multiscale crystal plasticity finite element method of dual-phase alloy was proposed and secondarily developed based on LS-DYNA software.Afterward,the texture evolution and slip mode of a Ti-5.5Mo-7.2Al-4.5Zr-2.6Sn-2.1Cr alloy,based on the realistic 3D microstructure,during cold rolling(20%thickness reduction)were systematically investigated.The relative activity of the■slip system in theαphase gradually increased,and then served as the main slip mode at lower Schmid factor(<0.2).In contrast,the contribution of the■slip system to the overall plastic deformation was relatively limited.For theβphase,the relative activity of the<111>{110}slip system showed an upward tendency,indicating the important role of the critical resolved shear stress relationship in the relative activity evolutions.Furthermore,the abnormally high strain of very fewβgrains was found,which was attributed to their severe rotations compelled by the neighboring pre-deformedαgrains.The calculated pole figures,rotation axes,and compelled rotation behavior exhibited good agreement to the experimental results.

Microstructure,Mechanical Properties and Texture Evolution of Mg-Al-Zn-La-Gd-Y Magnesium Alloy by Hot Extrusion and Multi-Pass Rolling

A high-ductility Mg-8.10Al-0.42Zn-0.51Mn-1.52La-1.10Gd-0.86 Y(wt%)alloy was developed by hot extrusion and multi-rolling processes.Relationships between microstructure,mechanical properties and texture evolution of the extruded and rolled alloy were investigated.The rolling process had significant effect on grain refinement of the extruded plate.The grain size reduced from 12.3 to 4.9μm with the increasing rolling pass.With the increase in rolling pass,the proportion of dynamic recrystallized(DRXed)grains increases due to particle-stimulated nucleation,grain boundary nucleation and twin induced nucleation.In the process of multiple rolling,the basal pole gradually tilted from normal direction to transverse direction due to the asymmetric deformation and irregular grain deformation,resulting in the weakening of the base texture.The results showed that grain refinement and texture weakening were the main reasons for the good ductility of the alloy.

Tensile deformation of fine-grained Mg at 4K,78K and 298K

The impact of grain size, ranging from 0.9 μm to 9 μm, on the mechanical properties of commercially pure Mg is investigated at temperatures of 4K, 78K, and 298K. The mechanisms governing plastic flow are influenced by both grain size and temperature. At 4K and 78K, dominant deformation modes in Mg involve dislocation glide and extension twinning, regardless of grain size. The interactions between basal and non-basal dislocations and dislocations with grain boundaries promote an unusually high rate of work hardening in the plastic regime, leading to premature failure. The yield stress follows the Hall-Petch relationship σy~ k/√d, with the slope k increasing with decreasing temperature. At 298K, in addition to dislocation glide and twinning, grain boundary sliding(GBS) becomes significant in samples with grain sizes below 3 μm, considerably enhancing the material's deformability. GBS activation provides an additional recovery mechanism for dislocations accumulating at grain boundaries, facilitating their absorption during sliding and rotation. Analysis of σ Θ relationship suggests that the basal slip is the dominant dislocation mode in Mg at 298K. Decreasing grain size suppresses dislocation activity and twinning and increases GBS, resulting in lower Θ and σ Θ values. Suppressing conventional deformation modes coupled with enhanced GBS yields stress softening, breaking down the Hall-Petch relationship in Mg below 3 μm grain size, leading to an inverse Hall-Petch behaviour. The work reports new data on the strength, ductility, work hardening and fracture behaviour, and their variations with Mg grain size across different temperature regimes.

Effects of deformation parameters on microstructure and texture of Mg−Zn−Ce alloy

Compression tests were performed on the Mg−6Zn−0.5Ce(wt.%)alloy using a Gleeble−1500 thermomechanical simulator testing system at temperatures of 250,300,350℃ and strain rates of 0.001,0.01,0.1 s^−1.The microstructure and texture evolution of the Mg−6Zn−0.5Ce alloy during hot compression were investigated by optical microscopy(OM)and electron backscattered diffraction(EBSD).The results showed that Zener−Hollomon parameters obtained from the deformation processes had a significant effect on the dynamic recrystallization and texture of the Mg−6Zn−0.5Ce alloy.The fraction of undynamically recrystallized(unDRXed)regions increased,and the dynamically recrystallized(DRXed)grain size decreased with increasing the Zener−Hollomon parameters.The texture intensity of the DRXed regions was weaker compared with that in the unDRXed regions,which resulted in a sharper texture intensity in the samples deformed with higher Zener−Hollomon parameters.The increase in recrystallized texture intensity was related to preferred grain growth.