The electromagnetic and microwave absorbing properties of FeCoB powder composites prepared by sin- gle-roller melt-spinning and mechanical milling processes were investigated in this paper. The result indicates that t...The electromagnetic and microwave absorbing properties of FeCoB powder composites prepared by sin- gle-roller melt-spinning and mechanical milling processes were investigated in this paper. The result indicates that the flake-like powders are obtained. As milling time increases, the flake-like powder particles tend to agglomerate, causing the flake-like powders decrease gradually. The milling time plays an important role in the electromagnetic parameters which relates to the shape and size of the powder particles. The calculation shows that the sample milled for 6 h could achieve an optimal reflection loss of -11.5 dB at 5.8 GHz, with mass fraction of 83 % and a matching thickness of 1.8 mm. The result also indicates that the microwave absorbing properties of the FeCoB powder composites are adjustable by changing their thickness, and can be applied as a thinner microwave absorbing material in the range of 2-8 GHz.展开更多
Fe73.5Cu1Nb3Si13.5B9 （or FeCuNbSiB） powder/ S-glass fiber-reinforced epoxy composite panels were pre- pared by mold pressing method. Metallographic analysis shows that the amorphous powders are evenly distributed be...Fe73.5Cu1Nb3Si13.5B9 （or FeCuNbSiB） powder/ S-glass fiber-reinforced epoxy composite panels were pre- pared by mold pressing method. Metallographic analysis shows that the amorphous powders are evenly distributed between the layers of S-glass fibers. The effects of the Fe- CuNbSiB powder mass fraction on the complex permittivity, complex permeability, and microwave absorption of the composite panels have been studied in the frequency range of 2.6-18.0 GHz. The complex permittivity of the composite panels with different mass fractions of the FeCuNbSiB powders shows several peaks in the 2.6-18.0 GHz fre- quency range. The complex permeability of the composites decreases with the increasing frequency in the frequency range of 8-18 GHz. The composite with FeCuNbSiB/epoxy mass ratio of 2.5：1.0 has excellent microwave absorption properties of a minimum reflection loss value -30.5 dB at 10.93 GHz for a thickness of 2 mm. A reflection loss exceeding -10 dB can be obtained in a broad frequency range of 3.2-18.0 GHz with a thickness of 1.15-5.00 mm. For the FeCuNbSiB composites, the magnetic loss is the dominant term for microwave absorption. The FeCuNbSiB powders are a possible candidate for high-performance microwave absorption filler.展开更多
Powder metallurgy （P/M） method has mainly been used to produce automobile parts such as self-lubrication beds, shock absorber parts, and gear wheels. In order to investigate the effect of porosity on the mechanical ...Powder metallurgy （P/M） method has mainly been used to produce automobile parts such as self-lubrication beds, shock absorber parts, and gear wheels. In order to investigate the effect of porosity on the mechanical and tribological properties in sintered steel, specimens with 10%, 15%, and 20% porosity were produced in a 10 mm×10 mm×55 mm prismatic shape by pre-alloying powders of the MPIF Fe-C-0.205 alloy used in the production of shock absorber pistons. Sintering was carried out at 900℃ for 45 min in an argon atmosphere. Tensile, charpy, and microhardness tests were performed on these specimens. In addition, the wear performance of a 2% Cu reinforced sintered steel alloy under dry sliding conditions was determined. Metallographic studies such as pore formation, worn surface, and fractured surface analyses were performed by scanning electron microscopy and optical microscopy. The results indicate that irregular pore formation tendencies increase with an increase in porosity （%）. Furthermore, an increase in porosity was shown to decrease the mechanical properties and increase the wear trace area and the friction coefficient of sintered steel.展开更多
BaO-La2O3-B2O3 （BLB） glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the ...BaO-La2O3-B2O3 （BLB） glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the absorbing coat because it is considered to be a good high temperature absorber. The effect of the coating temperature and coating time on the tensile strength of the glass coat was investigated and the proper coating parameters to get good mechanical properties were determined. In addition, the effects of the SiCN content on the tensile strength of the absorbing coat were also discussed. Results show that it is possible to prepare the glass coat using the BLB glass as a binder. That the coat formed at 730℃ for 30 min has the best tensile strength witnesses 730 ℃, 30 min to be the proper parameter to prepare the glass coat. The BLB glass coat without SiCN powder possesses good tensile strength and the introduction of the SiCN absorber into the glass coat will lower the tensile strength. As the SiCN content increases, the tensile strength of the absorbing coat decreases, which could be attributed to the aggregation of SiCN in the coats.展开更多
The effects of types and amounts of silane coupling agent on mechanical properties of vuleanized rubber microwave absorbing patch （VRMAP） were studied. The mechanisms of silane coupling agent＇s effects on mechanica...The effects of types and amounts of silane coupling agent on mechanical properties of vuleanized rubber microwave absorbing patch （VRMAP） were studied. The mechanisms of silane coupling agent＇s effects on mechanical properties of rubber microwave absorbing patch （ RMAP ） and microvave absorbing patch＇s （MAP＇s） mierostrueture were also discussed by using SEM and FT-IR. The experimental results show that the tensile strength of RMAP could be increased through adding the filler of carbonyl iron powder （CIP） modified by silane coupling agent. RMAP fiUed with CIP, which was treated by silane coupling agent KH550, possessed a high tensile strength of 11.5 MPa, which was 448% more than that of MAP whose filler wus not modified by any coupling agent. It was found that the optimal amount of KH550 was 1.0 phr to 100.0 phr carbonyl iron powder. The effects of different modifying techniques on RMAP＇s mechanical properties were also inrestigated. It is indieated that MAP whose filler is modified by the wet process has the highest tensile strength, but it is not the optimal modiifying technique due to complieated wet process. On the contrary, the dry process was very simple, and VRMAP possessed fairly high mechanical properties, therefore, it was the perfect modifying process.展开更多
Results of measurements of permeability, permittivity and radar absorption properties of composites on basis of carbonyl iron particles R-10 brand are presented in this paper. The calculations and experimental studies...Results of measurements of permeability, permittivity and radar absorption properties of composites on basis of carbonyl iron particles R-10 brand are presented in this paper. The calculations and experimental studies have shown that in the super high frequency (SHF) and extremely high frequency (EHF) ranges on the basis of two-layer structures with different content of carbonyl iron particles can create a radar absorbing coatings with a reflectivity of less than -10 dB over a wide bandwidth from 3.1 to 17.1 GHz and from 27 to 37 GHz. Absorbing properties of composites are saved in terahertz frequency range from 250 to 525 GHz.展开更多
Due to large volume and high hardness of thermal insulation materials mostly used in high temperature fields, a composite cooling powder and its thixotropic hydrogel for thermal protection are presented. The core of c...Due to large volume and high hardness of thermal insulation materials mostly used in high temperature fields, a composite cooling powder and its thixotropic hydrogel for thermal protection are presented. The core of composite cooling material powder is super absorbent polymer, composing with metal salt, polysaccharide hydrosol and inorganic particles and other modifiers through a series of composite process, which can be easily stored for a long time. When needed, the powder can be mixed with water to obtain a kind of thixotropic hydrogel in a very short time. Experimental results show this thermal protection technology with thixotropic ability has excellent thermal protection performance, meanwhile flexible, adhesive and low cost, which exerts instantaneous cooling, efficient thermal protection and long-lasting flame-retardant protection.展开更多
为提高辣椒粉吸光度的检测效率,以新疆辣椒粉为建模材料,使用波通、蔡司和赛默飞3个品牌的近红外光谱仪对辣椒粉进行扫描建模,确定最佳方式为赛默飞近红外光谱仪在波数精度16 cm^(-1)条件下采集光谱,利用偏最小二乘法建立模型。经过一...为提高辣椒粉吸光度的检测效率,以新疆辣椒粉为建模材料,使用波通、蔡司和赛默飞3个品牌的近红外光谱仪对辣椒粉进行扫描建模,确定最佳方式为赛默飞近红外光谱仪在波数精度16 cm^(-1)条件下采集光谱,利用偏最小二乘法建立模型。经过一阶导数+SG平滑两步光谱预处理方式,并选择主因子数为15,对模型进行优化。校正均方根误差(Root Mean Square Error of Calibration,RMSEC)为0.218,校正相关系数(Correlation Coefficient of Calibration,Rc)为0.9934;日内精密度(n=3)最大为1.22%,日间精密度(n=3)最大为0.98%,93%的样品化学实验值与近红外模型预测值两者之差在0.6以内,结果表明该近红外模型稳定性好,精确度高,能实现辣椒粉吸光度的快速检测。展开更多
基金financially supported by the National Hi-tech R&D Project Supporting Programs Funded by Ministry of Science&Technology of China(No.2012AA063202)the National Natural Science Foundation of China(Nos.50972013,50802008,and 51004011)+1 种基金the National Key Project of Scientific and Technical Supporting Programs Funded by Ministry of Science&Technology of China(Nos.2012BAC02B01,2012BAC12B05,2011BAE13B07,and 2011BAC10B02)the Guangdong Province&Ministry of Education Industry-Study-Research United Project(No.2009A090100017)
文摘The electromagnetic and microwave absorbing properties of FeCoB powder composites prepared by sin- gle-roller melt-spinning and mechanical milling processes were investigated in this paper. The result indicates that the flake-like powders are obtained. As milling time increases, the flake-like powder particles tend to agglomerate, causing the flake-like powders decrease gradually. The milling time plays an important role in the electromagnetic parameters which relates to the shape and size of the powder particles. The calculation shows that the sample milled for 6 h could achieve an optimal reflection loss of -11.5 dB at 5.8 GHz, with mass fraction of 83 % and a matching thickness of 1.8 mm. The result also indicates that the microwave absorbing properties of the FeCoB powder composites are adjustable by changing their thickness, and can be applied as a thinner microwave absorbing material in the range of 2-8 GHz.
基金financially supported by the National Natural Science Foundation of China (No. 60961001)the National Natural Science Fund Committee and the China Academy of Engineering Physics United Fund (No. 11076016)
文摘Fe73.5Cu1Nb3Si13.5B9 （or FeCuNbSiB） powder/ S-glass fiber-reinforced epoxy composite panels were pre- pared by mold pressing method. Metallographic analysis shows that the amorphous powders are evenly distributed between the layers of S-glass fibers. The effects of the Fe- CuNbSiB powder mass fraction on the complex permittivity, complex permeability, and microwave absorption of the composite panels have been studied in the frequency range of 2.6-18.0 GHz. The complex permittivity of the composite panels with different mass fractions of the FeCuNbSiB powders shows several peaks in the 2.6-18.0 GHz fre- quency range. The complex permeability of the composites decreases with the increasing frequency in the frequency range of 8-18 GHz. The composite with FeCuNbSiB/epoxy mass ratio of 2.5：1.0 has excellent microwave absorption properties of a minimum reflection loss value -30.5 dB at 10.93 GHz for a thickness of 2 mm. A reflection loss exceeding -10 dB can be obtained in a broad frequency range of 3.2-18.0 GHz with a thickness of 1.15-5.00 mm. For the FeCuNbSiB composites, the magnetic loss is the dominant term for microwave absorption. The FeCuNbSiB powders are a possible candidate for high-performance microwave absorption filler.
文摘Powder metallurgy （P/M） method has mainly been used to produce automobile parts such as self-lubrication beds, shock absorber parts, and gear wheels. In order to investigate the effect of porosity on the mechanical and tribological properties in sintered steel, specimens with 10%, 15%, and 20% porosity were produced in a 10 mm×10 mm×55 mm prismatic shape by pre-alloying powders of the MPIF Fe-C-0.205 alloy used in the production of shock absorber pistons. Sintering was carried out at 900℃ for 45 min in an argon atmosphere. Tensile, charpy, and microhardness tests were performed on these specimens. In addition, the wear performance of a 2% Cu reinforced sintered steel alloy under dry sliding conditions was determined. Metallographic studies such as pore formation, worn surface, and fractured surface analyses were performed by scanning electron microscopy and optical microscopy. The results indicate that irregular pore formation tendencies increase with an increase in porosity （%）. Furthermore, an increase in porosity was shown to decrease the mechanical properties and increase the wear trace area and the friction coefficient of sintered steel.
文摘BaO-La2O3-B2O3 （BLB） glass, suitable to be used as a sealing between metals, was chosen to be the binder in preparing glass coats on the Ti-alloy substrate. The SiCN nano-powder was introduced as the filler for the absorbing coat because it is considered to be a good high temperature absorber. The effect of the coating temperature and coating time on the tensile strength of the glass coat was investigated and the proper coating parameters to get good mechanical properties were determined. In addition, the effects of the SiCN content on the tensile strength of the absorbing coat were also discussed. Results show that it is possible to prepare the glass coat using the BLB glass as a binder. That the coat formed at 730℃ for 30 min has the best tensile strength witnesses 730 ℃, 30 min to be the proper parameter to prepare the glass coat. The BLB glass coat without SiCN powder possesses good tensile strength and the introduction of the SiCN absorber into the glass coat will lower the tensile strength. As the SiCN content increases, the tensile strength of the absorbing coat decreases, which could be attributed to the aggregation of SiCN in the coats.
文摘The effects of types and amounts of silane coupling agent on mechanical properties of vuleanized rubber microwave absorbing patch （VRMAP） were studied. The mechanisms of silane coupling agent＇s effects on mechanical properties of rubber microwave absorbing patch （ RMAP ） and microvave absorbing patch＇s （MAP＇s） mierostrueture were also discussed by using SEM and FT-IR. The experimental results show that the tensile strength of RMAP could be increased through adding the filler of carbonyl iron powder （CIP） modified by silane coupling agent. RMAP fiUed with CIP, which was treated by silane coupling agent KH550, possessed a high tensile strength of 11.5 MPa, which was 448% more than that of MAP whose filler wus not modified by any coupling agent. It was found that the optimal amount of KH550 was 1.0 phr to 100.0 phr carbonyl iron powder. The effects of different modifying techniques on RMAP＇s mechanical properties were also inrestigated. It is indieated that MAP whose filler is modified by the wet process has the highest tensile strength, but it is not the optimal modiifying technique due to complieated wet process. On the contrary, the dry process was very simple, and VRMAP possessed fairly high mechanical properties, therefore, it was the perfect modifying process.
文摘Results of measurements of permeability, permittivity and radar absorption properties of composites on basis of carbonyl iron particles R-10 brand are presented in this paper. The calculations and experimental studies have shown that in the super high frequency (SHF) and extremely high frequency (EHF) ranges on the basis of two-layer structures with different content of carbonyl iron particles can create a radar absorbing coatings with a reflectivity of less than -10 dB over a wide bandwidth from 3.1 to 17.1 GHz and from 27 to 37 GHz. Absorbing properties of composites are saved in terahertz frequency range from 250 to 525 GHz.
文摘Due to large volume and high hardness of thermal insulation materials mostly used in high temperature fields, a composite cooling powder and its thixotropic hydrogel for thermal protection are presented. The core of composite cooling material powder is super absorbent polymer, composing with metal salt, polysaccharide hydrosol and inorganic particles and other modifiers through a series of composite process, which can be easily stored for a long time. When needed, the powder can be mixed with water to obtain a kind of thixotropic hydrogel in a very short time. Experimental results show this thermal protection technology with thixotropic ability has excellent thermal protection performance, meanwhile flexible, adhesive and low cost, which exerts instantaneous cooling, efficient thermal protection and long-lasting flame-retardant protection.
文摘为提高辣椒粉吸光度的检测效率,以新疆辣椒粉为建模材料,使用波通、蔡司和赛默飞3个品牌的近红外光谱仪对辣椒粉进行扫描建模,确定最佳方式为赛默飞近红外光谱仪在波数精度16 cm^(-1)条件下采集光谱,利用偏最小二乘法建立模型。经过一阶导数+SG平滑两步光谱预处理方式,并选择主因子数为15,对模型进行优化。校正均方根误差(Root Mean Square Error of Calibration,RMSEC)为0.218,校正相关系数(Correlation Coefficient of Calibration,Rc)为0.9934;日内精密度(n=3)最大为1.22%,日间精密度(n=3)最大为0.98%,93%的样品化学实验值与近红外模型预测值两者之差在0.6以内,结果表明该近红外模型稳定性好,精确度高,能实现辣椒粉吸光度的快速检测。
