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Reductive Cleavage of S-S Bond by Sm/NiCl_2 or Sm/NiCl_2·6H_2O System: A New Method for the Preparation of Thiolesters
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作者 Hua Yue WU Red Er CHEN Yong Min ZHANG(Department of Cheniistry, Wenzhou Normal College, Wenzhou, 325000)(Departnieni of Chemistry. Zhejiang University at Xixi Campus, Hangzhou, 310028) 《Chinese Chemical Letters》 SCIE CAS CSCD 1999年第11期899-902,共4页
Disulfides were reduced by the Sm/NiCl2 or Sin/NiCI_2 6H_2O system to generate thiolateanion. which reacted further with anhydrides or acyl chlorides to afford thiolesters in good yieldsunder mild and neutral conditions.
关键词 Samarium-nickel (II) chloride. disulfide thiolester.
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Reductive Cleavage of the S-Si Bond in Phenylthio-trimethylsilane:A Novel Method for the Synthesis of Thiolesters 被引量:2
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作者 Zhang, SL Zhang, YM 《Chinese Chemical Letters》 SCIE CAS CSCD 1998年第1期25-27,共3页
Phenylthiotrimethylsilane is reduced hy samarium diiodide to yield samarium phenylthiolate. This new thiolate anion species reacts with acyl chlorides mildly to give thiolesters in good yields.
关键词 phenylthiotrimethylsilane samarium diiodide thiolester
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