Spectral analysis was a method of identifying substances, determining their chemical composition and calculating their content based on their spectral characteristics. This paper mainly discussed the application of va...Spectral analysis was a method of identifying substances, determining their chemical composition and calculating their content based on their spectral characteristics. This paper mainly discussed the application of various spectroscopic techniques, mainly including atomic absorption spectrometry (AAS) inductively coupled plasma emission spectrometry (ICP-AES) X-ray fluorescence spectroscopy (XRF) atomic fluorescence spectroscopy (AFS) direct reading spectroscopy (OES) glow discharge emission spectroscopy (GD-OSE) laser-induced breakdown spectroscopy (LIBS), in the formulation of non-ferrous metal standards in China. The AAS method was the most widely used single-element microanalysis method among the non-ferrous metal standards. The ICP-AES method was good at significant advantages in the simultaneous detection of multiple elements. The XRF method was increasingly used in the determination of primary and secondary trace elements due to its simple sample preparation and high efficiency. The AFS was mostly detected by single-element trace analysis. OES GD-OES and LIBS were playing an increasingly important role in the new demand area for non-ferrous metals. This paper discussed matrix elimination, sample digestion, sample preparation, instrument categories and other aspects of some standards, and summarized the advantages of spectral analysis and traditional chemical analysis methods. The new methods of future spectroscopic technology had been illustrated in the process of developing non-ferrous metal standards.展开更多
CAS 132-2006 formulation background and work courses
Flat panel display technology is maturing alongside the development of science and technology. The prices of flat panel display TV sets are becoming lower ... CAS 132-2006 formulation background and work courses
Flat panel display technology is maturing alongside the development of science and technology. The prices of flat panel display TV sets are becoming lower and lower. Flat panel display TV sets have begun entering the mainstream and are now the first choice of some consumers when making new TV purchases.Display TV Set Installation Service Point Explanation and AnalysisRepair, Retreat and Change Duty Stipulations. Peculiar use conditions, usage environments, and the practical circumstances of user consumption service requirements, etc., were also taken into account on the basis of extensive investigation, testing, and verification.……展开更多
The fruits of Piper cubeba have been used in Ayurvedic system of medicine for pain,tastelessness, painful urination and mouth diseases. Among its various chemical constituents,（-）-hinokinin, a trypanosomicidal diben...The fruits of Piper cubeba have been used in Ayurvedic system of medicine for pain,tastelessness, painful urination and mouth diseases. Among its various chemical constituents,（-）-hinokinin, a trypanosomicidal dibenzylbutyrolactone lignan, is found in significant quantities.For quality evaluation of P. cubeba fruit and its commercial formulations, there is an urgent need to develop an analytical method based on（-）-hinokinin. For this purpose, an HPLC method was developed using photo diode array detector and Waters HR C18 column with gradient elution consisting of water and acetonitrile. The developed method was validated as per ICH-Q2 B guidelines and found to be accurate, precise and linear over a wide range of concentrations（5–300 mg/m L）.（-）-Hinokinin contents were found to be in the range of 0.005–0.109%（m/m） in various P. cubeba samples. The developed method was extended to LC–MS for further identification and characterization of（-）-hinokinin in samples. The developed method is simple,rapid and specific, and can be used as a tool for quality control of P. cubeba fruits and its commercial formulations.展开更多
Silicon isotope analysis traditionally uses a standard-sample bracketing （SSB） method that relies upon greater instrument stability than can be consistently expected. The following proposed method reduces the level ...Silicon isotope analysis traditionally uses a standard-sample bracketing （SSB） method that relies upon greater instrument stability than can be consistently expected. The following proposed method reduces the level of instrumental stability required for the analysis process and provides a valid solution for high-precision and accurate studies of Si isotopic compositions. Rock samples were dissolved by using alkali fusion and acidification. Silicon isotopes were purified with an ion exchange resin. Interfering peaks for isotopes were separated by using a Nu Plasma 1700 multi-collector inductively coupled plasma mass spectrometry （MS） system in high-resolution mode （M/AM 〉 8000 RP）. Two magnesium isotopes （25Mg and 26Mg） and three silicon isotopes （28Si, 29Si, and 3;Si） were analyzed in the same data collection cycle. Mg isotopes were used as an internal standard to calibrate the mass discrimination effects in MS analysis of Si isotopes in combination with the SSB method in order to reduce the effects of MS interference and instrumental mass dis- crimination on the accuracy of measurements. The conventional SSB method without the Mg internal standard and the proposed SSB method with Mg calibration delivered consistent results within two standard deviations. When Mg was used as an internal standard for calibration, the analysis precision was better than 0.05 %0 amu.展开更多
In this article, we propose a generalized exp(-Φ(ξ))-expansion method and successfully implement it to find exact traveling wave solutions to the fifth order standard Sawada-Kotera (SK) equation. The exact traveling...In this article, we propose a generalized exp(-Φ(ξ))-expansion method and successfully implement it to find exact traveling wave solutions to the fifth order standard Sawada-Kotera (SK) equation. The exact traveling wave solutions are established in the form of trigonometric, hyperbolic, exponential and rational functions with some free parameters. It is shown that this method is standard, effective and easily applicable mathematical tool for solving nonlinear partial differential equations arises in the field of mathematical physics and engineering.展开更多
After a straightforward general relativistic calculation on a modified flat-spacetime metric (developed from the fluctuating vacuum energy interacting with a graviton field), a pair of n-valued covariant and contravar...After a straightforward general relativistic calculation on a modified flat-spacetime metric (developed from the fluctuating vacuum energy interacting with a graviton field), a pair of n-valued covariant and contravariant energy momentum tensors emerged analogous to quantized raising and lower operators. Detaching these operators from the general relativistic field equations, and then transporting them to act on extreme spacetimes, these operators were able to generate fundamental particle boson masses. In particular, the operators precisely generated Higgs mass. Then by applying a consistency approach to the gravitational field equations—similar to how Maxwell applied to the electromagnetic ones—it allowed for the coupling of spin-to-mass, further restricting the particle mass to be in precise agreement with CODATA experimental values. Since this is a massless field approach integrated discretely with a massive one, it overcomes various renormalizing difficulties;moreover it solves the mass hierarchal problem of the Standard Model of particle physics, and generates its spin and therefore shows quantum physics to be a subset of General Relativity, just as Einstein had first imagined.展开更多
This paper reports that low-temperature heat capacities of 4-（2-aminoethyl）-phenol （C8H11NO） are measured by a precision automated adiabatic calorimeter over the temperature range from 78 to 400 K. A polynomial eq...This paper reports that low-temperature heat capacities of 4-（2-aminoethyl）-phenol （C8H11NO） are measured by a precision automated adiabatic calorimeter over the temperature range from 78 to 400 K. A polynomial equation of heat capacities as a function of the temperature was fitted by the least square method. Based on the fitted polynomial, the smoothed heat capacities and thermodynamic functions of the compound relative to the standard reference temperature 298.15K were calculated and tabulated at the interval of 5K. The energy equivalent, εcalor, of the oxygen-bomb combustion calorimeter has been determined from 0.68g of NIST 39i benzoic acid to be εcalor=（14674.69±17.49）J·K^-1. The constant-volume energy of combustion of the compound at T=298.15 K was measured by a precision oxygen-bomb combustion calorimeter to be ΔcU=-（32374.25±12.93）J·g^-1. The standard molar enthalpy of combustion for the compound was calculated to be ΔcHm = -（4445.47 ± 1.77） kJ·mol^-1 according to the definition of enthalpy of combustion and other thermodynamic principles. Finally, the standard molar enthalpy of formation of the compound was derived to be ΔfHm（C8H11NO, s）=-（274.68 ±2.06） kJ·mol^-1, in accordance with Hess law.展开更多
This standard specifies the terms and definitions, theory, apparatus, specimens, test procedures, calcu- lation results, apparatus check and test reports, etc. of abrasion resistance at ambient temperature of refracto...This standard specifies the terms and definitions, theory, apparatus, specimens, test procedures, calcu- lation results, apparatus check and test reports, etc. of abrasion resistance at ambient temperature of refractory products.展开更多
The inspection and quarantine standard is one of important basics to executeinspection and quarantine by laws. In recent years, with the development of economy and trade inChina, standardization has played an importan...The inspection and quarantine standard is one of important basics to executeinspection and quarantine by laws. In recent years, with the development of economy and trade inChina, standardization has played an important role in inspection and quarantine. During 2002-2004,department of Standards of Inspection and Quarantine, Certification and Accreditation Administrationof China has organized the research of the standards of inspection and quarantine, and has builtstandard sub- systems of nine fields in inspection and quarantine.展开更多
According to the prime task of ''readjusting industrial structure,energetically developing service industry, completing service standards and promoting servicelevel'', which are raised in the 10th Five...According to the prime task of ''readjusting industrial structure,energetically developing service industry, completing service standards and promoting servicelevel'', which are raised in the 10th Five-Year Plan Outline of National Economy and SocialDevelopment, Standardization Administration of China (SAC), National Development and ReformCommission, Ministry of Civil Affairs of the People'' s Republic of China, Ministry of Constructionof P.R.C, Ministry of Commerce of the People''s Republic of China, Ministry of Culture of the People''s Republic of China, the People''s Bank of China, General Administration of Quality Supervision,Inspection and Quarantine of P.R.C (AQSIQ), the State Administration of Radio, Film and Television,State General Administration of Sport, National Tourism Administration, China Seismological Bureau,China Meteorological Administration, China Insurance Regulatory Commission, State Post Bureau, StateCultural Relics, State Administration of Traditional Chinese Medicine Bureau, China NationalTechnical Committee 264 on Service of Standardization Administration of China, China Consumers''Association and China National Institute of Standardization had compiled and officially ratified theDevelopment Planning of National Service Standard 2005-2008 by the end of 2005.展开更多
Instrument calibration is vital to a successful control system because signal inputs to the system controllers come from such instruments. This paper presents a method for actualizing a standard low-cost loop calibrat...Instrument calibration is vital to a successful control system because signal inputs to the system controllers come from such instruments. This paper presents a method for actualizing a standard low-cost loop calibrator for the famous 4-20 mA electrical signaling scheme. The loop calibrator generates a linear current signal from 4 to 20 mA over a 250 ? typical process instrument load for calibration. The realization of the loop calibrator relies on a voltage-to-current converter to build a constant current source. The voltage controlled constant current source is built from discrete components and an op-amp to keep the cost low. Results from simulations and the prototype demonstrate the performance of the 4-20 mA loop calibrator which utilizes a greatly reduced number of components. The cost of these components is approximately 34% of the least expensive calibrator sampled, though other production costs are not included. This conclusion reinforces the fact that loop calibrators can be cheaper.展开更多
A recent experimental finding replicated an earlier research result, both of which demonstrated conflict with a specific Standard Model prediction. The “Muon g - 2” studies have indicated that the degree of muon pre...A recent experimental finding replicated an earlier research result, both of which demonstrated conflict with a specific Standard Model prediction. The “Muon g - 2” studies have indicated that the degree of muon precession predicted by the Model is not the same as observed. The researchers offer many posteriori atheoretical hypotheses as possible explanations of their findings, but no fundamental theoretical understanding of the near discovery is among them. This article describes both an explication for the unexpected result and describes its underlying mechanism based on an existing cosmological theory, the Probabilistic Spacetime Theory. The paper also discusses the potential value of this theory.展开更多
文摘Spectral analysis was a method of identifying substances, determining their chemical composition and calculating their content based on their spectral characteristics. This paper mainly discussed the application of various spectroscopic techniques, mainly including atomic absorption spectrometry (AAS) inductively coupled plasma emission spectrometry (ICP-AES) X-ray fluorescence spectroscopy (XRF) atomic fluorescence spectroscopy (AFS) direct reading spectroscopy (OES) glow discharge emission spectroscopy (GD-OSE) laser-induced breakdown spectroscopy (LIBS), in the formulation of non-ferrous metal standards in China. The AAS method was the most widely used single-element microanalysis method among the non-ferrous metal standards. The ICP-AES method was good at significant advantages in the simultaneous detection of multiple elements. The XRF method was increasingly used in the determination of primary and secondary trace elements due to its simple sample preparation and high efficiency. The AFS was mostly detected by single-element trace analysis. OES GD-OES and LIBS were playing an increasingly important role in the new demand area for non-ferrous metals. This paper discussed matrix elimination, sample digestion, sample preparation, instrument categories and other aspects of some standards, and summarized the advantages of spectral analysis and traditional chemical analysis methods. The new methods of future spectroscopic technology had been illustrated in the process of developing non-ferrous metal standards.
文摘 CAS 132-2006 formulation background and work courses
Flat panel display technology is maturing alongside the development of science and technology. The prices of flat panel display TV sets are becoming lower and lower. Flat panel display TV sets have begun entering the mainstream and are now the first choice of some consumers when making new TV purchases.Display TV Set Installation Service Point Explanation and AnalysisRepair, Retreat and Change Duty Stipulations. Peculiar use conditions, usage environments, and the practical circumstances of user consumption service requirements, etc., were also taken into account on the basis of extensive investigation, testing, and verification.……
文摘The fruits of Piper cubeba have been used in Ayurvedic system of medicine for pain,tastelessness, painful urination and mouth diseases. Among its various chemical constituents,（-）-hinokinin, a trypanosomicidal dibenzylbutyrolactone lignan, is found in significant quantities.For quality evaluation of P. cubeba fruit and its commercial formulations, there is an urgent need to develop an analytical method based on（-）-hinokinin. For this purpose, an HPLC method was developed using photo diode array detector and Waters HR C18 column with gradient elution consisting of water and acetonitrile. The developed method was validated as per ICH-Q2 B guidelines and found to be accurate, precise and linear over a wide range of concentrations（5–300 mg/m L）.（-）-Hinokinin contents were found to be in the range of 0.005–0.109%（m/m） in various P. cubeba samples. The developed method was extended to LC–MS for further identification and characterization of（-）-hinokinin in samples. The developed method is simple,rapid and specific, and can be used as a tool for quality control of P. cubeba fruits and its commercial formulations.
基金funded by the National Natural Science Foundation of China(Grant Nos.41427804,41421002,41373004)Beijing SHRIMP Center Open Foundation,and Program for Changjiang Scholars and Innovative Research Team in University(Grant No.IRT1281)the MOST Research Foundation from the State Key Laboratory of Continental Dynamics(BJ08132-1)
文摘Silicon isotope analysis traditionally uses a standard-sample bracketing （SSB） method that relies upon greater instrument stability than can be consistently expected. The following proposed method reduces the level of instrumental stability required for the analysis process and provides a valid solution for high-precision and accurate studies of Si isotopic compositions. Rock samples were dissolved by using alkali fusion and acidification. Silicon isotopes were purified with an ion exchange resin. Interfering peaks for isotopes were separated by using a Nu Plasma 1700 multi-collector inductively coupled plasma mass spectrometry （MS） system in high-resolution mode （M/AM 〉 8000 RP）. Two magnesium isotopes （25Mg and 26Mg） and three silicon isotopes （28Si, 29Si, and 3;Si） were analyzed in the same data collection cycle. Mg isotopes were used as an internal standard to calibrate the mass discrimination effects in MS analysis of Si isotopes in combination with the SSB method in order to reduce the effects of MS interference and instrumental mass dis- crimination on the accuracy of measurements. The conventional SSB method without the Mg internal standard and the proposed SSB method with Mg calibration delivered consistent results within two standard deviations. When Mg was used as an internal standard for calibration, the analysis precision was better than 0.05 %0 amu.
文摘In this article, we propose a generalized exp(-Φ(ξ))-expansion method and successfully implement it to find exact traveling wave solutions to the fifth order standard Sawada-Kotera (SK) equation. The exact traveling wave solutions are established in the form of trigonometric, hyperbolic, exponential and rational functions with some free parameters. It is shown that this method is standard, effective and easily applicable mathematical tool for solving nonlinear partial differential equations arises in the field of mathematical physics and engineering.
文摘After a straightforward general relativistic calculation on a modified flat-spacetime metric (developed from the fluctuating vacuum energy interacting with a graviton field), a pair of n-valued covariant and contravariant energy momentum tensors emerged analogous to quantized raising and lower operators. Detaching these operators from the general relativistic field equations, and then transporting them to act on extreme spacetimes, these operators were able to generate fundamental particle boson masses. In particular, the operators precisely generated Higgs mass. Then by applying a consistency approach to the gravitational field equations—similar to how Maxwell applied to the electromagnetic ones—it allowed for the coupling of spin-to-mass, further restricting the particle mass to be in precise agreement with CODATA experimental values. Since this is a massless field approach integrated discretely with a massive one, it overcomes various renormalizing difficulties;moreover it solves the mass hierarchal problem of the Standard Model of particle physics, and generates its spin and therefore shows quantum physics to be a subset of General Relativity, just as Einstein had first imagined.
基金supported by the National Natural Science Foundation of China (Grant No 20673050)
文摘This paper reports that low-temperature heat capacities of 4-（2-aminoethyl）-phenol （C8H11NO） are measured by a precision automated adiabatic calorimeter over the temperature range from 78 to 400 K. A polynomial equation of heat capacities as a function of the temperature was fitted by the least square method. Based on the fitted polynomial, the smoothed heat capacities and thermodynamic functions of the compound relative to the standard reference temperature 298.15K were calculated and tabulated at the interval of 5K. The energy equivalent, εcalor, of the oxygen-bomb combustion calorimeter has been determined from 0.68g of NIST 39i benzoic acid to be εcalor=（14674.69±17.49）J·K^-1. The constant-volume energy of combustion of the compound at T=298.15 K was measured by a precision oxygen-bomb combustion calorimeter to be ΔcU=-（32374.25±12.93）J·g^-1. The standard molar enthalpy of combustion for the compound was calculated to be ΔcHm = -（4445.47 ± 1.77） kJ·mol^-1 according to the definition of enthalpy of combustion and other thermodynamic principles. Finally, the standard molar enthalpy of formation of the compound was derived to be ΔfHm（C8H11NO, s）=-（274.68 ±2.06） kJ·mol^-1, in accordance with Hess law.
文摘This standard specifies the terms and definitions, theory, apparatus, specimens, test procedures, calcu- lation results, apparatus check and test reports, etc. of abrasion resistance at ambient temperature of refractory products.
文摘The inspection and quarantine standard is one of important basics to executeinspection and quarantine by laws. In recent years, with the development of economy and trade inChina, standardization has played an important role in inspection and quarantine. During 2002-2004,department of Standards of Inspection and Quarantine, Certification and Accreditation Administrationof China has organized the research of the standards of inspection and quarantine, and has builtstandard sub- systems of nine fields in inspection and quarantine.
文摘According to the prime task of ''readjusting industrial structure,energetically developing service industry, completing service standards and promoting servicelevel'', which are raised in the 10th Five-Year Plan Outline of National Economy and SocialDevelopment, Standardization Administration of China (SAC), National Development and ReformCommission, Ministry of Civil Affairs of the People'' s Republic of China, Ministry of Constructionof P.R.C, Ministry of Commerce of the People''s Republic of China, Ministry of Culture of the People''s Republic of China, the People''s Bank of China, General Administration of Quality Supervision,Inspection and Quarantine of P.R.C (AQSIQ), the State Administration of Radio, Film and Television,State General Administration of Sport, National Tourism Administration, China Seismological Bureau,China Meteorological Administration, China Insurance Regulatory Commission, State Post Bureau, StateCultural Relics, State Administration of Traditional Chinese Medicine Bureau, China NationalTechnical Committee 264 on Service of Standardization Administration of China, China Consumers''Association and China National Institute of Standardization had compiled and officially ratified theDevelopment Planning of National Service Standard 2005-2008 by the end of 2005.
文摘Instrument calibration is vital to a successful control system because signal inputs to the system controllers come from such instruments. This paper presents a method for actualizing a standard low-cost loop calibrator for the famous 4-20 mA electrical signaling scheme. The loop calibrator generates a linear current signal from 4 to 20 mA over a 250 ? typical process instrument load for calibration. The realization of the loop calibrator relies on a voltage-to-current converter to build a constant current source. The voltage controlled constant current source is built from discrete components and an op-amp to keep the cost low. Results from simulations and the prototype demonstrate the performance of the 4-20 mA loop calibrator which utilizes a greatly reduced number of components. The cost of these components is approximately 34% of the least expensive calibrator sampled, though other production costs are not included. This conclusion reinforces the fact that loop calibrators can be cheaper.
文摘A recent experimental finding replicated an earlier research result, both of which demonstrated conflict with a specific Standard Model prediction. The “Muon g - 2” studies have indicated that the degree of muon precession predicted by the Model is not the same as observed. The researchers offer many posteriori atheoretical hypotheses as possible explanations of their findings, but no fundamental theoretical understanding of the near discovery is among them. This article describes both an explication for the unexpected result and describes its underlying mechanism based on an existing cosmological theory, the Probabilistic Spacetime Theory. The paper also discusses the potential value of this theory.
