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IPS e.max Press铸瓷与合金嵌体治疗后牙牙体缺损效果对比研究
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作者 周冰 王子华 李佳彧 《河南外科学杂志》 2024年第2期148-150,共3页
目的探讨IPS e.max Press铸瓷与合金嵌体治疗后牙牙体缺损的效果。方法前瞻性纳入2020-05—2022-05三门峡市中心医院口腔科收治的后牙牙体缺损患者,根据修复材料分为IPS e.max Press铸瓷嵌体组(铸瓷组)和合金嵌体组(合金组)。比较2组患... 目的探讨IPS e.max Press铸瓷与合金嵌体治疗后牙牙体缺损的效果。方法前瞻性纳入2020-05—2022-05三门峡市中心医院口腔科收治的后牙牙体缺损患者,根据修复材料分为IPS e.max Press铸瓷嵌体组(铸瓷组)和合金嵌体组(合金组)。比较2组患者的基线资料。治疗前后检测患者的龈沟液中炎性因子、评价牙周健康情况。治疗3个月后评价牙体缺损边缘密合度和美牙效果。结果共纳入86例(132颗牙)患者,每组43例(66颗牙)。2组患者的基线资料差异无统计学意义(P>0.05)。治疗后铸瓷组患者的IL-6、IL-8、CXCL16水平和GI、SBI及PLI评分均低于合金组;牙体缺损边缘密合度优于合金组,美牙效果满意率高于合金组。差异均有统计学意义(P<0.05)。结论与合金嵌体比较,采用IPS e.max Press铸瓷嵌体治疗后牙牙体缺损有利于降低龈沟液中炎性因子水平,改善牙周健康状况和牙体缺损边缘密合度,并可提高患者对美牙效果的满意度。但仍需进行更大样本量的前瞻性随机对照研究予以证实。 展开更多
关键词 后牙牙体缺损 IPS e.max press铸瓷嵌体 合金嵌体 牙周健康
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IPS e.max press热压铸造陶瓷全冠及二氧化锆全瓷冠对前牙修复患者牙龈健康美观度的影响
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作者 刘小瑜 陈西文 +2 位作者 庄梦瑶 张美玲 刘佳佳 《河北医学》 CAS 2024年第7期1140-1145,共6页
目的:比较IPS e.max press热压铸造陶瓷全冠及二氧化锆全瓷冠对前牙修复患者牙龈健康、美观度的影响,为前牙美学修复的材料选择提供临床参考。方法:以2021年5月至2022年5月于我院接受前牙修复的104例患者为研究对象,以随机数字表法分为... 目的:比较IPS e.max press热压铸造陶瓷全冠及二氧化锆全瓷冠对前牙修复患者牙龈健康、美观度的影响,为前牙美学修复的材料选择提供临床参考。方法:以2021年5月至2022年5月于我院接受前牙修复的104例患者为研究对象,以随机数字表法分为两组,分别52例。观察组、对照组分别以IPS e.max press铸瓷全冠、二氧化锆全瓷冠修复,比较两组患者的临床修复效果及修复后的牙龈指数、菌斑指数、龈沟出血指数、龈沟液炎性因子水平。结果:观察组边缘密合度、继发龋情况均优于对照组(P<0.05);修复后,观察组牙龈指数、菌斑指数等显著小于对照组,龈沟液IL-6、IL-8及TNF-α水平显著低于对照组(P<0.05);修复12个月后,观察组PES评分高于对照组(P<0.05)。结论:相比于二氧化锆全瓷冠,IPS e.max press铸瓷全冠具有良好的前牙美学修复效果,可降低龈沟液炎性因子水平,改善牙龈健康,并能提高前牙美观度。 展开更多
关键词 IPS e.max press铸瓷全冠 二氧化锆全瓷冠 牙龈指数 龈沟液 炎性因子
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Electrospinning-hot pressing technique for the fabrication of thermal and electrical storage membranes and its applications
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作者 Panpan Che Baoshan Xie +7 位作者 Penghui Cao Youfu Lv Daifei Liu Huali Zhu Xianwen Wu Zhangxing He Jian Chen Chuanchang Li 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第9期1945-1964,共20页
The combination of electrospinning and hot pressing,namely the electrospinning-hot pressing technique(EHPT),is an efficient and convenient method for preparing nanofibrous composite materials with good energy storage ... The combination of electrospinning and hot pressing,namely the electrospinning-hot pressing technique(EHPT),is an efficient and convenient method for preparing nanofibrous composite materials with good energy storage performance.The emerging composite membrane prepared by EHPT,which exhibits the advantages of large surface area,controllable morphology,and compact structure,has attracted immense attention.In this paper,the conduction mechanism of composite membranes in thermal and electrical energy storage and the performance enhancement method based on the fabrication process of EHPT are systematically discussed.Moreover,the state-of-the-art applications of composite membranes in these two fields are introduced.In particular,in the field of thermal energy storage,EHPT-prepared membranes have longitudinal and transverse nanofibers,which generate unique thermal conductivity pathways;also,these nanofibers offer enough space for the filling of functional materials.Moreover,EHPT-prepared membranes are beneficial in thermal management systems,building energy conservation,and electrical energy storage,e.g.,improving the electrochemical properties of the separators as well as their mechanical and thermal stability.The application of electrospinning-hot pressing membranes on capacitors,lithium-ion batteries(LIBs),fuel cells,sodium-ion batteries(SIBs),and hydrogen bromine flow batteries(HBFBs)still requires examination.In the future,EHPT is expected to make the field more exciting through its own technological breakthroughs or be combined with other technologies to produce intelligent materials. 展开更多
关键词 electrospinning-hot pressing technique thermal storage electrical storage composite membranes NANOFIBER
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Ultrahigh strength and improved electrical conductivity in an aging strengthened copper alloy processed by combination of equal channel angular pressing and thermomechanical treatment
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作者 WANG Xu LI Zhou +1 位作者 MENG Xiang-peng XIAO Zhu 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第6期1823-1837,共15页
In this paper,equal channel angular pressing and thermomechanical treatment was employed to improve the strength and electrical conductivity of an aging strengthened Cu-Ti-Cr-Mg alloy,and the microstructure and proper... In this paper,equal channel angular pressing and thermomechanical treatment was employed to improve the strength and electrical conductivity of an aging strengthened Cu-Ti-Cr-Mg alloy,and the microstructure and properties of the alloy were investigated in detail.The results showed that the samples deformed by the combination of cryogenic equal channel angular pressing(ECAP)and rolling had good comprehensive properties after aging at 400℃.The tensile strength of the peak-aged and over-aged samples was 1120 MPa and 940 MPa,with their corresponding electrical conductivity of 14.7%IACS and 22.1%IACS,respectively.ECAP and cryogenic rolling introduced high density dislocations,leading to the inhibition of the softening effects and refinement of the grains.After a long time aging at 400℃,the alloy exhibited ultra-high strength with obvious increasing electrical conductivity.The high strength was attributed to the synergistic effect of work hardening,grain refinement strengthening and precipitation strengthening.The precipitation of a large amount of Ti atoms from the matrix led to the high electrical conductivity of the over-aged sample. 展开更多
关键词 Cu-Ti alloy equal channel angular pressing ROLLING aging treatment high strength
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Effect of hot isostatic pressure on the microstructure and tensile properties of γ'-strengthened superalloy fabricated through induction-assisted directed energy deposition
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作者 Jianjun Xu Hanlin Ding +1 位作者 Xin Lin Feng Liu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第5期1089-1097,共9页
The microstructure characteristics and strengthening mechanism of Inconel738LC(IN-738LC) alloy prepared by using induction-assisted directed energy deposition(IDED) were elucidated through the investigation of samples... The microstructure characteristics and strengthening mechanism of Inconel738LC(IN-738LC) alloy prepared by using induction-assisted directed energy deposition(IDED) were elucidated through the investigation of samples subjected to IDED under 1050℃ preheating with and without hot isostatic pressing(HIP,1190℃,105 MPa,and 3 h).Results show that the as-deposited sample mainly consisted of epitaxial columnar crystals and inhomogeneously distributed γ’ phases in interdendritic and dendritic core regions.After HIP,grain morphology changed negligibly,whereas the size of the γ’ phase became increasingly even.After further heat treatment(HT,1070℃,2 h + 845℃,24 h),the γ’ phase in the as-deposited and HIPed samples presented a bimodal size distribution,whereas that in the as-deposited sample showed a size that remained uneven.The comparison of tensile properties revealed that the tensile strength and uniform elongation of the HIP + HTed sample increased by 5% and 46%,respectively,due to the synergistic deformation of bimodal γ’phases,especially large cubic γ’ phases.Finally,the relationship between phase transformations and plastic deformations in the IDEDed sample was discussed on the basis of generalized stability theory in terms of the trade-off between thermodynamics and kinetics. 展开更多
关键词 directed energy deposition Ni-based superalloys high-temperature preheating hot isostatic pressing MICROSTRUCTURE tensile properties
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Improving mechanical properties and high-temperature oxidation of press hardened steel by adding Cr and Si
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作者 Rong Zhu Yonggang Yang +4 位作者 Baozhong Zhang Borui Zhang Lei Li Yanxin Wu Zhenli Mi 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2024年第8期1865-1875,共11页
This work investigated the effect of Cr and Si on the mechanical properties and oxidation resistance of press hardened steel.Results indicated that the microstructure of the Cr-Si micro-alloyed press hardened steel co... This work investigated the effect of Cr and Si on the mechanical properties and oxidation resistance of press hardened steel.Results indicated that the microstructure of the Cr-Si micro-alloyed press hardened steel consisted of lath martensite,M_(23)C_(6)carbides,and retained austenite.The retained austenite and carbides are responsible for the increase in elongation of the micro-alloyed steel.In addition,after oxidation at 930℃for 5 min,the thickness of the oxide scales on the Cr-Si micro-alloyed press hardened steel is less than 5μm,much thinner than 45.50μm-thick oxide scales on 22MnB5.The oxide scales of the Cr-Si micro-alloyed steel are composed of Fe_(2)O_(3),Fe_(3)O_(4),mixed spinel oxide(FeCr_(2)O_(4)and Fe_(2)SiO_(4)),and amorphous SiO_(2).Adding Cr and Si significantly reduces the thickness of the oxide scales and prevents the generation of the FeO phase.Due to the increase of spinel FeCr_(2)O_(4)and Fe_(2)SiO_(4)phase in the inner oxide scale and the amorphous SiO_(2)close to the substrate,the oxidation resistance of the Cr-Si micro-alloyed press hardened steel is improved. 展开更多
关键词 Cr-Si micro-alloyed press hardened steel mechanical properties oxidation resistance amorphous SiO_(2)
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Ballistic performance of titanium-based layered composites made using blended elemental powder metallurgy and hot isostatic pressing
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作者 Pavlo Markovsky Jacek Janiszewski +5 位作者 Dmytro Savvakin Oleksandr Stasyuk Bartosz Fikus Victor Samarov Vianey Ellison Sergey V.Prikhodko 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第9期1-14,共14页
Metal matrix composites tiles based on Ti-6Al-4V(Ti64)alloy,reinforced with 10,20,and 40(vol%)of either TiC or TiB particles were made using press-and-sinter blended elemental powder metallurgy(BEPM)and then bonded to... Metal matrix composites tiles based on Ti-6Al-4V(Ti64)alloy,reinforced with 10,20,and 40(vol%)of either TiC or TiB particles were made using press-and-sinter blended elemental powder metallurgy(BEPM)and then bonded together into 3-layer laminated plates using hot isostatic pressing(HIP).The laminates were ballistically tested and demonstrated superior performance.The microstructure and properties of the laminates were analyzed to determine the effect of the BEPM and HIP processing on the ballistic properties of the layered plates.The effect of porosity in sintered composites on further diffusion bonding of the plates during HIP is analyzed to understand the bonding features at the interfaces between different adjacent layers in the laminate.Exceptional ballistic performance of fabricated structures was explained by a significant reduction in the residual porosity of the BEPM products by their additional processing using HIP,which provides an unprecedented increase in the hardness of the layered composites.It is argued that the combination of the used two technologies,BEPM and HIP is principally complimentary for the materials in question with the abilities to solve the essential problems of each used individually. 展开更多
关键词 Metal matrix composites Powder metallurgy Titanium hydride powder Master alloy Titanium carbide Titanium boride Hot isostatic pressing Ballistic tests
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IPS e.max Press全瓷嵌体在后牙修复中的应用效果观察
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作者 闭艳妲 李振强 王佳琼 《交通医学》 2024年第3期310-312,共3页
目的:分析IPS e.max Press全瓷嵌体在后牙修复中的临床效果。方法:回顾性分析80例后牙修复患者临床资料,按照治疗方法不同分为对照组和观察组各40例。对照组采用氧化锆嵌体修复,观察组采用IPS e.max Press全瓷嵌体修复。比较两组修复效... 目的:分析IPS e.max Press全瓷嵌体在后牙修复中的临床效果。方法:回顾性分析80例后牙修复患者临床资料,按照治疗方法不同分为对照组和观察组各40例。对照组采用氧化锆嵌体修复,观察组采用IPS e.max Press全瓷嵌体修复。比较两组修复效果、菌斑指数、咀嚼功能及患者满意度。结果:修复后半年观察组修复体完整性、边缘密合性、边缘变色、颜色匹配、继发龋评分分别为(0.43±0.08)分、(0.31±0.03)分、(0.49±0.06)分、(0.46±0.05)分和(1.05±0.07)分,低于对照组的(0.56±0.07)分、(0.47±0.05)分、(0.61±0.08)分、(0.58±0.06)分和(1.21±0.09)分,修复后3年观察组修复体完整性、边缘密合性、边缘变色、颜色匹配、继发龋评分分别为(0.51±0.05)分、(0.43±0.05)分、(0.61±0.07)分、(0.57±0.06)分和(0.91±0.04)分,低于对照组的(0.72±0.08)分、(0.65±0.07)分、(0.88±0.09)分、(0.72±0.08)分和(0.99±0.06)分,差异均有统计学意义(P<0.05)。修复后观察组菌斑指数(1.07±0.08)分,低于对照组的(1.71±0.09)分,修复后观察组咀嚼功能(95.46±3.41)%,优于对照组的(79.25±4.34)%,差异均有统计学意义(P<0.05)。观察组患者总满意率97.5%,高于对照组的80.0%,差异有统计学意义(P<0.05)。结论:IPS e.max Press全瓷嵌体修复后牙的临床效果优于氧化锆嵌体。 展开更多
关键词 IPS e.max press全瓷嵌体 后牙修复 修复效果 菌斑指数 咀嚼功能
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Pressure generation under deformation in a large-volume press
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作者 Saisai Wang Xinyu Zhao +8 位作者 Kuo Hu Bingtao Feng Xuyuan Hou Yiming Zhang Shucheng Liu Yuchen Shang Zhaodong Liu Mingguang Yao Bingbing Liu 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第9期622-626,共5页
Deformation can change the transition pathway of materials under high pressure,thus significantly affects physical and chemical properties of matters.However,accurate pressure calibration under deformation is challeng... Deformation can change the transition pathway of materials under high pressure,thus significantly affects physical and chemical properties of matters.However,accurate pressure calibration under deformation is challenging and thereby causes relatively large pressure uncertainties in deformation experiments,resulting in the synthesis of complex multiphase materials.Here,pressure generations of three types of deformation assemblies were well calibrated in a Walker-type largevolume press(LVP)by electrical resistance measurements combined with finite element simulations(FESs).Hard Al_(2)O_(3) or diamond pistons in shear and uniaxial deformation assemblies significantly increase the efficiency of pressure generation compared with the conventional quasi-hydrostatic assembly.The uniaxial deformation assembly using flat diamond pistons possesses the highest efficiency in these deformation assemblies.This finding is further confirmed by stress distribution analysis based on FESs.With this deformation assembly,we found shear can effectively promote the transformation of C60 into diamond under high pressure and realized the synthesis of phase-pure diamond at relatively moderate pressure and temperature conditions.The present developed techniques will help improve pressure efficiencies in LVP and explore the new physical and chemical properties of materials under deformation in both science and technology. 展开更多
关键词 shear/uniaxial DEFORMATION pressURE calibration finite element simulations large- VOLUME press high pressURE
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Modulation effects of pressing manipulation on local inflammatory responses and ERK/NF-κB pathway in trigger point model rats
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作者 LIU Dan JIANG Quanrui +5 位作者 KUANG Xiaoxia PAN Jieling ZENG Li LI Jiangshan LIU Xiaowei LI WU 《Journal of Acupuncture and Tuina Science》 CAS CSCD 2024年第5期371-380,共10页
Objective:To investigate the mechanism of trigger point deactivation induced by pressing manipulation in a rat model and to explore its potential regulation of the inflammatory response through the extracellular signa... Objective:To investigate the mechanism of trigger point deactivation induced by pressing manipulation in a rat model and to explore its potential regulation of the inflammatory response through the extracellular signal-regulated kinase(ERK)/nuclear factor-κB(NF-κB)pathway.Methods:Fifty male Sprague-Dawley rats were randomly divided into a blank group,a model group,a pressing manipulation group,an ERK agonist group,and a pressing manipulation+ERK agonist group,with 10 rats in each group.Except for the blank group,rats in other groups were used to establish the trigger point rat model using the blunt blow combined with the eccentric exercise method.The pressing manipulation group underwent pressing manipulation intervention at the trigger points.The ERK agonist group received an injection of recombinant human epidermal growth factor via the tail vein.The pressing manipulation+ERK agonist group received interventions from both the pressing manipulation and ERK agonist groups.The pressure pain threshold(PPT)was measured by a mechanical pain threshold detector before and after the intervention.The histological changes were evaluated by hematoxylin-eosin staining after the intervention;the expression levels of ERK,phosphorylated ERK(p-ERK),NF-κB p65(p65),phosphorylated NF-κB p65(p-p65),and phosphorylated NF-κB inhibitor(p-IκB)were detected by Western blotting;the levels of interleukin(IL)-1β,IL-6,and tumor necrosis factor(TNF)-αwere detected by enzyme-linked immunosorbent assay.Results:The PPT increased(P<0.05);the inflammatory cells disappeared;the ratios of p-ERK/ERK,p-p65/p65,and p-IκB/β-actin,also the levels of IL-1β,IL-6,and TNF-αall decreased in the pressing manipulation group after the intervention compared with the model group(P<0.05).The PPT decreased significantly(P<0.05),the inflammatory cell presence increased,and the ratios of p-ERK/ERK and p-p65/p65 were elevated(P<0.05);additionally,the levels of IL-6 and TNF-αwere significantly higher in the pressing manipulation+ERK agonist group compared with the pressing manipulation group(P<0.05).The PPT was significantly lower(P<0.05),the inflammatory cell count was higher,the ratios of p-ERK/ERK and p-IκB/β-actin and the levels of IL-1βand TNF-αwere significantly higher in the ERK agonist group compared with the pressing manipulation+ERK agonist group(P<0.05).Conclusion:Pressing manipulation can effectively alleviate inflammation and pain in trigger point model rats,potentially by inhibiting the ERK/NF-κB signaling pathway. 展开更多
关键词 TUINA MASSAGE pressing Manipulation Ashi Point Trigger Points ERK/NF-κB Signaling Pathway INFLAMMATION Rats
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Effect of the capsule on deformation and densification behavior of nickel-based superalloy compact during hot isostatic pressing 被引量:3
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作者 Lebiao Yang Xiaona Ren +4 位作者 Chao Cai Pengju Xue MIrfan Hussain Yusheng Shi Changchun Ge 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第1期122-130,共9页
The Shima yield criterion used in finite element analysis for nickel-based superalloy powder compact during hot isostatic pressing(HIP) was modified through uniaxial compression experiments. The influence of cylindric... The Shima yield criterion used in finite element analysis for nickel-based superalloy powder compact during hot isostatic pressing(HIP) was modified through uniaxial compression experiments. The influence of cylindrical capsule characteristics on FGH4096M superalloy powder compact deformation and densification behavior during HIP was investigated through simulations and experiments. Results revealed the simulation shrinkage prediction fitted well with the experimental shrinkage including a maximum shrinkage error of 1.5%. It was shown that the axial shrinkage was 1.7% higher than radial shrinkage for a cylindrical capsule with the size of ∮50 mm × 100 mm due to the force arm difference along the axial and radial direction of the capsule. The stress deviated from the isostatic state in the capsule led to the uneven shrinkage and non-uniform densification of the powder compact. The ratio of the maximum radial displacement to axial displacement increased from0.47 to 0.75 with the capsule thickness increasing from 2 to 4 mm. The pressure transmission is related to the capsule thickness, the capsule material performance, and physical parameters in the HIP process. 展开更多
关键词 hot isostatic pressing nickel-based superalloy compact CAPSULE DENSIFICATION DEFORMATION
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Effects of microstructure characteristics on the tensile properties and fracture toughness of TA15 alloy fabricated by hot isostatic pressing 被引量:2
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作者 Langping Zhu Yu Pan +6 位作者 Yanjun Liu Zhiyu Sun Xiangning Wang Hai Nan Muhammad-Arif Mughal Dong Lu Xin Lu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2023年第4期697-706,共10页
Powder hot isostatic pressing(HIP) is an effective method to achieve near-net-shape manufacturing of high-quality complex thinwalled titanium alloy parts, and it has received extensive attention in recent years. Howev... Powder hot isostatic pressing(HIP) is an effective method to achieve near-net-shape manufacturing of high-quality complex thinwalled titanium alloy parts, and it has received extensive attention in recent years. However, there are few reports about the microstructure characteristics on the strengthening and toughening mechanisms of powder hot isostatic pressed(HIPed) titanium alloys. Therefore, TA15powder was prepared into alloy by HIP approach, which was used to explore the microstructure characteristics at different HIP temperatures and the corresponding tensile properties and fracture toughness. Results show that the fabricated alloy has a “basket-like structure” when the HIP temperature is below 950℃, consisting of lath clusters and surrounding small equiaxed grains belts. When the HIP temperature is higher than 950℃, the microstructure gradually transforms into the Widmanstatten structure, accompanied by a significant increase in grain size. The tensile strength and elongation are reduced from 948 MPa and 17.3% for the 910℃ specimen to 861 MPa and 10% for the 970℃ specimen.The corresponding tensile fracture mode changes from transcrystalline plastic fracture to mixed fracture including intercrystalline cleavage.The fracture toughness of the specimens increases from 82.64 MPa·m^(1/2)for the 910℃ specimen to 140.18 MPa·m^(1/2)for the 970℃ specimen.Specimens below 950℃ tend to form holes due to the prior particle boundaries(PPBs), which is not conducive to toughening. Specimens above 950℃ have high fracture toughness due to the crack deflection, crack branching, and shear plastic deformation of the Widmanstatten structure. This study provides a valid reference for the development of powder HIPed titanium alloy. 展开更多
关键词 POWDER titanium alloy hot isostatic pressing STRENGTH fracture toughness
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Effect of hot isostatic pressing processing parameters on microstructure and properties of Ti60 high temperature titanium alloy 被引量:2
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作者 Tian-yu Liu Kun Shi +6 位作者 Jun Zhao Shi-bing Liu You-wei Zhang Hong-yu Liu Tian-yi Liu Xiao-ming Chen Xin-min Mei 《China Foundry》 SCIE CAS CSCD 2023年第1期49-56,共8页
Hot isostatic pressing parameters are critical to Ti60 high temperature titanium alloy castings which have wide application perspective in aerospace.In order to obtain optimal processing parameters,the effects of hot ... Hot isostatic pressing parameters are critical to Ti60 high temperature titanium alloy castings which have wide application perspective in aerospace.In order to obtain optimal processing parameters,the effects of hot isostatic pressing parameters on defects,composition uniformity,microstructure and mechanical properties of Ti60 cast high temperature titanium alloy were investigated in detail.Results show that increasing temperature and pressure of hot isostatic pressing can reduce defects,especially,the internal defects are substantially eliminated when the temperature exceeds 920℃or the pressure exceeds 125 MPa.The higher temperature and pressure can improve the microstructure uniformity.Besides,the higher pressure can promote the composition uniformity.With the temperature increases from 880℃to 960℃,α-laths are coarsened.But with increasing pressure,the grain size of prior-βphase,the widths ofα-laths andα-colony are reduced.The tensile strength of Ti60 alloy is 949 MPa,yield strength is 827 MPa,and the elongation is 11%when the hot isostatic pressing parameters are 960℃/125 MPa/2 h,which exhibits the best match between the strength and plasticity. 展开更多
关键词 hot isostatic pressing processing parameters Ti60 titanium alloy DEFECTS composition uniformity microstructure mechanical properties
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Simple shear extrusion versus equal channel angular pressing:A comparative study on the microstructure and mechanical properties of an Mg alloy 被引量:2
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作者 A.Rezaei R.Mahmudi +1 位作者 C.Cayron R.E.Logé 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第5期1769-1790,共22页
Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The mi... Two severe plastic deformation(SPD)techniques of simple shear extrusion(SSE)and equal channel angular pressing(ECAP)were employed to process an extruded Mg-6Gd-3Y-1.5Ag(wt%)alloy at 553 K for 1,2,4 and 6 passes.The microstructural evolutions were studied by electron back scattered diffraction(EBSD)analysis and transmission electron microscopy(TEM).The initial grain size of 7.5μm in the extruded alloy was reduced to about 1.3μm after 6 SPD passes.Discontinuous dynamic recrystallization was suggested to be operative in both SSE and ECAP,with also a potential contribution of continuous dynamic recrystallization at the early stages of deformation.The difference in the shear strain paths of the two SPD techniques caused different progression rate of dynamic recrystallization(DRX),so that the alloys processed by ECAP exhibited higher fractions of recrystallization and high angle grain boundaries(HAGBs).It was revealed that crystallographic texture was also significantly influenced by the difference in the strain paths of the two SPD methods,where dissimilar basal plane texture components were obtained.The compression tests,performed along extrusion direction(ED),indicated that the compressive yield stress(CYS)and ultimate compressive strength(UCS)of the alloys after both SEE and ECAP augmented continuously by increasing the number of passes.ECAP-processed alloys had lower values of CYS and UCS compared to their counterparts processed by SSE.This difference in the mechanical responses was attributed to the different configurations of basal planes with respect to the loading direction(ED)of each SPD technique. 展开更多
关键词 Mg-Gd-Y alloys Severe plastic deformation Simple shear extrusion Equal channel angular pressing Dynamic recrystallization Mechanical properties
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Superplastic behavior of a fine-grained Mg-Gd-Y-Ag alloy processed by equal channel angular pressing 被引量:1
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作者 A.Rezaei R.Mahmudi R.E.Logé 《Journal of Magnesium and Alloys》 SCIE EI CAS CSCD 2023年第10期3815-3828,共14页
An extruded Mg-6Gd-3Y-1.5Ag(wt%) alloy was processed by 6 passes of equal channel angular pressing(ECAP) at 553 K using route Bc to refine the microstructure. Electron back-scattered diffraction(EBSD) analysis showed ... An extruded Mg-6Gd-3Y-1.5Ag(wt%) alloy was processed by 6 passes of equal channel angular pressing(ECAP) at 553 K using route Bc to refine the microstructure. Electron back-scattered diffraction(EBSD) analysis showed a fully recrystallized microstructure for the extruded alloy with a mean grain size of 8.6 μm. The microstructure of the ECAP-processed alloy was uniformly refined through dynamic recrystallization(DRX). This microstructure contained fine grains with an average size of 1.3 μm, a high fraction of high angle grain boundaries(HAGBs), and nano-sized Mg_(5)Gd-type particles at the boundaries of the DRXed grains, detected by transmission electron microscopy(TEM). High-temperature shear punch testing(SPT) was used to evaluate the superplastic behavior of both the extruded and ECAP-processed alloys by measuring the strain rate sensitivity(SRS) index(m-value). While the highest m-value for the extruded alloy was measured to be 0.24 at 673 K, the ECAP-processed alloy exhibited much higher m-values of 0.41 and 0.52 at 598 and 623 K, respectively,delineating the occurrence of superplastic flow. Based on the calculated average activation energy of 118 kJ mol^(-1) and m-values close to 0.5, the deformation mechanism for superplastic flow at the temperatures of 598 and 623 K for the ECAP-processed alloys was recognized to be grain boundary sliding(GBS) assisted by grain boundary diffusion. 展开更多
关键词 Mg-Gd-Y alloys Equal channel angular pressing SUPERPLASTICITY Strain rate sensitivity Grain boundary sliding
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Influence of twist extrusion process on consolidation of pure aluminum powder in tubes by equal channel angular pressing and torsion 被引量:4
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作者 王晓溪 何敏 +2 位作者 朱珍 薛克敏 李萍 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第7期2122-2129,共8页
In comparison with the conventional equal channel angular pressing(ECAP) process,a comprehensive study of influence of twist extrusion(TE) process on consolidating pure aluminum powder in tubes(PITs) by equal ch... In comparison with the conventional equal channel angular pressing(ECAP) process,a comprehensive study of influence of twist extrusion(TE) process on consolidating pure aluminum powder in tubes(PITs) by equal channel angular pressing and torsion(ECAPT) was conducted via three-dimensional(3D) finite element simulation,experimental investigation and theoretical analysis.Simulation results revealed that during the consolidation of aluminum powder particles by ECAPT,TE process played a significant role of back pressure.Due to the torsional shear and high hydrostatic pressure exerted by twist channel,both the magnitude and homogeneity of the effective strain were increased markedly.After one pass of ECAPT process using a square channel with an inner angle of 90° and a twist slope angle of 36.5° at 200℃,commercial pure aluminum powder particles were successfully consolidated to nearly full density.Simulation and experimental results showed good agreement.In the microstructure observations,grains were greatly refined.At the same time,porosities were effectively eliminated by shrinking in size and breaking into small ones.Microhardness test indicated that strain distribution of ECAPT-processed billet was more homogeneous with respect to the ECAP-processed one.All these improvements may be attributed to the extreme intense shear strain induced during ECAPT and the increase in self-diffusion coefficient of aluminum due to the back pressure exerted by TE process. 展开更多
关键词 aluminum powder equal channel angular pressing and torsion powder consolidation back pressure
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In-situ ultrasonic calibrations of pressure and temperature in a hinge-type double-stage cubic large volume press 被引量:1
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作者 Qingze Li Xiping Chen +3 位作者 Lei Xie Tiexin Han Jiacheng Sun Leiming Fang 《Chinese Physics B》 SCIE EI CAS CSCD 2022年第6期272-277,共6页
Here,simultaneous in-situ calibration of pressures and temperatures was performed in a hinge-type second-stage cubic large volume press(LVP)up to 15 GPa and 1400 K by an acoustic travel-time approach.Based on the rece... Here,simultaneous in-situ calibration of pressures and temperatures was performed in a hinge-type second-stage cubic large volume press(LVP)up to 15 GPa and 1400 K by an acoustic travel-time approach.Based on the recently reported P-tSand P-T-tP-tSequations for Al2O3buffer rod,the cell pressures and temperatures in the chamber of LVP were insitu determined,in comparison with those by conventional off-line(or fixed-points)pressure calibration method and direct thermocouple measurement,respectively.It is found that the cell pressures of the LVP chamber are significantly reduced after annealing at simultaneous high pressures and high temperatures,owing to the stress relaxation as accumulate in the LVP chamber.This acoustic travel-time method is verified to be a good way for precise determination of thermal(cell)pressures at high temperature conditions,and is of great importance and necessity to conduct in-situ physical property measurements under extreme high P-T conditions,especially when the precious synchrotron x-ray/neutron diffraction beams are not available. 展开更多
关键词 cubic press simultaneous in-situ calibration of pressures and temperatures acoustic travel-time high pressure and high temperature
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Preparation of Al-doped ZnO sputter target by hot pressing 被引量:6
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作者 王星明 白雪 +4 位作者 段华英 石志霞 孙静 卢世刚 黄松涛 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2011年第7期1550-1556,共7页
Al-doped ZnO (AZO) target was prepared by hot pressing using ZnO and Al2O3 powder in mass ratio of 98:2.The effects of hot pressing conditions including temperature,pressure and preserving time on relative density ... Al-doped ZnO (AZO) target was prepared by hot pressing using ZnO and Al2O3 powder in mass ratio of 98:2.The effects of hot pressing conditions including temperature,pressure and preserving time on relative density were investigated.Pore evolution and phase structure change during densification process were studied.The results show that AZO target with super high relative density of 99% was prepared by two-stage hot pressing method under pressure of 35MPa,temperature of 1 050℃ and 1 150℃ with preserving time of 1 h,respectively.At temperature around 1 050℃,the number of isolated pore wasminimum.At temperature lower than 900℃,there existed Al2O3 phase.At temperature higher than 1 000℃,ZnAl2O4 phase was generated and its content was increased with temperature increasing.Hot pressing method had the advantage over pressureless sintering that the content of ZnAl2O4 was lower and sintering temperature could be also lower.With increasing the hot pressing temperature and preserving time,the electric resistivity of AZO target decreased greatly.A low resistivity of 3 10-3 cm was achieved under the temperature of 1 100℃,pressure of 35MPa and preserving time of 10 h. 展开更多
关键词 aluminum-doped ZnO (AZO) sputter target hot pressing PORE phase structure
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Effect of equal-channel angular pressing and aging on corrosion behavior of ZK60 Mg alloy 被引量:6
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作者 李鑫 江静华 +3 位作者 赵永好 马爱斌 文道静 朱运田 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第12期3909-3920,共12页
Commercial ZK60 Mg alloy was processed by multi-pass equal-channel angular pressing(ECAP) and subsequent aging to investigate the effect of grain refinement and second-phase redistribution on its corrosion behavior.... Commercial ZK60 Mg alloy was processed by multi-pass equal-channel angular pressing(ECAP) and subsequent aging to investigate the effect of grain refinement and second-phase redistribution on its corrosion behavior. Electrochemical tests show that the fine-grained samples after more ECAP passes have higher corrosion current densities(Jcorr) in the polarization curves, lower charge-transfer resistance(Rt) values in the EIS plots. The severe plastic deformation decreases the alloy corrosion resistance besides the well-known strengthening and toughening. Scanning Kelvin probe(SKP) measurement shows that the anodic and cathode sites are homogeneously distributed on the surface of the fine-grained alloy, which inhibits localized corrosion. The SKP potential, having linear relationship with the corrosion potential(φcorr), decreases with increasing the ECAP pass. Furthermore, the post-ECAP aging can slightly improve the corrosion resistance of the fine-grained ZK60 Mg alloy and enhance the comprehensive performances, due to the stress relief and uniform distribution of second-phase particles. 展开更多
关键词 ZK60 Mg alloy equal-channel angular pressing AGING corrosion resistance fine-grains
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Microstructure and mechanical properties of Mg-Gd-Y-Zr alloy processed by equal channel angular pressing 被引量:7
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作者 张帆 张可翔 +4 位作者 谭成文 于晓东 马红磊 王富耻 才鸿年 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2011年第10期2140-2146,共7页
Microstructure evolution and texture development and their effects on mechanical properties of a Mg-Gd-Y-Zr alloy during equal channel angular pressing(ECAP) were investigated.It is found that the microstructure is ... Microstructure evolution and texture development and their effects on mechanical properties of a Mg-Gd-Y-Zr alloy during equal channel angular pressing(ECAP) were investigated.It is found that the microstructure is still inhomogeneous after four passes,and two zones,namely the fine grain zone(FGZ) and the coarse grain zone(CGZ) are formed.The grain refinement occurs mainly by particle-stimulated nucleation(PSN) mechanism,which led to a more random texture after four passes of ECAP.In the ECAP-processed alloy,the strength did not increase while the ductility was enhanced dramatically compared with the as-received condition.The change of ductility of this alloy was discussed in terms of texture and second phase particles. 展开更多
关键词 Mg-Gd-Y-Zr magnesium alloy equal channel angular pressing(ECAP) grain size TEXTURE second phase particles mechanical properties
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