The effects of strain rate on the microstructural evolution and deformation mechanism of a Ni-Co based superalloy were investigated by isothermal compression tests performed atγ'sub-solvus(1090℃)andγ'super-...The effects of strain rate on the microstructural evolution and deformation mechanism of a Ni-Co based superalloy were investigated by isothermal compression tests performed atγ'sub-solvus(1090℃)andγ'super-solvus temperatures(1150℃)with a wide strain rate range from 0.001 to 10 s^(-1)under a true strain of 0.693.Electron backscatter diffraction(EBSD),electron channeling contrast imaging(ECCI)and transmission electron microscope(TEM)techniques were used to characterize the microstructures.The results revealed that the dynamic recrystallization(DRX)volume fraction increased and stored energy of theγ'matrix grains decreased with increasing the strain rate duringγ'sub-solvus temperature deformation,while the opposite phenomena were observed duringγ'super-solvus temperature deformation.The comprehensive effect of initial grain size,primaryγ'phase,twins and adiabatic temperature rise led to these results.The primaryγ'particles undergone the deformation behavior within itself and obviously accelerated the DRX of the matrix.The microstructural evolution proved that discontinuous dynamic recrystallization(DDRX)was the dominant mechanism during the hot deformation carried out at bothγ'sub-solvus andγ'super-solvus temperatures.Primaryγ'particles obviously accelerated the nucleation step and retarded the growth step of DDRX duringγ'sub-solvus temperature deformation.Besides,the acceleration effect of primaryγ'particles on DDRX increased with the increase of strain rate.Continuous dynamic recrystallization(CDRX)was confirmed to be an assistant mechanism duringγ'super-solvus temperature deformation and was promoted with the increase of strain rate.展开更多
The temperature changes at the rim,1/2 radius,and bore of the turbine disk during the solution treatment were measured.Based on the measured temperature data,solution treatment experiments with different cooling rates...The temperature changes at the rim,1/2 radius,and bore of the turbine disk during the solution treatment were measured.Based on the measured temperature data,solution treatment experiments with different cooling rates(14,51,and 93℃/min)were performed,and the solution temperatures were 1120 and 1080℃.At all three cooling rates,the multimodal size distribution of γ' precipitates was detected,and the size of γ' precipitates is inversely related to the cooling rate.Only the secondary and tertiary γ' precipitates were found at a solution temperature of 1120℃,and the secondary γ' precipitates progressed from spherical(93 and 51℃/min)to flower-like(14℃/min)shape,with the flower-like γ' precipitates regulated by aggregation.At a solution temperature of 1080℃,the γ' precipitates evolve from cuboids(93 and 51℃/min)to irregular shapes(14℃/min).Irregular γ' precipitates are affected by the lattice mismatch between the matrix and the γ' precipitates.展开更多
基金the financial support from the National Natural Science Foundation of China(No.51671189)the Ministry of Science and Technology of China(Nos.2017YFA0700703 and 2019YFA0705304)。
文摘The effects of strain rate on the microstructural evolution and deformation mechanism of a Ni-Co based superalloy were investigated by isothermal compression tests performed atγ'sub-solvus(1090℃)andγ'super-solvus temperatures(1150℃)with a wide strain rate range from 0.001 to 10 s^(-1)under a true strain of 0.693.Electron backscatter diffraction(EBSD),electron channeling contrast imaging(ECCI)and transmission electron microscope(TEM)techniques were used to characterize the microstructures.The results revealed that the dynamic recrystallization(DRX)volume fraction increased and stored energy of theγ'matrix grains decreased with increasing the strain rate duringγ'sub-solvus temperature deformation,while the opposite phenomena were observed duringγ'super-solvus temperature deformation.The comprehensive effect of initial grain size,primaryγ'phase,twins and adiabatic temperature rise led to these results.The primaryγ'particles undergone the deformation behavior within itself and obviously accelerated the DRX of the matrix.The microstructural evolution proved that discontinuous dynamic recrystallization(DDRX)was the dominant mechanism during the hot deformation carried out at bothγ'sub-solvus andγ'super-solvus temperatures.Primaryγ'particles obviously accelerated the nucleation step and retarded the growth step of DDRX duringγ'sub-solvus temperature deformation.Besides,the acceleration effect of primaryγ'particles on DDRX increased with the increase of strain rate.Continuous dynamic recrystallization(CDRX)was confirmed to be an assistant mechanism duringγ'super-solvus temperature deformation and was promoted with the increase of strain rate.
基金supported by the National Science and Technology Major Project(2017-VI-0018-0090).
文摘The temperature changes at the rim,1/2 radius,and bore of the turbine disk during the solution treatment were measured.Based on the measured temperature data,solution treatment experiments with different cooling rates(14,51,and 93℃/min)were performed,and the solution temperatures were 1120 and 1080℃.At all three cooling rates,the multimodal size distribution of γ' precipitates was detected,and the size of γ' precipitates is inversely related to the cooling rate.Only the secondary and tertiary γ' precipitates were found at a solution temperature of 1120℃,and the secondary γ' precipitates progressed from spherical(93 and 51℃/min)to flower-like(14℃/min)shape,with the flower-like γ' precipitates regulated by aggregation.At a solution temperature of 1080℃,the γ' precipitates evolve from cuboids(93 and 51℃/min)to irregular shapes(14℃/min).Irregular γ' precipitates are affected by the lattice mismatch between the matrix and the γ' precipitates.
