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Synthesis of di-μ-oxo-tetra-(α-pentyloxy) tin(Ⅳ) phthalocyanine
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作者 Yi Ru Peng Yu Hong Cao Pei Feng Chen Xiao Xia Huang 《Chinese Chemical Letters》 SCIE CAS CSCD 2008年第3期273-276,共4页
Axially substituted tin phthalocyanines, namely dichloride-tetra-(α-pentyloxy) tin (Ⅳ) phthalocyanine 2, dihydroxy-tetra-(α-pentyloxy) tin (Ⅳ) phthalocyanine 3 and its dimmer di-μ-oxo-tetra-(α-pentyloxy... Axially substituted tin phthalocyanines, namely dichloride-tetra-(α-pentyloxy) tin (Ⅳ) phthalocyanine 2, dihydroxy-tetra-(α-pentyloxy) tin (Ⅳ) phthalocyanine 3 and its dimmer di-μ-oxo-tetra-(α-pentyloxy) tin(Ⅳ) phthalocyanine 4 were synthesized. The catalytic effect of H2O-free CaCl2 in quinoline was used for condensation of dihydroxy tin phthalocyanine 3 to the cofacially array dimmer 4. Their structures were characterized by UV-vis, IR, elemental analysis, MS, as well as ^1HNMR spectroscopy. 展开更多
关键词 Axially substituted tin (Ⅳ) phthalocyanine DIMMER Synthesis Characterization
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