HPLC法测定天麻头风灵颗粒中阿魏酸的含量

目的建立HPLC测定天麻头风灵颗粒中阿魏酸含量的方法。方法采用高效液相色谱法,固定相为Diamonsil ODS C18色谱柱(250mm×4.6mm,5μm),流动相为甲醇-乙腈-1%冰乙酸(14∶14∶72),检测波长为316nm,流速为1.0ml/min。结果阿魏酸在2.13～17.04μg/ml范围内与峰面积线性良好(r=0.9999,n=6);平均加样回收率为99.81%,RSD=1.52%(n=6)。结论本方法简便,准确,可靠,灵敏度高,重现性好,可用于天麻头风灵颗粒的质量控制。

“伪造”天象与《隋书·天文志》的执笔意图——袁充相关史事辨析

在《隋书·袁充传》的记事中,太史令袁充上奏炀帝的诸条天象为“假托天文”、“变动星占”,即伪造。当时及后世均对袁充多有批评。但根据现代天文学手段计算,袁充上奏中可考的部分均基本符合史实,并非随意捏造。袁充上奏的天象为实,只是他避重就轻,粉饰占辞,以谄媚炀帝。其性质并非天象上的造伪,而是解释上的附会。同一天象,《天文志》与《袁充传》的占辞完全相反,这是由于《天文志》占辞为撰者李淳风根据占书推算的结果,而非当时太史监的解释。李淳风的执笔意图有两个方面:一是后见之明的不自觉解释,二是证明隋亡的天意及李唐的正统。

Statistical and causes analysis of storm surges along Tianjin coast during the past 20 years

Based on tidal data statistical analysis for 20 years of Tanggu Marine Environmental Monitoring Station from 1991 to 2010, we concluded that an average of nearly 10 days of 100 cm above water increase took place at Tianjin coast every year. The maximum high tide and average tide of Tianjin coast occurred in summer and autumn, and the maximum water increase also occurred in summer and autumn. Days with water increase more than 100 cm mostly occurred in spring, autumn and winter. Then we summarized the causes of coastal storm surge disaster in Tianjin based on astronomical tide factors, meteorological factors, sea level rise, land subsidence, and geographic factors, et al. Finally, we proposed storm surge disaster prevention measures.

Determination of Griffonilide in Roots of Semiaquilegia adoxoides by RP-HPLC

Aim To establish the method for determination of benzofuranones derivative, griffonilide, in the roots of Semiaquilegia adoxoides （DC.） Makino by RP- HPLC. Methods Kromasil C18 column was used with a mobile phase of methanol-water （ containing 0. 01% trifluoroacetic acid and 0. 05 % tetrahydrofuran） （3：97）. The detecting wavelength was 260 nm. Results The calibration curve was linear over the range of 0. 004 - 0. 4 mg·mL^-1 with the correlation coefficient of 1.00 000. The average recovery was 98. 77 % with RSD 2. 77 %. Determinations of ten samples from different areas showed that the contents of griffonilide in the roots of S. adoxoides are 0. 17 -0. 49 mg·g^-1. Conclusion The method provides an accurate and sensitive way to detect griffonilide in the roots of S. adoxoides .

Intensified East Asian summer monsoon and associated precipitation mode shift under the 1.5 ℃ global warming target

In this study, the East Asian summer climate changes under the 1.5 ℃ global warming （1.5 GW） target in 30 simulations derived from 15 coupled models within the Coupled Model Intercomparison Program phase 5 （CMIP5） are examined. Compared with the current summer climate （1975-2005）, both surface air temperature and precipitation increase significantly over the East Asian continent during the 1.5 GW period （average period 2021-2051）. In northeastern China this is particularly pronounced with regional averaged precipitation increases of more than 7.2%, which is greater than that for the whole East Asian continent （approximately 4.2%）. Due to stronger enhancement of precipitation north of 40°N, the leading empirical orthogonal function （EOF） mode of summer precipitation over the East Asian continent changes from tripolar-like mode to dipole mode. As there is stronger surface warming over the East Asian continent than that over surrounding ocean, the land-sea thermal contrast is enhanced during the 1.5 GW period. As a result, the monsoon circulation in the lower troposphere is significantly strengthened, which causes the increased summer precipitation over the East Asian continent. In addition, larger interannual variabilities of East Asian summer monsoon circulation and associated precipitation are also suggested for the 1.5 GW period.

Ambulatory blood-pressure monitoring, antihypertensive therapy and the risk of fall injuries in elderly hypertensive patients

Background Fall injuries are common among the elderly. The aim of this study was to investigate whether blood-pressure patterns, as measured by 24-h ambulatory blood pressure monitoring （ABPM）, or intensification of antihypertensive therapy following the 24-h ABPM, may be associated with fall injuries in hypertensive elderly patients. Methods In a retrospective study, community-based elderly patients （age ≥ 70 years） who were referred to 24-h ABPM were evaluated for fall injuries within one-year post-ABPM. We compared the clinical characteristics, 24-h ABPM patterns and the intensification of hypertensive therapy following 24-h ABPM, between patients with and without a fall injury. Results Overall 1032 hypertensive elderly patients were evaluated. Fifty-five （5.3%） had a fall injury episode in the year following ABPM. Patients with a fall injury were significantly older, and with higher rates of previous falls. Lower 24-h diastolic blood-pressure （67.3 ± 7.6 vs. 70.7 ± 8.8 mmHg; P 〈 0.005） and increased pulse-pressure （74.7 ± 14.3 vs. 68.3 ± 13.7 mmHg; P 〈 0.005）, were found in the patients with a fall injury, compared to those without a fall injury. After adjustment for age, gender, diabetes mellitus and previous falls, lower diastolic blood-pressure and increased pulse-pressure were independent predictors of fall injury. Intensification of antihypertensive treatment following the 24-h ABPM was not associated with an increased rate of fall injury. Conclusions Low diastolic blood-pressure and increased pulse-pressure in 24-h ABPM were associated with an increased risk of fall injury in elderly hypertensive patients. Intensification of antihypertensive treatment following 24-h ABPM was not associated with an increased risk of fall injury.

REASONS FOR THE LATE ONSET AND ANOMALOUS SOUTHWARD PERSISTENCE OF THE SOUTH CHINA SEA SUMMER MONSOON IN 2005

Features of atmospheric circulation and thermal structures are discussed using the NCAR/NCEP data to reveal the reasons for the late onset and anomalous southward persistence of the South China Sea Summer Monsoon(SCSSM) in 2005.The results show that three factors are crucial.First,a strong Arabian High overlaps with a high-latitude blocking high and channels strong cold air to southern Asia.Second,the Tibetan Plateau has a bigger snow cover than usual in spring and the melting of snow cools down the surface.Third,the Somali Jet breaks out at a much later date,being not conducive to convection over Indochina.The former two factors restrict atmospheric sensible heating over the Tibetan Plateau and nearby regions while the third one limits latent heating over Indochina.All of the factors slow down atmospheric warming and postpone the onset of SCSSM.Long after the onset of SCSSM,strong cold air over India advances the Southwest Monsoon northward slowly,resulting in weaker convection and latent heating over the Tibetan Plateau and nearby areas.The negative feedback conversely inhibits further northward movement of Southwest Monsoon.

CONNECTION OF THE SOUTH CHINA SEA SUMMER MONSOON TO MARITIME CONTINENT CONVECTION AND ENSO

The relationship between the intensity of the South China Sea summer monsoon （SCSSM） and the Nino3.4 index and anomalous atmospheric circulation patterns associated with a strong and weak SCSSM are investigated using the NCEP/NCAR reanalysis data, Extended Reconstructed Sea Surface Temperature （ERSST） data and Climate Prediction Center Merged Analysis of Precipitation （CMAP） data. The SCSSM is significantly positively correlated with the Nino3.4 index in the succeeding northern autumn and winter. In the strong minus weak SCSSM composite, a positive East Asia-Pacific teleconnection （EAP） pattern and a negative Europe-Asian-Pacific teleconnection （EUP） pattern appear in the 500 hPa height difference field; low-level cross-equatorial flows are strengthened over the Maritime Continent （MC） region; positive （negative） precipitation anomalies occur in the South China Sea and western north Pacific （MC）. A possible mechanism through which SCSSM affects ENSO is proposed. A strong （weak） SCSSM strengthens （weakens） cross-equatorial flows over the MC. The anomalous cross-equatorial flows cool （warm） the SST around the MC through enhanced （reduced） surface latent heat fluxes. The cooling （warming） further leads to suppressed （enhanced） convection over the MC, and causes the anomalous westerly （easterly） in the equatorial western Pacific, which favors the onset of E1 Nino （La Nina） through modulating the positive air-sea feedback process.

THE RELATIONSHIP OF THE PRECEDING WINTER MJO ACTIVITIES AND THE SUMMER PRECIPITATION IN YANGTZE-HUAIHE RIVER BASIN OF CHINA

The first two series(RMM1 and RMM2) of RMM Index(all-Season Real-time Multivariate MJO Index) are computed to obtain the interannual variation of the preceding winter(preceding December to current February) MJO strength,according to which active(or inactive) years of preceding winter MJO are divided.By utilizing the data provided by NCEP/NCAR,CMAP and China's 160 stations from 1979 to 2008,we studied the preceding winter MJO strength and discovered that the summer precipitation in the basin are of significantly negative correlation,i.e.when the preceding winter MJO is relatively active,the summer precipitation in the basin decreases,and vise verse.We also analyzed the causes.When the preceding winter MJO is relatively active,its release of potential heat facilities Inter-Tropical Convergence Zone(ITCZ) to strengthen and locate northward in winter and propagate northeastward.This abnormal situation lasts from winter to summer.In mid-May,ITCZ jumps northward to the South China Sea,the western Pacific subtropical high withdraws eastward,and the South China Sea summer monsoon sets off and strengthens.In summer,ITCZ propagates to South China Sea-subtropical western Pacific,the zonal circulation of subtropical Pacific strengthens,and a local meridional circulation of the South China Sea to the basin area forms,giving rise to the East Asia Pacific teleconnection wave-train.An East Asian monsoon trough and the Meiyu front show opposite features from south to north,the East Asian summer monsoon strengthens and advances northward.As a result,the summer monsoon is weakened as the basin is controlled by the subtropical high continually,with less rain in summer.On the contrary,when the preceding winter MJO is inactive,ITCZ weakens and is located southward,the subtropical high is located southward in summer,and the basin is in a region of ascending airflow with prevailing southwest wind.The East Asian monsoon trough and EASM weaken so that summer monsoon is reduced in the basin where precipitation increases.

NUMERICAL SIMULATION OF SOUTH CHINA SEA MONSOON ONSET BASED ON GRAPES MODEL AND EXPERIMENTS ON INITIAL MODEL FIELDS

The Global and Regional Assimilation and Prediction System (GRAPES), a limited-area regional model, was used to simulate the onset of South China Sea summer monsoon. In view of the relatively insufficient information about the initial field in simulation predictions, the Advanced Microwave Sounding Unit-B (AMSU-B) data from a NOAA satellite were introduced to improve the initial values. By directly using the 3-dimensional variational data assimilation system of GRAPES, two schemes for assimilation tests were designed. In the design, Test 1 (T1) assimilates both sounding and AMSU-B data, and Test 2 (T2) assimilates only the conventional sounding data, before applying the model in simulation forecasts. Comparative experiments showed that the model was very sensitive to initial fields and successful in reproducing the monsoon onset, allocation of high- and low-level wind fields during the pentad of onset, and the northward advancement of the monsoon and monsoon rain bands. The scheme, however, simulated rainfall and the location of the subtropical high with deviations from observations. The simulated location of the subtropical high was more westward and northward and the simulated rainfall for the South China Sea was larger and covered a broader area.

QUALITY CONTROL OF SINGLE DOPPLER RADAR DATA AND RETRIEVAL OF HORIZONTAL WIND FOR A LANDING TYPHOON

The removal of noise and velocity ambiguity and retrieval and verification of horizontal wind field is a prerequisite to make the best and fullest use of Doppler radar measurements. This approach was applied to the Doppler radar data collected during August 2005 for a landing typhoon Matsa (0509) in Yantai, Shangdong Province, and the verified result shows that the quality control for this dataset was successful. The horizontal wind field was retrieved and then verified by studying the characteristics of the radar radial velocity and large-scale wind field and the vertical cross section of the radial velocity determined with the typhoon center as the circle center and comparing it with satellite imagery. The results show that the meso- and small-scale systems in Matsa and its horizontal and vertical structure could be clearly retrieved using the dataset collected by single Doppler radar, and a shear or a convergence was corresponding with a band of severe storm around Matsa. At the same time, the retrieved wind field from single Doppler radar is proved to be a reliable and high-resolution dataset in analyzing the inner meso-scale structure of Matsa. It is also proved that the method for removing the velocity ambiguity could be an effective approach for preliminary quality control of the Doppler radar data, and the VAP method could also be a reasonable solution for the analysis of mesoscale wind field.

CLIMATOLOGICAL VARIATION FEATURES OF TYPHOON PRECIPITATION INFLUENCING FUJIAN FOR THE PAST 46 YEARS

The results of an analysis of the temporal and spatial distribution of typhoon precipitation influencing Fujian from 1960 to 2005 show that typhoon precipitation in Fujian province occurs from May to November, with the most in August. There has been a decreasing trend since 1960. Typhoon precipitation gradually decreases from the coastal region to the northwestern mainland of Fujian and the maximum typhoon precipitation occurs in the northeast and the south of Fujian. Typhoon torrential rain is one of the extreme rainfall events in Fujian. High frequencies of typhoon torrential rain occur in the coastal and southwest regions of the province. With the impact of Fujian＇s terrain, typhoon precipitation occurs more easily to the east of the mountains than to the west. Atmospheric circulation at 500 hPa over Asia and sea surface temperature anomalies of the equatorial eastern Pacific are analyzed, with the finding that they are closely connected with the anomaly of typhoon precipitation influencing Fujian, possibly mainly by modulating the northbound track of typhoons via changing the atmosphere circulation to lead to the anomaly of typhoon precipitation over the province

CLIMATIC CHARACTERISTICS OF TYPHOON PRECIPITATION OVER CHINA

The spatio-temporal characteristics of typhoon precipitation over China are analyzed in this study. The results show that typhoon precipitation covers most of central-eastern China. Typhoon precipitation gradually decreases from the southeastern coastal regions to the northwestern mainland. The maximum annual typhoon precipitation exceeds 700 mm in central-eastern Taiwan and part of Hainan, while the minimum annual typhoon precipitation occurs in parts of Inner Mongolia, Shanxi, Shaanxi and Sichuan, with values less than 10 mm. Generally, typhoons produce precipitation over China during April - December with a peak in August. The annual typhoon precipitation time series for observation stations are examined for long-term trends. The results show that decreasing trends exist in most of the stations from 1957 to 2004 and are statistically significant in parts of Taiwan, Hainan, coastal Southeast China and southern Northeast China. The anomaly of typhoon precipitation mainly results from that of the general circulation over Asia and the Walker Cell circulation over the equatorial central and eastern Pacific. Typhoon torrential rain is one of the extreme rainfall events in the southeastern coastal regions and parts of central mainland. In these regions, torrential rains are mostly caused by typhoons.

DEVELOPMENT FOR HIGH PRECISION SIX COMPONENT STRAIN GAUGE BALANCE

The measurement accuracy of a wind tunnel balance is the key factor to improve the measurement accuracy for a test model in the wind tunnel. In order to improve the measurement accuracy of the wind tunnel balance, a great deal of investigation is carried out in China. This paper summarizes a program to improve the measurement accuracy of wind tunnel balances. In the program, the investigation is carried out in three aspects (1) designing a drag component of the balance in low interactions (2) choosing high quality foil strain gauges with temperature self-compensation (3) choosing the excellent gauges and mounting them meticulously. As an example, these research achievements are applied in a φ18 six component balance. The measurement accuracy of a GB-04 standard model in a transonic wind tunnel with the φ18 six component balance comes up to the advanced world standard.

A Study on Snowstorm Weather in Coastal Area of Western Antarctic

In this paper, based on the observational data of 1995 in the Chinese Antarctic Great Wall Station the snowstorm is studied synoptically. It is found that there are two kinds of snowstorms with different physical characteristics and that the happening of snowstorm is always accompanied by a near-ground level inversion layer. The function of the inversion layer is analyzed, too. It is indicated that the strong ESE-wind type snowstorm is mainly caused by katabatic wind and gradient wind together. This idea is new and different from the general concept that there is no katabatic wind in the western Antarctic area.

A COMPREHENSIVE ANALYSIS OF INTERACTIONS BETWEEN MESO-SCALE CONVECTIVE CLOUD CLUSTERS IN TYPHOONS AND MESOSCALE HEAVY RAINS

In this paper, time and space distribution regularity of meso-scale heavy rains in five selected typhoons which landed at Fujian from 1996 to 1998 has been analyzed. Besides, with hourly digitized satellite infrared imagery, the features of the mesoscale are revealed for the genesis and evolution of mesoscale convective systems in typhoons. It indicates that the intensity of mesoscale storms is closely connected with the temperature and the area of the coldest cloud cluster. The heavy rainfall usually emerges on the eastern side of the mesoscale convective cloud clusters, where the cloud mass is developing and with a dense gradient and big curvature of isoline of the cloud top temperature.

A STUDY ON VARIABLE QUANTITATIVE PRECIPITATION ESTIMATION USING DOPPLER RADAR DATA

With the pros and cons of the traditional optimization and probability pairing methods thoroughly considered, an improved optimal pairing window probability technique is developed using a dynamic relationship between the base reflectivity Z observed by radar and real time precipitation I by rain gauge. Then, the Doppler radar observations of base reflectivity for typhoons Haitang and Matsa in Wenzhou are employed to establish various Z-I relationships, which are subsequently used to estimate hourly precipitation of the two typhoons. Such estimations are calibrated by variational techniques. The results show that there exist significant differences in the Z-I relationships for the typhoons, leading to different typhoon precipitation efficiencies. The typhoon precipitation estimated by applying radar base reflectivity is capable of exhibiting clearly the spiral rain belts and mesoscale cells, and well matches the observed rainfall. Error statistical analyses indicate that the estimated typhoon precipitation is better with variational calibration than the one without. The variational calibration technique is able to maintain the characteristics of the distribution of radar-estimated typhoon precipitation, and to significantly reduce the error of the estimated precipitation in comparison with the observed rainfall.

Seasonal Prediction Assessment of the South Asian Summer Monsoon: ENSEMBLES versus DEMETER

The seasonal forecasting skill with respect to the South Asian summer monsoon(SASM) was compared between the European Commission FP7 project(ENSEMBLES) and the Development of a European Multimodel Ensemble System for Seasonal to Interannual Prediction project(DEMETER). The Webster-Yang index(WYI) was chosen to represent the intensity of the SASM. First, the authors compared the ability to forecast the zonal wind at 850 h Pa(U850) and 200 h Pa(U200) between ENSEMBLES and DEMETER models. The results indicated that the models from the European Centre for Medium-Range Weather Forecasts, International Organization(ECMWF) and UK Met Office(UKMO) in ENSEMBLES possess greater skill in seasonally forecasting the JJA(June, July, and August) U850, U200, and U850 minus U200 than in DEMETER. Compared to in DEMETER, the JJA U200 and U850 minus U200 forecasting skill was greater for the model from MétéoFrance(MF) in ENSEMBLES over most of the SASM region. The three coupled models(ECMWF, MF, and UKMO), especially the UKMO model in ENSEMBLES, all demonstrated improved skill in their seasonal forecasts compared to in DEMETER with respect to the interannual variability of the SASM. The three ENSEMBLES models also showed better ability in forecasting the sea surface temperature anomalies(SSTAs) over the eastern equatorial Pacific and North Indian Ocean, and more accurately reproduced the large-scale atmospheric circulation and precipitation over northern India, which are related to the SASM. It seems that the couple between the atmospheric system and external forcing of ENSMBLES over Indian Ocean and Pacific is better than that of DEMETER.