800 MPa grade ultralow carbon bainitic (NULCB) steel is the recently developed new generation steel, which was produced by thermo mechanical controlled processing & relaxation-precipitation controlling transformati...800 MPa grade ultralow carbon bainitic (NULCB) steel is the recently developed new generation steel, which was produced by thermo mechanical controlled processing & relaxation-precipitation controlling transformation (TMCP&RPC) tech- nique. The microstructure and the mechanical properties of the heat-affected zone (HAZ) in NULCB steel under laser welding conditions were investigated by using a Gleeble-1500 thermal simulator. The experimental results indicate that the simplex microstructure in the HAZ is granular bainite that consists of bainite-ferrite (BF) lath and M-A constituent when the cooling time from 800 to 500℃ (t8/5) is 0.3-30 s, and the M-A constituent consists of twinned martensite and residual austenite. As t8/5 increases, the hardness and tensile strength of HAZ decreases, but they are higher than that of the base metal, indicating the absence of softened zone after laser welding. The impact toughness of HAZ increases at first and then decreases when t8/5 increases. The impact energy of HAZ is much higher than that of the base metal when t8/5 is between 3 and 15 s. It indicates that excellent low temperature toughness can be obtained under appropriate laser welding conditions.展开更多
The microstructure evolution of heat-affected zone (HAZ) in the multi-pass underwater welded joints is investigated in the present work, and it can be characterized by four zones, marked as Region A, B, C and D, res...The microstructure evolution of heat-affected zone (HAZ) in the multi-pass underwater welded joints is investigated in the present work, and it can be characterized by four zones, marked as Region A, B, C and D, respectively. The microstructure in Region A is the mixture of lath martensite and residual austenite. Besides this structure, lots of acicular ferrite appears in Region B as well, and the grain size becomes larger. Lath ferrite combined with granular bainite is observed in Region C. In Region D, tempered sorbite, granular bainite and fine acicular ferrite are found within the grains, while massive ferrite and Widmanstatten structure are distributed along the grain boundary: The thermal effect of multi-pass welding makes the microstructure and property more and more uniform in the ttAZ, and the largest hardness 356 HV in the HAZ appears in Region A.展开更多
The main aim of this study was to investigate liquation cracking in the heat-affected zone(HAZ)of the IN939 superalloy upon tungsten inert gas welding.A solid solution and age-hardenable filler metals were further stu...The main aim of this study was to investigate liquation cracking in the heat-affected zone(HAZ)of the IN939 superalloy upon tungsten inert gas welding.A solid solution and age-hardenable filler metals were further studied.On the pre-weld heat-treated samples,upon solving the secondaryγ′particles in the matrix,primaryγ′particles in the base metal grew to"ogdoadically diced cubes"of about 2μm in side lengths.The pre-weld heat treatment reduced the hardness of the base metal to about HV 310.Microstructural studies using optical and fieldemission scanning electron microscopy revealed that the IN939 alloy was susceptible to liquation cracking in the HAZ.The constitutional melting of the secondary,eutectic,and Zr-rich phases promoted the liquation cracking in the HAZ.The microstructure of the weld fusion zones showed the presence of fine spheroidalγ′particles with sizes of about 0.2μm after the post-weld heat treatment,which increased the hardness of the weld pools to about HV 350 and 380 for the Hastelloy X and IN718 filler metals,respectively.Application of a suitable solid solution filler metal could partially reduce the liquation cracking in the HAZ of IN939 alloy.展开更多
Fracture parameters of welded joints with different strength matching and crack depth in weld metal are investigated by using the methods of elastoplastic finite element analysis and three point bend specimen test. Th...Fracture parameters of welded joints with different strength matching and crack depth in weld metal are investigated by using the methods of elastoplastic finite element analysis and three point bend specimen test. The results show that for shallow crack, the plastic zone turns large in loading process, and the fracture toughness turns high. The extent of the plastic zone of overmatched joint is larger than that of undermatched joint because it will extends to parent metal from the weld metal in loading process for the same CTOD value. The plastic zone of undermatched joint is restricted within the weld, and the size of that is small. Overmatched joint shows the fracture behaviour of shallow crack may more easily than the undermatched joint, while the two sorts of joint specimens have the same crack depth. Therefore, the fracture-resistant capability of overmatched weld is better than that of undermatched weld. when the toughness of weld metals is similar for both overmatched and undermatched joints.展开更多
The simulated fine grained heat-affected zone (FGHAZ) specimens for P92 welded joints were prepared by heat treatment, then the creep tests were carried out at 650 ℃ under the applied stress of 90-120 MPa to investig...The simulated fine grained heat-affected zone (FGHAZ) specimens for P92 welded joints were prepared by heat treatment, then the creep tests were carried out at 650 ℃ under the applied stress of 90-120 MPa to investigate high-temperature creep behavior of FGHAZ. The results show that the creep property of FGHAZ is much inferior to that of the base metal, which exhibits the much higher steady creep rate and shorter time to creep fracture. The power law equation can describe the steady creep rate dependence on applied stress, indicating that the stress exponent n of FGHAZ is distinguished between two regions with n=15.1 at high stresses (more than 100 MPa) and n=8.64 at lower stresses. Based on Monkman-Grant equation, the relationship between the secondary creep rate and time to rupture is obtained to evaluate the creep life of FGHAZ with the applied stress above 100 MPa.展开更多
In this study, the effects of Zr-Ti combined deoxidation and AI deoxidation on the impact toughness of coarse- grained heat-affected zone in high-strength low-alloy steels were investigated. More fine oxides were form...In this study, the effects of Zr-Ti combined deoxidation and AI deoxidation on the impact toughness of coarse- grained heat-affected zone in high-strength low-alloy steels were investigated. More fine oxides were formed in the Zr-Ti-killed steel than in Al-killed steel. It was also found that more acicular ferrite grains were formed in the coarse-grained heat-affected zone in the Zr-Ti-killed steel than in Al-killed steel. The impact toughness of coarse-grained heat-affected zone of Zr-Ti-kiUed steel was higher than that of Al-killed steel. The good impact toughness was attributable to the pinning effect of fine oxides and the formation of acicular ferrite grains on fine oxides.展开更多
The mechanical properties and microstructure features of the fine-grained heat-affected zone(FGHAZ) of ASTM4130 steel was investigated by optical microscope(OM),scanning electron microscope(SEM),transmission ele...The mechanical properties and microstructure features of the fine-grained heat-affected zone(FGHAZ) of ASTM4130 steel was investigated by optical microscope(OM),scanning electron microscope(SEM),transmission electron microscope(TEM),and welding thermal simulation test.It is found that serious embrittlement occurs in the FGHAZ with an 81.37% decrease of toughness,compared with that of the base metal.Microstructure analysis reveals that the FGHAZ is mainly composed of acicular,equiaxed ferrite,granular ferrite,martensite,and martensite-austenite(M-A) constituent.The FGHAZ embrittlement is mainly induced by granular ferrite because of carbides located at its boundaries and sub-boundaries.Meanwhile,the existence of martensite and M-A constituent,which distribute in a discontinuous network,is also detrimental to the mechanical properties.展开更多
Because of the size limitation of weld joints in different regions, the traditional standard bar specimen is not suitable to investigate the mechanical properties of weld joints. In this study, miniature specimens wer...Because of the size limitation of weld joints in different regions, the traditional standard bar specimen is not suitable to investigate the mechanical properties of weld joints. In this study, miniature specimens were extracted from specific regions(base metal, weld metal, and three heat-affected zones) of API X80 and X70 weld joints. Uniaxial tensile tests were conducted to obtain the mechanical properties of different regions, and then uniaxial ratcheting tests were conducted to investigate the ratcheting behaviors of the different regions under the same peak and nominal stresses. Under both the tensile tests and ratcheting tests, the weld joints exhibit heterogeneous results, such as different mechanical properties and ratcheting behaviors, which were region dependent. Furthermore, the yield strength and yield-to-tensile strength ratio contribute differently to the ratcheting response.展开更多
The structure-property relationship in heat-affected zone (HAZ)of a low-carbon steel bearing V-N subjected to gasshielded arc welding was explored.The microstructural characteristics of base metal (BM),coarse-grained ...The structure-property relationship in heat-affected zone (HAZ)of a low-carbon steel bearing V-N subjected to gasshielded arc welding was explored.The microstructural characteristics of base metal (BM),coarse-grained HAZ (CGHAZ),fine-grained HAZ,and intercritical HAZ were significantly different.The effect of grain-refinement strengthening and transformation hardening on HAZ contributed to equivalent hardness of 260.8-278.5 HV in comparison with BM hardness of 272.0 HV.Moreover,excellent impact toughness at -20 ℃ was obtained because of high resistance to crack propagation by high-misorientation boundaries,leading to impact fracture consisting of dimples.In CGHAZ,free N was partly fixed by V(C,N)precipitates,such that the deterioration effect of N on toughness was considered to be nearly eliminated.In comparison with CGHAZ,weld metal contained higher fraction of acicular ferrite with fine plates,while the impact toughness was inferior because of the detrimental influence of coarse inclusions from the welding wire.The nanoscale V(C,N)precipitates in CGHAZ had weak effect on toughness because of small size.展开更多
800 MPa grade new ultra-low carbon bainitic (NULCB) steel is the recently developed new generation steel. The microstructure in the coarse-grained heat affected zone (CGHAZ) of NULCB steel under laser welding cond...800 MPa grade new ultra-low carbon bainitic (NULCB) steel is the recently developed new generation steel. The microstructure in the coarse-grained heat affected zone (CGHAZ) of NULCB steel under laser welding conditions was investigated by thermal simulation. The influence of the cooling time from 800℃ to 500℃.t8/5 (0.3-30 s), on the microstructure of the CGHAZ was discussed. The experimental results indicate that the microstructnre of the CGHAZ is only the granular bainite which consists of bainitic ferrite (BF) lath and M-A constituent while t8/5 is 0.3-30 s. The M-A constituent consists of twinned martensite and residual austenite, and the change of the volume fraction of the residual austenite in the M-A constituent is very small when t8/5 is between 0.3 and 30 s. The morphology of the M-A constituent obviously changes with the variation of t8/5.As t8/5 increases, tile average width, gross and shape parameter of the M-A constituent increase, while the line density of the M-A constituent decreases.展开更多
The intercritical heat-affected zone(ICHAZ) of X80 pipeline steel was simulated by using the Gleeble-3500thermal/mechanical simulator according to the thermal cycle of in-service welding.The microstructures of ICHAZ...The intercritical heat-affected zone(ICHAZ) of X80 pipeline steel was simulated by using the Gleeble-3500thermal/mechanical simulator according to the thermal cycle of in-service welding.The microstructures of ICHAZ with different cooling rates were examined,and the hardness,the toughness and corresponding fractography were investigated.Results show that untransformed bainite and ferrite as well as retransformed fine bainite and martensite–austenite(M–A)constituents constitute the microstructure of ICHAZ.The two different morphologies of M–A constituents are stringer and block.Second phase particles which mainly composed of Ti,Nb,C,Fe and Cu coarsened in ICHAZ.Compared with normal welding condition,the toughness of ICHAZ is poor when the cooling time is short under in-service welding condition because of the large area fraction and size of M–A constituents that connect into chains and distribute at the grain boundaries.The Vickers hardness of ICHAZ that decreases with the increase in the cooling time is independent with the area fraction of M–A constituents.展开更多
The tenacity of heat-affected zone (HAZ) will decline and the size of grains will increase, because of the overheating on HAZ when submerged are welding (SAW) is ased to thick plate with high heat input. The shapi...The tenacity of heat-affected zone (HAZ) will decline and the size of grains will increase, because of the overheating on HAZ when submerged are welding (SAW) is ased to thick plate with high heat input. The shaping will worsen when SAW is used to thin plate with high current at high speed. A new SAW technology, the pulsed direct current (DC) automatic SAW, will be put forward in this paper in order to overcome the above shortcomings. And a pulsed controller with micro-controller unit (MCU) as the core, nixie tube (NT) and keyboard as the man-machine conversation interface is developed. The main functions of the pulsed controller include the output of pulsed welding current and the working with twinwire. The research has widely prospects in application with significant meanings in theory and practical engineering.展开更多
Expulsion is an undesired event during resistance spot welding because the weld quality deteriorates. It is the ejection of molten metal from the weld nugget which usually occurs due to applying a high current for a s...Expulsion is an undesired event during resistance spot welding because the weld quality deteriorates. It is the ejection of molten metal from the weld nugget which usually occurs due to applying a high current for a short welding time. Expulsion has a significant impact on the final yield strength of the weld, thus the detection and characterization of expulsion events is significant for the quality assurance of resistance spot welds. In this study, hardness mapping, using a scanning hardness machine, was used as a quality assurance technique for re- sistance spot welding. Hardness tests were conducted on a resistance spot welded sample to prepare a hardness map. The test results showed good correlation between the hardness map and metallographic cross sections. The technique also provided further fundamental understand- ing of the resistance spot welding process, especially regarding the occurrence of expulsion in the nugget.展开更多
基金This work was financially supported by the Major State Basic Research Development Program of China (No.1998061500)
文摘800 MPa grade ultralow carbon bainitic (NULCB) steel is the recently developed new generation steel, which was produced by thermo mechanical controlled processing & relaxation-precipitation controlling transformation (TMCP&RPC) tech- nique. The microstructure and the mechanical properties of the heat-affected zone (HAZ) in NULCB steel under laser welding conditions were investigated by using a Gleeble-1500 thermal simulator. The experimental results indicate that the simplex microstructure in the HAZ is granular bainite that consists of bainite-ferrite (BF) lath and M-A constituent when the cooling time from 800 to 500℃ (t8/5) is 0.3-30 s, and the M-A constituent consists of twinned martensite and residual austenite. As t8/5 increases, the hardness and tensile strength of HAZ decreases, but they are higher than that of the base metal, indicating the absence of softened zone after laser welding. The impact toughness of HAZ increases at first and then decreases when t8/5 increases. The impact energy of HAZ is much higher than that of the base metal when t8/5 is between 3 and 15 s. It indicates that excellent low temperature toughness can be obtained under appropriate laser welding conditions.
文摘The microstructure evolution of heat-affected zone (HAZ) in the multi-pass underwater welded joints is investigated in the present work, and it can be characterized by four zones, marked as Region A, B, C and D, respectively. The microstructure in Region A is the mixture of lath martensite and residual austenite. Besides this structure, lots of acicular ferrite appears in Region B as well, and the grain size becomes larger. Lath ferrite combined with granular bainite is observed in Region C. In Region D, tempered sorbite, granular bainite and fine acicular ferrite are found within the grains, while massive ferrite and Widmanstatten structure are distributed along the grain boundary: The thermal effect of multi-pass welding makes the microstructure and property more and more uniform in the ttAZ, and the largest hardness 356 HV in the HAZ appears in Region A.
文摘The main aim of this study was to investigate liquation cracking in the heat-affected zone(HAZ)of the IN939 superalloy upon tungsten inert gas welding.A solid solution and age-hardenable filler metals were further studied.On the pre-weld heat-treated samples,upon solving the secondaryγ′particles in the matrix,primaryγ′particles in the base metal grew to"ogdoadically diced cubes"of about 2μm in side lengths.The pre-weld heat treatment reduced the hardness of the base metal to about HV 310.Microstructural studies using optical and fieldemission scanning electron microscopy revealed that the IN939 alloy was susceptible to liquation cracking in the HAZ.The constitutional melting of the secondary,eutectic,and Zr-rich phases promoted the liquation cracking in the HAZ.The microstructure of the weld fusion zones showed the presence of fine spheroidalγ′particles with sizes of about 0.2μm after the post-weld heat treatment,which increased the hardness of the weld pools to about HV 350 and 380 for the Hastelloy X and IN718 filler metals,respectively.Application of a suitable solid solution filler metal could partially reduce the liquation cracking in the HAZ of IN939 alloy.
文摘Fracture parameters of welded joints with different strength matching and crack depth in weld metal are investigated by using the methods of elastoplastic finite element analysis and three point bend specimen test. The results show that for shallow crack, the plastic zone turns large in loading process, and the fracture toughness turns high. The extent of the plastic zone of overmatched joint is larger than that of undermatched joint because it will extends to parent metal from the weld metal in loading process for the same CTOD value. The plastic zone of undermatched joint is restricted within the weld, and the size of that is small. Overmatched joint shows the fracture behaviour of shallow crack may more easily than the undermatched joint, while the two sorts of joint specimens have the same crack depth. Therefore, the fracture-resistant capability of overmatched weld is better than that of undermatched weld. when the toughness of weld metals is similar for both overmatched and undermatched joints.
基金Project (20080430997) supported by the Postdoctoral Science Foundation of China
文摘The simulated fine grained heat-affected zone (FGHAZ) specimens for P92 welded joints were prepared by heat treatment, then the creep tests were carried out at 650 ℃ under the applied stress of 90-120 MPa to investigate high-temperature creep behavior of FGHAZ. The results show that the creep property of FGHAZ is much inferior to that of the base metal, which exhibits the much higher steady creep rate and shorter time to creep fracture. The power law equation can describe the steady creep rate dependence on applied stress, indicating that the stress exponent n of FGHAZ is distinguished between two regions with n=15.1 at high stresses (more than 100 MPa) and n=8.64 at lower stresses. Based on Monkman-Grant equation, the relationship between the secondary creep rate and time to rupture is obtained to evaluate the creep life of FGHAZ with the applied stress above 100 MPa.
基金This work was supported by the China Postdoctoral Science Foundation C Grant No. 2014M550414 ) and the National Natural Science Foundation of China ( Grant No. 51401152).
文摘In this study, the effects of Zr-Ti combined deoxidation and AI deoxidation on the impact toughness of coarse- grained heat-affected zone in high-strength low-alloy steels were investigated. More fine oxides were formed in the Zr-Ti-killed steel than in Al-killed steel. It was also found that more acicular ferrite grains were formed in the coarse-grained heat-affected zone in the Zr-Ti-killed steel than in Al-killed steel. The impact toughness of coarse-grained heat-affected zone of Zr-Ti-kiUed steel was higher than that of Al-killed steel. The good impact toughness was attributable to the pinning effect of fine oxides and the formation of acicular ferrite grains on fine oxides.
基金supported by the National High-Tech Research and Development Program of China (No.2006AA09A103-6)
文摘The mechanical properties and microstructure features of the fine-grained heat-affected zone(FGHAZ) of ASTM4130 steel was investigated by optical microscope(OM),scanning electron microscope(SEM),transmission electron microscope(TEM),and welding thermal simulation test.It is found that serious embrittlement occurs in the FGHAZ with an 81.37% decrease of toughness,compared with that of the base metal.Microstructure analysis reveals that the FGHAZ is mainly composed of acicular,equiaxed ferrite,granular ferrite,martensite,and martensite-austenite(M-A) constituent.The FGHAZ embrittlement is mainly induced by granular ferrite because of carbides located at its boundaries and sub-boundaries.Meanwhile,the existence of martensite and M-A constituent,which distribute in a discontinuous network,is also detrimental to the mechanical properties.
基金supported by the National Natural Science Foundation of China (No. 51435012)
文摘Because of the size limitation of weld joints in different regions, the traditional standard bar specimen is not suitable to investigate the mechanical properties of weld joints. In this study, miniature specimens were extracted from specific regions(base metal, weld metal, and three heat-affected zones) of API X80 and X70 weld joints. Uniaxial tensile tests were conducted to obtain the mechanical properties of different regions, and then uniaxial ratcheting tests were conducted to investigate the ratcheting behaviors of the different regions under the same peak and nominal stresses. Under both the tensile tests and ratcheting tests, the weld joints exhibit heterogeneous results, such as different mechanical properties and ratcheting behaviors, which were region dependent. Furthermore, the yield strength and yield-to-tensile strength ratio contribute differently to the ratcheting response.
基金the National Natural Science Foundation of China (Grant No.51604072)the Fundamental Research Funds for the Central Universities (Grant No.N170704016)the National High-Tech R&D Program (863 Program)of China (Grant No.2015AA03A501).
文摘The structure-property relationship in heat-affected zone (HAZ)of a low-carbon steel bearing V-N subjected to gasshielded arc welding was explored.The microstructural characteristics of base metal (BM),coarse-grained HAZ (CGHAZ),fine-grained HAZ,and intercritical HAZ were significantly different.The effect of grain-refinement strengthening and transformation hardening on HAZ contributed to equivalent hardness of 260.8-278.5 HV in comparison with BM hardness of 272.0 HV.Moreover,excellent impact toughness at -20 ℃ was obtained because of high resistance to crack propagation by high-misorientation boundaries,leading to impact fracture consisting of dimples.In CGHAZ,free N was partly fixed by V(C,N)precipitates,such that the deterioration effect of N on toughness was considered to be nearly eliminated.In comparison with CGHAZ,weld metal contained higher fraction of acicular ferrite with fine plates,while the impact toughness was inferior because of the detrimental influence of coarse inclusions from the welding wire.The nanoscale V(C,N)precipitates in CGHAZ had weak effect on toughness because of small size.
文摘800 MPa grade new ultra-low carbon bainitic (NULCB) steel is the recently developed new generation steel. The microstructure in the coarse-grained heat affected zone (CGHAZ) of NULCB steel under laser welding conditions was investigated by thermal simulation. The influence of the cooling time from 800℃ to 500℃.t8/5 (0.3-30 s), on the microstructure of the CGHAZ was discussed. The experimental results indicate that the microstructnre of the CGHAZ is only the granular bainite which consists of bainitic ferrite (BF) lath and M-A constituent while t8/5 is 0.3-30 s. The M-A constituent consists of twinned martensite and residual austenite, and the change of the volume fraction of the residual austenite in the M-A constituent is very small when t8/5 is between 0.3 and 30 s. The morphology of the M-A constituent obviously changes with the variation of t8/5.As t8/5 increases, tile average width, gross and shape parameter of the M-A constituent increase, while the line density of the M-A constituent decreases.
基金supported by Key Project of Tianjin Municipal Science and Technology Support Program (No.11ZCGYSF00100)Tianjin Natural Science Foundation (No.11JCYBJC06000)the Gansu province Science and Technology Support Program (No.1204GKCA007)
文摘The intercritical heat-affected zone(ICHAZ) of X80 pipeline steel was simulated by using the Gleeble-3500thermal/mechanical simulator according to the thermal cycle of in-service welding.The microstructures of ICHAZ with different cooling rates were examined,and the hardness,the toughness and corresponding fractography were investigated.Results show that untransformed bainite and ferrite as well as retransformed fine bainite and martensite–austenite(M–A)constituents constitute the microstructure of ICHAZ.The two different morphologies of M–A constituents are stringer and block.Second phase particles which mainly composed of Ti,Nb,C,Fe and Cu coarsened in ICHAZ.Compared with normal welding condition,the toughness of ICHAZ is poor when the cooling time is short under in-service welding condition because of the large area fraction and size of M–A constituents that connect into chains and distribute at the grain boundaries.The Vickers hardness of ICHAZ that decreases with the increase in the cooling time is independent with the area fraction of M–A constituents.
文摘The tenacity of heat-affected zone (HAZ) will decline and the size of grains will increase, because of the overheating on HAZ when submerged are welding (SAW) is ased to thick plate with high heat input. The shaping will worsen when SAW is used to thin plate with high current at high speed. A new SAW technology, the pulsed direct current (DC) automatic SAW, will be put forward in this paper in order to overcome the above shortcomings. And a pulsed controller with micro-controller unit (MCU) as the core, nixie tube (NT) and keyboard as the man-machine conversation interface is developed. The main functions of the pulsed controller include the output of pulsed welding current and the working with twinwire. The research has widely prospects in application with significant meanings in theory and practical engineering.
文摘Expulsion is an undesired event during resistance spot welding because the weld quality deteriorates. It is the ejection of molten metal from the weld nugget which usually occurs due to applying a high current for a short welding time. Expulsion has a significant impact on the final yield strength of the weld, thus the detection and characterization of expulsion events is significant for the quality assurance of resistance spot welds. In this study, hardness mapping, using a scanning hardness machine, was used as a quality assurance technique for re- sistance spot welding. Hardness tests were conducted on a resistance spot welded sample to prepare a hardness map. The test results showed good correlation between the hardness map and metallographic cross sections. The technique also provided further fundamental understand- ing of the resistance spot welding process, especially regarding the occurrence of expulsion in the nugget.