For samples in the gaseous state at room temperature and ambient pressure,mature technology has been developed to encapsulate them in a diamond anvil cell(DAC).However,the large volume press(LVP)can only treat samples...For samples in the gaseous state at room temperature and ambient pressure,mature technology has been developed to encapsulate them in a diamond anvil cell(DAC).However,the large volume press(LVP)can only treat samples with starting materials in solid or liquid form.We have achieved stable encapsulation and reaction treatment of carbon dioxide in a centimeter sized sample chamber for a long time(over 10 min)under conditions of temperature higher than 1200C and pressure over 5 GPa through the use of integrated low-temperature freezing and rapid compression sealing method for LVP cell assemblies.This technology can also be applied to the packaging of other gaseous or liquid samples,such as ammonia,sulfur dioxide,water,etc.in LVP devices.展开更多
The aim of this study is to design special blends of oils with a balance between the major fatty acid groups {(saturated (SFA): monounsaturated (MUFA): polyunsaturated (PUFA) SMP} and, at the same time, with a desirab...The aim of this study is to design special blends of oils with a balance between the major fatty acid groups {(saturated (SFA): monounsaturated (MUFA): polyunsaturated (PUFA) SMP} and, at the same time, with a desirable balanced ratio between the essential fatty acids (omega-6/omega-3). The encapsulation techniques were used to protect these balanced omega oils from oxidative deterioration and to enhance their bioaccessibility. The efficiency of whey protein concentrates incorporation with various wall materials in the microcapsules by spray or freeze-drying methods was evaluated in terms of stability of internally trapped oil against oxidative degradation. An ultrasonic or microfluidizer was used to prepare nanoemulsions, which were then dried by freeze drying or spray drying to produce microcapsule powder in order to minimize lipid oxidation Whey protein concentrate was combined with maltodextrin and Arabic gum at 8:2:1 ratio. Particle size, zeta potential, emulsion stability, and oxidative stability were evaluated in the feed emulsions used in particle manufacturing. In addition, the encapsulation efficiency and in-vitro digestion and morphology of encapsulated powder were assessed. The highest level of encapsulation efficiency was achieved using a microfluidizer and drying with a spray dryer, these powders also showed the highest emulsion and oxidative stability;microfluidized powders dried with a freeze drier had the lowest encapsulation effectiveness. Some health benefits (particularly for maintaining human health and preventing or reducing certain diseases) are expected to come from consuming fatty foods that contain balanced fatty acids as well as a certain ratio of omega-6 and omega-3 fatty acids.展开更多
基金supported by the National Key R&D Program of China(Grant No.2023YFA1406200).
文摘For samples in the gaseous state at room temperature and ambient pressure,mature technology has been developed to encapsulate them in a diamond anvil cell(DAC).However,the large volume press(LVP)can only treat samples with starting materials in solid or liquid form.We have achieved stable encapsulation and reaction treatment of carbon dioxide in a centimeter sized sample chamber for a long time(over 10 min)under conditions of temperature higher than 1200C and pressure over 5 GPa through the use of integrated low-temperature freezing and rapid compression sealing method for LVP cell assemblies.This technology can also be applied to the packaging of other gaseous or liquid samples,such as ammonia,sulfur dioxide,water,etc.in LVP devices.
基金Scientific and Technological Research Council of Turkey(TUITAK),program 2221Also,the authors express their gratitude ITMO Fellowship and Professorship Program(Micro fellowship).
文摘The aim of this study is to design special blends of oils with a balance between the major fatty acid groups {(saturated (SFA): monounsaturated (MUFA): polyunsaturated (PUFA) SMP} and, at the same time, with a desirable balanced ratio between the essential fatty acids (omega-6/omega-3). The encapsulation techniques were used to protect these balanced omega oils from oxidative deterioration and to enhance their bioaccessibility. The efficiency of whey protein concentrates incorporation with various wall materials in the microcapsules by spray or freeze-drying methods was evaluated in terms of stability of internally trapped oil against oxidative degradation. An ultrasonic or microfluidizer was used to prepare nanoemulsions, which were then dried by freeze drying or spray drying to produce microcapsule powder in order to minimize lipid oxidation Whey protein concentrate was combined with maltodextrin and Arabic gum at 8:2:1 ratio. Particle size, zeta potential, emulsion stability, and oxidative stability were evaluated in the feed emulsions used in particle manufacturing. In addition, the encapsulation efficiency and in-vitro digestion and morphology of encapsulated powder were assessed. The highest level of encapsulation efficiency was achieved using a microfluidizer and drying with a spray dryer, these powders also showed the highest emulsion and oxidative stability;microfluidized powders dried with a freeze drier had the lowest encapsulation effectiveness. Some health benefits (particularly for maintaining human health and preventing or reducing certain diseases) are expected to come from consuming fatty foods that contain balanced fatty acids as well as a certain ratio of omega-6 and omega-3 fatty acids.