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Hollow cerium nanoparticles synthesized by one-step method for multienzyme activity to reduce colitis in mice
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作者 Lin Mi Kai Zhang +3 位作者 Jian-Xia Ma Jian-Feng Yao Yi-Li Tong Zhi-Jun Bao 《World Journal of Gastroenterology》 2025年第5期94-104,共11页
BACKGROUND Inflammatory bowel disease(IBD)is a common chronic intestinal inflammatory disease.High oxidative stress is a treatment target for IBD.Cerium oxide(CeO2)nanomaterials as nanozymes with antioxidant activity ... BACKGROUND Inflammatory bowel disease(IBD)is a common chronic intestinal inflammatory disease.High oxidative stress is a treatment target for IBD.Cerium oxide(CeO2)nanomaterials as nanozymes with antioxidant activity are potential drugs for the treatment of colitis.AIM To synthesize hollow cerium(H-CeO2)nanoparticles by one-step method and to validate the therapeutic efficacy of H-CeO2 in IBD.METHODS H-CeO2 was synthesized by one-step method and examined its characterization and nanoenzymatic activity.Subsequently,we constructed dextran sulfate so-dium(DSS)-induced colitis in mice to observe the effects of H-CeO2 on colonic inflammation.The effects of H-CeO2 on colon inflammation and reactive oxygen species(ROS)levels in IBD mice were detected by hematoxylin and eosin staining and dichlorofluorescein diacetate staining,respectively.Finally,the biological sa-fety of H-CeO2 on mice was evaluated by hematoxylin and eosin staining,blood routine,and blood biochemistry.RESULTS H-CeO2 nanoparticles prepared by the one-step method were uniform,monodi-sperse and hollow.H-CeO2 had a good ability to scavenge ROS,∙OH and∙OOH.H-CeO2 reduced DSS-induced decreases in body weight and colon length,colonic epithelial damage,inflammatory infiltration,and ROS accumulation.H-CeO2 administration reduced the disease activity index of DSS-induced animals from about 8 to 5.H-CeO2 had no significant effect on body weight,total platelet count,hemoglobin,white blood cell,and red blood cell counts in healthy mice.No significant damage to major organs was observed in healthy mice following H-CeO2 administration.CONCLUSION The one-step synthesis of H-CeO2 nanomaterials had good antioxidant activity,biosafety,and inhibited deve-lopment of DSS-induced IBD in mice by scavenging ROS. 展开更多
关键词 Inflammatory bowel disease Nanozymes Hollow cerium nanoparticles one-step method Cerium oxide biosafety
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Efficient Preparation and Electrochemical Properties of BiOCl/Graphite by One-step Solvothermal Method
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作者 门丽娟 FEI Chi +3 位作者 LIU An 陈春钰 ZHOU Jiankang JU Dianchun 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS CSCD 2024年第3期651-657,共7页
We used the surface-pretreated graphite paper(Gp)as a carrier and loaded BiOCl with high selectivity to Cl^(-)on its surface by solvothermal method to form BiOCl@Gp electrode.The morphology,structure,and composition o... We used the surface-pretreated graphite paper(Gp)as a carrier and loaded BiOCl with high selectivity to Cl^(-)on its surface by solvothermal method to form BiOCl@Gp electrode.The morphology,structure,and composition of the materials were characterized by scanning electron microscopy and nitrogen adsorption/desorption,and the results showed that the spherical BiOCl particles were uniformly dispersed on the surface of the Gp,forming a mesoporous BiOCl@Gp composite with a specific surface area of 22.82 m^(2)/g and a pore volume of 0.043 cm3/g.Furthermore,cyclic voltammetry and electrochemical impedance spectroscopy were used to test the electrochemical properties of the composites,and the stability of BiOCl and the high conductivity of Gp were synergistic,the BiOCl@Gp exhibited a specific capacitance of 30.2 F·g^(-1) at a current density of 0.5 A·g^(-1),and the selectivity of the BiOCl@Gp materials for Cl^(-)was significantly higher than that of SO_(4)^(2-),NO_(2)^(-),and HCO_(3)^(-).Therefore,BiOCl@Gp composite electrode materials can be used for the selective adsorption of Cl^(-)in wastewater,in order to achieve efficient wastewater recycling. 展开更多
关键词 solvothermal method bismuth oxychloride ELECTROCHEMISTRY electrode materials
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Determination of the flooding zone during a dam break in a channel with a bend in the presence of several obstacles by the VOF method
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作者 Alibek ISSAKHOV Zhansaya RAKHYMZHANOVA Aizhan ABYLKASSYMOVA 《Journal of Mountain Science》 SCIE CSCD 2024年第11期3754-3766,共13页
This paper aims to investigate a dam break in a channel with a bend in the presence of several obstacles.To accurately determine the flood zones,it is necessary to take into account many factors such as terrain,reserv... This paper aims to investigate a dam break in a channel with a bend in the presence of several obstacles.To accurately determine the flood zones,it is necessary to take into account many factors such as terrain,reservoir volume.Numerical modeling was used to determine the flood zone.Numerical modeling based on the Navier-Stokes equations with a turbulent k-epsilon RNG model,the Volume of Fluid(VOF)method and the PISO algorithm were used to analyze the flow in a bend channel at an angle of 10 with the obstacles.To verify the numerical model,a test on dam break in the 450 channel was conducted.The simulation results were compared with experimental data and with the numerical data of existing data.Having been convinced of the correctness of the mathematical model,the authors carried out a numerical simulation of the main problem in three versions:without barriers,with one obstacle,with two obstacles.According to the obtained numerical results,it can be noted that irregular landforms held the flow,a decrease in water level and a slower time for water emergence could be seen.Thus,the water flow without an obstacle,with one obstacle and with two obstacles showed 4.2 s,4.4 s and 4.6 s of the time of water appearance,respectively.This time shift can give a certain advantage when conducting various events to evacuate people. 展开更多
关键词 Vof method PISO algorithm Dam break Navier-Stokes equation
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Numerical Investigations on the Resonance Errors of Multiscale Discontinuous Galerkin Methods for One-Dimensional Stationary Schrödinger Equation
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作者 Bo Dong Wei Wang 《Communications on Applied Mathematics and Computation》 EI 2024年第1期311-324,共14页
In this paper,numerical experiments are carried out to investigate the impact of penalty parameters in the numerical traces on the resonance errors of high-order multiscale discontinuous Galerkin(DG)methods(Dong et al... In this paper,numerical experiments are carried out to investigate the impact of penalty parameters in the numerical traces on the resonance errors of high-order multiscale discontinuous Galerkin(DG)methods(Dong et al.in J Sci Comput 66:321–345,2016;Dong and Wang in J Comput Appl Math 380:1–11,2020)for a one-dimensional stationary Schrödinger equation.Previous work showed that penalty parameters were required to be positive in error analysis,but the methods with zero penalty parameters worked fine in numerical simulations on coarse meshes.In this work,by performing extensive numerical experiments,we discover that zero penalty parameters lead to resonance errors in the multiscale DG methods,and taking positive penalty parameters can effectively reduce resonance errors and make the matrix in the global linear system have better condition numbers. 展开更多
关键词 Discontinuous Galerkin(DG)method Multiscale method Resonance errors one-dimensional Schrödinger equation
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Prediction of the Photofading of Selected Derivatives of 5-(4-X-Phenylazo)-3-Cyano-1-(H or Ethyl)-6-Hydroxy-4-Methyl-2-Pyridone: Theoretical Studies, Comparison of AM1 and PM3 Methods
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作者 Krzysztof Wojciechowski Lucjan Szuster 《Computational Chemistry》 CAS 2024年第2期25-56,共32页
We analysed the photooxidation reaction in the electro-(1O2) and nucleophilic (O2•−) reaction of 2-pyridone azo derivatives. First, we calculated the energy (enthalpies) of tautomers formation, which is a measure of d... We analysed the photooxidation reaction in the electro-(1O2) and nucleophilic (O2•−) reaction of 2-pyridone azo derivatives. First, we calculated the energy (enthalpies) of tautomers formation, which is a measure of durability and the probability of their formation. We performed the light fastness calculations of the monoazopyridone dyes. Using the semi-empirical methods of quantum chemistry AM1 and PM3, the reactivity indicators of superdelocalisability (SrE(N)) and the electron density distribution in ground state on the highest occupied HOMO orbital and the lowest unoccupied excited state LUMO in 2-pyridone phenylazo derivatives were calculated. Superdelocalisability coefficients enable the stability to oxidising agents of various chemical molecules depending on the tautomeric forms in which they may occur. The results of the electron density calculations at the HOMO and LUMO boundary orbitals allow to determine the tendency to electrophilic attack with singlet oxygen 1O2 or nucleophilic attack of the superoxide anion O2•−on a specific atom in the molecule. The structure of the dyes was optimised with MM+, MD and AM1 or PM3 until a constant energy value was achieved with a convergence criterion of 0.01 kcal/mol. 展开更多
关键词 Photochemical Degradation AM1 and PM3 methods Boundary Orbitals Electron Densities Electrophilic and Nucleophilic Reaction HOMO and LUMO Orbitals
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The forecasting efficiency under different selected regions by Pattern Informatics Method and seismic potential estimation in the North-South Seismic Zone
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作者 Weixi Tian Yongxian Zhang 《Earthquake Science》 2024年第4期368-382,共15页
In 2022,four earthquakes with M_(S)≥6.0 including the Menyuan M_(S)6.9 and Luding M_(S)6.8 earthquakes occurred in the North-South Seismic Zone(NSSZ),which demonstrated high and strong seismicity.Pattern Informatics(... In 2022,four earthquakes with M_(S)≥6.0 including the Menyuan M_(S)6.9 and Luding M_(S)6.8 earthquakes occurred in the North-South Seismic Zone(NSSZ),which demonstrated high and strong seismicity.Pattern Informatics(PI)method,as an effective long and medium term earthquake forecasting method,has been applied to the strong earthquake forecasting in Chinese mainland and results have shown the positive performance.The earthquake catalog with magnitude above M_(S)3.0 since 1970 provided by China Earthquake Networks Center was employed in this study and the Receiver Operating Characteristic(ROC)method was applied to test the forecasting efficiency of the PI method in each selected region related to the North-South Seismic Zone systematically.Based on this,we selected the area with the best ROC testing result and analyzed the evolution process of the PI hotspot map reflecting the small seismic activity pattern prior to the Menyuan M_(S)6.9 and Luding M_(S)6.8 earthquakes.A“forward”forecast for the area was carried out to assess seismic risk.The study shows the following.1)PI forecasting has higher forecasting efficiency in the selected study region where the difference of seismicity in any place of the region is smaller.2)In areas with smaller differences of seismicity,the activity pattern of small earthquakes prior to the Menyuan M_(S)6.9 and Luding M_(S)6.8 earthquakes can be obtained by analyzing the spatio-temporal evolution process of the PI hotspot map.3)The hotspot evolution in and around the southern Tazang fault in the study area is similar to that prior to the strong earthquakes,which suggests the possible seismic hazard in the future.This study could provide some ideas to the seismic hazard assessment in other regions with high seismicity,such as Japan,Californi,Turkey,and Indonesia. 展开更多
关键词 Luding M_(S)6.8 and Menyuan M_(S)6.9 earthquake Pattern Informatics method North-South Seismic Zone earthquake forecasting seismic activity pattern.
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Insight Into the Separation-of-Variable Methods for the Closed-Form Solutions of Free Vibration of Rectangular Thin Plates
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作者 Yufeng Xing Ye Yuan Gen Li 《Computer Modeling in Engineering & Sciences》 SCIE EI 2025年第1期329-355,共27页
The separation-of-variable(SOV)methods,such as the improved SOV method,the variational SOV method,and the extended SOV method,have been proposed by the present authors and coworkers to obtain the closed-form analytica... The separation-of-variable(SOV)methods,such as the improved SOV method,the variational SOV method,and the extended SOV method,have been proposed by the present authors and coworkers to obtain the closed-form analytical solutions for free vibration and eigenbuckling of rectangular plates and circular cylindrical shells.By taking the free vibration of rectangular thin plates as an example,this work presents the theoretical framework of the SOV methods in an instructive way,and the bisection–based solution procedures for a group of nonlinear eigenvalue equations.Besides,the explicit equations of nodal lines of the SOV methods are presented,and the relations of nodal line patterns and frequency orders are investigated.It is concluded that the highly accurate SOV methods have the same accuracy for all frequencies,the mode shapes about repeated frequencies can also be precisely captured,and the SOV methods do not have the problem of missing roots as well. 展开更多
关键词 Separation-of-variable method Rayleigh quotient nodal line eigenvalue equation bisection method
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Synthesis of Vanadium Nitride by a One Step Method 被引量:6
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作者 Sansan YU Nianxin FU +1 位作者 Feng GAO Zhitong SUI 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2007年第1期43-46,共4页
Vanadium nitrides were prepared via one step method of carbothermal reduction and nitridation of vanadium trioxide. Thermalgravimetric analysis (TGA) and X-ray diffraction were used to determine the reaction paths o... Vanadium nitrides were prepared via one step method of carbothermal reduction and nitridation of vanadium trioxide. Thermalgravimetric analysis (TGA) and X-ray diffraction were used to determine the reaction paths of vanadium carbide, namely the following sequential reaction: V2O3→V8C7 in higher temperature stage, the rule of vanadium nitride synthesized was established, and defined conditions of temperature for the production of the carbides and nitrides were determined. Vanadium oxycarbide may consist in the front process of carbothermal reduction of vanadium trioxide. In one step method for vanadium nitride by carbothermal reduction and nitridation of vanadium trioxide, the nitridation process is simultaneous with the carbothermal reduction. A one-step mechanism of the carbothermal reduction with simultaneous nitridation leaded to a lower terminal temperature in nitridation process for vanadium nitride produced, compared with that of carbothermal reduction process without nitridation. The grain size and shape of vanadium nitride were uniform, and had the shape of a cube. The one step method combined vacuum carborization and nitridation (namely two step method) into one process. It simplified the technological process and decreased the costs. 展开更多
关键词 Vanadium nitride Vanadium trioxide Carbothermal reduction NITRIDATION one step method
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Measurement of mouse liver glutathione S-transferase activity by the integrated method 被引量:10
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作者 廖飞 李甲初 +2 位作者 康格非 曾昭淳 左渝萍 《Journal of Medical Colleges of PLA(China)》 CAS 2003年第5期295-300,共6页
Objective: The integrated method was investigated to measure Vm/Km of mouse liver glutathione S-transfer-ase (GST) activity on GSH and 7-Cl-4-nitrobenzofurazozan. Methods: Presetting concentration of one substrate twe... Objective: The integrated method was investigated to measure Vm/Km of mouse liver glutathione S-transfer-ase (GST) activity on GSH and 7-Cl-4-nitrobenzofurazozan. Methods: Presetting concentration of one substrate twenty-fold above the other's and taking maximum product absorbance Am as parameter while Km as constant, Vm/Km was obtained by nonlinear fitting of GST reaction curve to the integrated Michaelis-Menten equation In [Am/(Am -Ai)] + Ai/ ( ξ× Km ) = ( Vm/Km )×ti (1). Results: Vm/Km for GST showed slight dependence on initial substrate concentration and data range, but it was resistant to background absorbance, error in reaction origin and small deviation in presetting Km. Vm/Km was proportional to the amount of GST with upper limit higher than that by initial rate. There was close correlation between Vm/Km and initial rate of the same GST. Consistent results were obtained by this integrated method and classical initial rate method for the measurement of mouse liver GST. Conclusion: With the concentration of one substrate twenty-fold above the other's, this integrated method was reliable to measure the activity of enzyme on two substrates , and substrate concentration of the lower one close to its apparent Km was able to be used. 展开更多
关键词 integrated method glutathione S-transferase nonlinear fitting reaction curve predictor variable enzyme activity measurement
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Synthesis of Substituted u-Oxo-bis[tetra-phenyl porphyrinatoiron] Compounds from Free Base Porphyrins by a One-pot Method 被引量:2
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作者 佘远斌 冯连顺 +1 位作者 王爱欣 李修艳 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2008年第3期369-372,共4页
A novel method for synthesis of substituted u-oxo-bis[tetraphenyl porphyrinatoiron] compotmds ([TRPPFe]20) based on the reaction among free base porphyrins (TRPPH2), FeSO4·7H2O and H2O in one pot was proposed... A novel method for synthesis of substituted u-oxo-bis[tetraphenyl porphyrinatoiron] compotmds ([TRPPFe]20) based on the reaction among free base porphyrins (TRPPH2), FeSO4·7H2O and H2O in one pot was proposed and investigated. Four kinds of [TRPPFe]2O were synthesized by this novel synthetic method, and their structures were characterized by elemental analysis, infrared spectra and UV-vis spectroscopy. The reaction conditions, including the effect of different iron salts on the formation of [TRPPFe]2O, the reaction time between FeSO4-7H2O and TRPPH2, the molar ratio of FeSO4-7H2O/TRPPH2 as well as the volume ratio of H2O/DMF, were investigated. The [TRPPFe]2O yield of 93% 98% could be obtained under the following optimal conditions: the reaction time of FeSOn-7H2O with TRPPH2 was about 10 h, the molar ratio of FeSOn-7H2O/TRPPH2 about 5 : 1, and the volume ratio of H2O/DMF exceeded 2 : 1. Further research indicated that only TRPPFeCI were formed once FeSOn-7H2O was replaced by FeCl2-4H2O, the reason of which might be that halogen ions in iron salts interfered the formation of [TRPPFe]2O, suggesting that halogen ions should be avoided in this novel synthetic method. 展开更多
关键词 substituted u-oxo-bis[tetraphenylporphyrinatoiron] compounds one-pot method free base porphyrins
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Study of the segmentation of active fault by the boundary element method──analysis of the Xianshuihe fault zone
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作者 张超 陈连旺 +1 位作者 赵国光 贺群禄 《Acta Seismologica Sinica(English Edition)》 CSCD 1994年第2期227-234,共8页
On the basis of the recent geological surveys and the relevant studies of the Xianshuihe fault zone, this paper analyzes the seismogenic mechanism of some faults and characteristic morphology on the fault zone by the ... On the basis of the recent geological surveys and the relevant studies of the Xianshuihe fault zone, this paper analyzes the seismogenic mechanism of some faults and characteristic morphology on the fault zone by the boundary element method and discusses the fault segmentation and the related distribution of the earthquake ruptures. The main conclusions are: For the first order segmentation, the Xianshuihe fault zone can be divided into three major segments (the northwestern Luhuo-Qianning segment, the middle linking fracture region and the southeastern Kangding segment). Among them, the differences are not only in geometry and structure, but also in mechanical property and dynamics. Some of the characteristic morphologies on the Xianshuihe fault zone reflect the effects in cumulative deformation due to long-term fault movement, and reveal the fault segmentation in different orders. Such morphologies control, to some extent, the developments and the distributions of the earthquake ruptures on the fault zone. 展开更多
关键词 boundary element method fault segmentation characteristic morphology Xianshuihe fault zone
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Discrimination between upper versus lower airway components to the rise of total airway resistance measured by Pennock’s method after nasal irritant challenge
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作者 Zuzana Biringerova Silvia Gavliakova +2 位作者 Eva Hanuskova Tomas Buday Jana Plevkova 《Open Journal of Molecular and Integrative Physiology》 2013年第3期104-110,共7页
Terminals of the trigeminal afferents innervating nasal mucosa are called gate keepers, since these fibres detect substances entering the airways. Trigeminal excitation by irritants initiates airway defensive mechanis... Terminals of the trigeminal afferents innervating nasal mucosa are called gate keepers, since these fibres detect substances entering the airways. Trigeminal excitation by irritants initiates airway defensive mechanisms, and it is also attributed to the influence of lower airways resistance in a term of nasobronchial reflex. This phenomenon is frequently under debate, because some investigators were unable to confirm its existence. The aim of our study was to determine, whether pharmacological approach could be useful to reach high accuracy and better interpretation of the data obtained by Pennock’s method. Pennock’s method, which is frequently used to measure airway resistance in vivo (Raw) in fact measures total airway resistance, however, the data are usually interpreted in a terms of bronchomotor response. The upper airway component, which represents approximately 40% of Raw, is commonly not considered as being important in this method. 30 Dunkin Hartley guinea pigs were exposed to nasal stimuli (TRPA1 agonist—irritant allylisothiocyanate (10 mM, AITC), TRPM8 agonist with cooling potential menthol (10-3 M) and saline as a control). Raw was measured pre challenge as baseline, after nasal provocation and further, after nasal inhalation of histamine and methacholine (10-6 M) each. The data showed rise of Raw only after nasal AITC challenge, with further increased responsiveness to histamine and methacholine (5.3 vs 10.18 vs 11.26 vs 17.32 cmH2O.s-1, p 0.05). No significant changes were detected after saline, or menthol respectively. Data obtained in further experiment and its analysis showed that pre-treatment with nasal administration of 1% oxymetazoline but without salbutamol inhalation prevented the rise of Raw after nasal irritant challenges. Raw after nasal irritant challenges rises rather due to nasal response than due to narrowing of the lower airways. 展开更多
关键词 AIRWAYS Resisatnce In Vivo Pennock’s method
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Effect of viscosity on stability and accuracy of the two-component lattice Boltzmann method with a multiple-relaxation-time collision operator investigated by the acoustic attenuation model
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作者 Le Bai Ming-Lei Shan +3 位作者 Yu Yang Na-Na Su Jia-Wen Qian Qing-Bang Han 《Chinese Physics B》 SCIE EI CAS CSCD 2022年第3期364-374,共11页
A two-component lattice Boltzmann method(LBM) with a multiple-relaxation-time(MRT) collision operator is presented to improve the numerical stability of the single relaxation time(SRT) model. The macroscopic and the m... A two-component lattice Boltzmann method(LBM) with a multiple-relaxation-time(MRT) collision operator is presented to improve the numerical stability of the single relaxation time(SRT) model. The macroscopic and the momentum conservation equations can be retrieved through the Chapman–Enskog(C-E) expansion analysis. The equilibrium moment with the diffusion term is calculated, a diffusion phenomenon is simulated by utilizing the developed model, and the numerical stability is verified. Furthermore, the binary mixture channel model is designed to simulate the sound attenuation phenomenon, and the obtained simulation results are found to be consistent with the analytical solutions. The sound attenuation model is used to study the numerical stability and calculation accuracy of the LBM model. The simulation results show the stability and accuracy of the MRT model and the SRT model under different viscosity conditions. Finally,we study the influence of the error between the macroscopic equation of the MRT model and the standard incompressible Navier–Stokes equation on the calculation accuracy of the model to demonstrate the general applicability of the conclusions drawn by the sound attenuation model in the present study. 展开更多
关键词 two-component lattice Boltzmann method acoustic attenuation
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Dark Color ZnO Quasi-One-Dimensional Nanostructures Grown by Hydrothermal Method and Modulation of their Optical Properties
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作者 Hao Chen Na Dong +2 位作者 Kai Wang Yi Yao Faqiang Xu 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2019年第6期708-714,I0003,共8页
Zinc oxide has a large energy gap and thus it has potential application in the field of solar cells by tuning the absorption of sunlight. In order to enhance its absorption of sunlight,dark color zinc oxides have been... Zinc oxide has a large energy gap and thus it has potential application in the field of solar cells by tuning the absorption of sunlight. In order to enhance its absorption of sunlight,dark color zinc oxides have been prepared by traditional hydrothermal method directly using a zinc foil as both source and substrate. We found that we could tune the optical properties of ZnO samples by changing the temperature. In particular, increasing temperature could significantly reduce the reflectivity of solar energy in the visible range. We speculate that the phenomenon is relevant to the sharp cone morphology of the ZnO nanorods grown on the surface of Zn foils, which furthermore enhance refraction and reflection of light in the nanorods. The capacity to improve the light absorption of ZnO may have a bright application in raising the efficiency of solar cells. 展开更多
关键词 Hydrothermal method Dark color ZnO samples Enhanced optical properties
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Optimization of micro milling electrical discharge machining of Inconel 718 by Grey-Taguchi method 被引量:3
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作者 林茂用 曹中丞 +3 位作者 许春耀 邱蕙 黄鹏丞 林裕城 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第3期661-666,共6页
The optimization of micro milling electrical discharge machining(EDM) process parameters of Inconel 718 alloy to achieve multiple performance characteristics such as low electrode wear,high material removal rate and... The optimization of micro milling electrical discharge machining(EDM) process parameters of Inconel 718 alloy to achieve multiple performance characteristics such as low electrode wear,high material removal rate and low working gap was investigated by the Grey-Taguchi method.The influences of peak current,pulse on-time,pulse off-time and spark gap on electrode wear(EW),material removal rate(MRR) and working gap(WG) in the micro milling electrical discharge machining of Inconel 718 were analyzed.The experimental results show that the electrode wear decreases from 5.6×10-9 to 5.2×10-9 mm3/min,the material removal rate increases from 0.47×10-8 to 1.68×10-8 mm3/min,and the working gap decreases from 1.27 to 1.19 μm under optimal micro milling electrical discharge machining process parameters.Hence,it is clearly shown that multiple performance characteristics can be improved by using the Grey-Taguchi method. 展开更多
关键词 Inconel 718 alloy micro milling electrical discharge machining electrode wear material removal rate working gap Grey-Taguchi method
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Performances of fissured red sandstone after thermal treatment with constant-amplitude and low-cycle impacts 被引量:1
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作者 Yongjun Chen Tubing Yin +3 位作者 P.G.Ranjith Xibing Li Qiang Li Dengdeng Zhuang 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第2期561-587,共27页
In the engineering practices,it is increasingly common to encounter fractured rocks perturbed by temperatures and frequent dynamic loads.In this paper,the dynamic behaviors and fracture characteristics of red sandston... In the engineering practices,it is increasingly common to encounter fractured rocks perturbed by temperatures and frequent dynamic loads.In this paper,the dynamic behaviors and fracture characteristics of red sandstone considering temperatures(25℃,200℃,400℃,600℃,and 800℃)and fissure angles(0°,30°,60°,and 90°)were evaluated under constant-amplitude and low-cycle(CALC)impacts actuated by a modified split Hopkinson pressure bar(SHPB)system.Subsequently,fracture morphology and second-order statistics within the grey-level co-occurrence matrix(GLCM)were examined using scanning electron microscopy(SEM).Meanwhile,the deep analysis and discussion of the mechanical response were conducted through the synchronous thermal analyzer(STA)test,numerical simulations,one-dimensional stress wave theory,and material structure.The multiple regression models between response variables and interactive effects of independent variables were established using the response surface method(RSM).The results demonstrate the fatigue strength and life diminish as temperatures rise and increase with increasing fissure angles,while the strain rate exhibits an inverse behavior.Furthermore,the peak stress intensification and strain rate softening observed during CALC impact exhibit greater prominence at increased fissure angles.The failure is dominated by tensile damage with concise evolution paths and intergranular cracks as well as the compressor-crushed zone which may affect the failure mode after 400℃.The second-order statistics of GLCM in SEM images exhibit a considerable dependence on the temperatures.Also,thermal damage dominated by thermal properties controls the material structure and wave impedance and eventually affects the incident wave intensity.The tensile wave reflected from the fissure surface is the inherent mechanism responsible for the angle effect exhibited by the fatigue strength and life.Ultimately,the peak stress intensification and strain rate softening during impact are determined by both the material structure and compaction governed by thermal damage and tensile wave. 展开更多
关键词 Red sandstone Temperature FISSURE Constant-amplitude and low-cycle(CALC) impact Fatigue failure Response surface method(RSM)
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Thermoelectric Properties of n-type Poly(nickel 1,1,2,2-ethenetetrathiolate)Prepared by a New One-step Solvothermal Method
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作者 WANG Yijiang YAO Qin +1 位作者 QU Sanyin CHEN Lidong 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2022年第4期760-764,共5页
Poly(nickel 1,1,2,2-ethenetetrathiolate)(poly[Na_(x)(Ni-ett)])is one of the most promising n-type organic thermoelectric materials which can be used in wearable devices.However,the conventional solution method is time... Poly(nickel 1,1,2,2-ethenetetrathiolate)(poly[Na_(x)(Ni-ett)])is one of the most promising n-type organic thermoelectric materials which can be used in wearable devices.However,the conventional solution method is time-consuming and the prepared poly[Na_(x)(Ni-ett)]usually has poor crystallinity,which does not benefit for achieving high thermoelectric performance.Here,a new one-step solvothermal method under the high reaction temperature and high vapor pressure was developed to prepare poly[Na_(x)(Ni-ett)]with a quite short period.The experimental results show crystallinity and electrical conductivity are greatly enhanced as compared with those prepared by conventional solution method.As a result,a maximum ZT value of 0.04 was achieved at 440 K,which is about four times of the polymer prepared by the conventional solution method.This study may provide a new route to enhance the TE properties of n-type organic thermoelectric materials. 展开更多
关键词 theRMOELECTRIC organic materials n-type poly[Na_(x)(Ni-ett)] solvothermal method
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Cascading multi-segment rupture process of the 2023 Turkish earthquake doublet on a complex fault system revealed by teleseismic P wave back projection method 被引量:1
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作者 Bonan Cao Zengxi Ge 《Earthquake Science》 2024年第2期158-173,共16页
In this study,the vertical components of broadband teleseismic P wave data recorded by China Earthquake Network are used to image the rupture processes of the February 6th,2023 Turkish earthquake doublet via back proj... In this study,the vertical components of broadband teleseismic P wave data recorded by China Earthquake Network are used to image the rupture processes of the February 6th,2023 Turkish earthquake doublet via back projection analysis.Data in two frequency bands(0.5-2 Hz and 1-3 Hz)are used in the imaging processes.The results show that the rupture of the first event extends about 200 km to the northeast and about 150 km to the southwest,lasting~90 s in total.The southwestern rupture is triggered by the northeastern rupture,demonstrating a sequential bidirectional unilateral rupture pattern.The rupture of the second event extends approximately 80 km in both northeast and west directions,lasting~35 s in total and demonstrates a typical bilateral rupture feature.The cascading ruptures on both sides also reflect the occurrence of selective rupture behaviors on bifurcated faults.In addition,we observe super-shear ruptures on certain fault sections with relatively straight fault structures and sparse aftershocks. 展开更多
关键词 2023 Turkish earthquake doublet back projection method cascading segmented rupture process coseismic triggering super-shear ruptures
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Hybrid Strategy of Partitioned and Monolithic Methods for Solving Strongly Coupled Analysis of Inverse and Direct Piezoelectric and Circuit Coupling
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作者 Daisuke Ishihara Syunnosuke Nozaki +1 位作者 Tomoya Niho Naoto Takayama 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第8期1371-1386,共16页
The inverse and direct piezoelectric and circuit coupling are widely observed in advanced electro-mechanical systems such as piezoelectric energy harvesters.Existing strongly coupled analysis methods based on direct n... The inverse and direct piezoelectric and circuit coupling are widely observed in advanced electro-mechanical systems such as piezoelectric energy harvesters.Existing strongly coupled analysis methods based on direct numerical modeling for this phenomenon can be classified into partitioned or monolithic formulations.Each formulation has its advantages and disadvantages,and the choice depends on the characteristics of each coupled problem.This study proposes a new option:a coupled analysis strategy that combines the best features of the existing formulations,namely,the hybrid partitioned-monolithic method.The analysis of inverse piezoelectricity and the monolithic analysis of direct piezoelectric and circuit interaction are strongly coupled using a partitioned iterative hierarchical algorithm.In a typical benchmark problem of a piezoelectric energy harvester,this research compares the results from the proposed method to those from the conventional strongly coupled partitioned iterative method,discussing the accuracy,stability,and computational cost.The proposed hybrid concept is effective for coupled multi-physics problems,including various coupling conditions. 展开更多
关键词 Structure-piezoelectric-circuit interaction energy harvesting partitioned method monolithic method hybrid method
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Study on Extraction of Effective Aroma Components from Formula Tobacco by the Supercritical CO2 Extraction Method and Its Aroma Composition
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作者 Shoujie NIE Guangyu MENG +7 位作者 Shoutao CAO Shuaicheng TIAN Zhiguang LIU Cuishu LENG Guofeng YU Qiulin LIU Xulun WEI Quanjiang DONG 《Agricultural Biotechnology》 CAS 2020年第5期117-119,共3页
[Objectives]This study was conducted to improve the sensory quality and industrial availability of tobacco extracts.[Methods]The L9(34)design was adopted to carried out an extraction experiment,in which formula tobacc... [Objectives]This study was conducted to improve the sensory quality and industrial availability of tobacco extracts.[Methods]The L9(34)design was adopted to carried out an extraction experiment,in which formula tobacco was extracted using supercritical CO2,and the extract was concentrated by vacuum distillation.Through sensory evaluation and chemical analysis,the function determination and chemical composition analysis of the tobacco extracts were carried out,and the optimal supercritical fluid extraction process was finally determined.[Results]The obtained optimal supercritical fluid extraction conditions were as follows:extraction temperature 55℃,extraction pressure 25 MPa,CO2 flow rate of 20 L/h,and entrainer of 95%ethanol.The tobacco extract obtained under the optimal conditions endowed the cigarettes with full and delicate aroma,less irritation and clean aftertaste and made the flavor of the cigarettes overall coordinated and softer,so the sensory quality was significantly improved.[Conclusions]The tobacco extract obtained by the supercritical CO2 extraction method from formula tobacco can effectively improve the quality of cigarettes. 展开更多
关键词 Supercritical extraction method Aroma component Orthogonal test TOBACCO Flavor and fragrance
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