The effects of the addition of rare earth （RE） elements on the void band in the diffusion layer, and the re sistances to both oxidation and spalling of aluminized steel were investigated through high temperature oxi...The effects of the addition of rare earth （RE） elements on the void band in the diffusion layer, and the re sistances to both oxidation and spalling of aluminized steel were investigated through high temperature oxidation and spalling tests. The results showed that RE had significant effects on the void band in the diffusion layer and the properties of aluminized steel. After diffusion treatment, a considerable number of the voids between the middle layer and transitional layer of pure aluminized coating, aggregated into wavy-line-shaped void bands parallel to the outer surface. For the RE added aluminized coating, only a few voids aggregated into intermittent block shapes. During high temperature oxidation at 800 ℃ for 200 h, the wavy void band of pure aluminized coating aggregated further into a linear crack parallel to the outer surface, and the internal oxidation occurred within them; the open cracks perpendicular to the surface penetrated through the diffusion layer. For the RE added aluminized coating, only a few voids aggregated into intermittent meniscus shapes. During cyclic spalling tests, the peeling, spallation, and pulver ulent cracking occurred along the void band in the diffusion layer of pure aluminized coating, but only a little spallation occurred in the diffusion layer of the RE-added aluminized coating, in which cracks perpendicular to the surface were much smaller than those of pure aluminized coating and did not penetrate through the diffusion layer. It is evident that RE addition can restrain the formation and aggregation of voids and subsequently improve the resistances to oxidation and spalling. The mechanism of the RE effect on the void band in the diffusion layer is also discussed.展开更多
The structural changes around a crack tip in a high density polyethylene were investigated by means of scanning synchrotron microfocus small-angle X-ray scattering technique. The scattering data confirm the process of...The structural changes around a crack tip in a high density polyethylene were investigated by means of scanning synchrotron microfocus small-angle X-ray scattering technique. The scattering data confirm the process of craze structure development near a crack tip based on the evolution of voids. In addition, it was found that the main stress in the plastic zone near a crack tip exhibited a gradient distribution with respect to its strength and direction. The whole damaged area showed a strain distribution indicating a flow behavior toward the crack tip.展开更多
Micron-sized internal cracks were introduced into rounded bars of pure iron by low cycle fatigue,and the cracks had irregular penny-shaped morphology with the critical diameter of about 30μm and the thickness of 0.5...Micron-sized internal cracks were introduced into rounded bars of pure iron by low cycle fatigue,and the cracks had irregular penny-shaped morphology with the critical diameter of about 30μm and the thickness of 0.5～1.5μm.The initi- ation and propagation of the cracks were investigated quantitatively as well as their location and geometry.After vacuum annealing of the samples fatigued,the mor- phology in a two-dimensional longitudinal section of cracks within grains had evolved from initially elliptical one into arrays of spherical voids controlled by surface diffu- sion.Furthermore,a typical morphology for a broken crack with a center spherical void surrounded by outer doughnut-like cavities was observed along a perpendicu- lar section of the specimen.Subsequently the spherical voids shrink and diminish gradually dominated by bulk diffusion.A physical model to heal an internal micro- crack was proposed,in particular for the various healing stages controlled by the related dominant diffusion mechanism and their dependencies upon the morphology and geometry of an original micro-crack in materials.展开更多
为研究预制裂纹不同偏移距离时运动裂纹与空孔的相互作用规律,采用动态焦散线实验系统,将预制裂纹的偏移距离设定为唯一变量,对含空孔的有机玻璃(PMMA)试件进行冲击三点弯实验。研究表明,存在两个临界距离:(6 mm (2 R)、9 mm (3 R)),在...为研究预制裂纹不同偏移距离时运动裂纹与空孔的相互作用规律,采用动态焦散线实验系统,将预制裂纹的偏移距离设定为唯一变量,对含空孔的有机玻璃(PMMA)试件进行冲击三点弯实验。研究表明,存在两个临界距离:(6 mm (2 R)、9 mm (3 R)),在该偏移距离下,裂纹扩展轨迹、动态断裂特性发生显著改变:(1)预制裂纹偏移距离不大于3 mm时,裂纹贯穿空孔,发生二次起裂,且二次起裂的速度与应力强度因子显著大于一次起裂,无偏移时裂纹轨迹的分形维数为最小值;(2)偏移距离增大至6 mm时,裂纹不再贯穿空孔,空孔对裂纹先吸引后排斥,裂纹速度与应力强度因子先减小后增大,裂纹轨迹的分形维数达到最大值;(3)偏移距离大于6 mm时,空孔对裂纹的吸引作用逐渐减小,大于9 mm后,空孔对裂纹的吸引不再显著,裂纹起裂后即向落锤加载方向扩展直至贯穿试件。展开更多
基金Item Sponsored by Key Science and Technology Plan Foundation of Henan of China (0423023500) and Natural ScienceFoundation of Henan Province (0511021600)
文摘The effects of the addition of rare earth （RE） elements on the void band in the diffusion layer, and the re sistances to both oxidation and spalling of aluminized steel were investigated through high temperature oxidation and spalling tests. The results showed that RE had significant effects on the void band in the diffusion layer and the properties of aluminized steel. After diffusion treatment, a considerable number of the voids between the middle layer and transitional layer of pure aluminized coating, aggregated into wavy-line-shaped void bands parallel to the outer surface. For the RE added aluminized coating, only a few voids aggregated into intermittent block shapes. During high temperature oxidation at 800 ℃ for 200 h, the wavy void band of pure aluminized coating aggregated further into a linear crack parallel to the outer surface, and the internal oxidation occurred within them; the open cracks perpendicular to the surface penetrated through the diffusion layer. For the RE added aluminized coating, only a few voids aggregated into intermittent meniscus shapes. During cyclic spalling tests, the peeling, spallation, and pulver ulent cracking occurred along the void band in the diffusion layer of pure aluminized coating, but only a little spallation occurred in the diffusion layer of the RE-added aluminized coating, in which cracks perpendicular to the surface were much smaller than those of pure aluminized coating and did not penetrate through the diffusion layer. It is evident that RE addition can restrain the formation and aggregation of voids and subsequently improve the resistances to oxidation and spalling. The mechanism of the RE effect on the void band in the diffusion layer is also discussed.
基金supported by the"Hundred Talents Project"of the Chinese Academy of Sciences,the National Basic Research Program of China(No.2005CB623800)National Natural Science Foundation of China(Nos.50603024, 50621302) and HASYLAB projectⅡ-20052011
文摘The structural changes around a crack tip in a high density polyethylene were investigated by means of scanning synchrotron microfocus small-angle X-ray scattering technique. The scattering data confirm the process of craze structure development near a crack tip based on the evolution of voids. In addition, it was found that the main stress in the plastic zone near a crack tip exhibited a gradient distribution with respect to its strength and direction. The whole damaged area showed a strain distribution indicating a flow behavior toward the crack tip.
基金The project supported by the National Outstanding Young Investigator Grant of China (59925104)the National Natural Science Foundation of China (59889101)
文摘Micron-sized internal cracks were introduced into rounded bars of pure iron by low cycle fatigue,and the cracks had irregular penny-shaped morphology with the critical diameter of about 30μm and the thickness of 0.5～1.5μm.The initi- ation and propagation of the cracks were investigated quantitatively as well as their location and geometry.After vacuum annealing of the samples fatigued,the mor- phology in a two-dimensional longitudinal section of cracks within grains had evolved from initially elliptical one into arrays of spherical voids controlled by surface diffu- sion.Furthermore,a typical morphology for a broken crack with a center spherical void surrounded by outer doughnut-like cavities was observed along a perpendicu- lar section of the specimen.Subsequently the spherical voids shrink and diminish gradually dominated by bulk diffusion.A physical model to heal an internal micro- crack was proposed,in particular for the various healing stages controlled by the related dominant diffusion mechanism and their dependencies upon the morphology and geometry of an original micro-crack in materials.
