Polyphenols were obtained from the natural dried Lonicerae flos by ultrasound-assisted extraction with ethanol as the solvent.Single factor experiment and response surface methodology were employed to optimize the ext...Polyphenols were obtained from the natural dried Lonicerae flos by ultrasound-assisted extraction with ethanol as the solvent.Single factor experiment and response surface methodology were employed to optimize the extraction conditions.Ultra-performance liquid chromatrography(UPLC)-tandem mass spectrometry(MS/MS)was employed to identify polyphenols based on the plant widely targeted metabolomics database in a qualitative and quantitative manner.The results showed that the optimal extraction conditions for total phenols from Lonicerae flos were ultrasound-assisted extraction with a solid-to-liquid ratio of 10∶1 g/mL and 57%ethanol at 70 W and 60°C for 11 min.The yield of total phenols extracted under the optimal conditions reached 71.08 mg/g.The phenols in Lonicerae flos were mainly chlorogenic acid isomers,and the flavonoids were mainly nobiletin,galuteolin,and homoarbutin.展开更多
Four different types of three-body model composed of rock and coal with different strength and stiffness were established in order to study the failure characteristics of compound model such as roof-coal-floor. Throug...Four different types of three-body model composed of rock and coal with different strength and stiffness were established in order to study the failure characteristics of compound model such as roof-coal-floor. Through stress analysis of the element with variable strength and stiffness extracted from the strong-weak interface, the tri-axial compressive strength of the weak body and strong body near the interface as well as the areas away from the contact surface was found. Then, on the basis of three-dimensional fast Lagrangian method of continua and strain softening constitutive model composed of Coulomb-Mohr shear failure with tensile cut-off, stress and strain relationship of the four three-body combined models were analyzed under different confining pressures by numerical simulation. Finally, the different features of local shear zones and plastic failure areas of the four different models and their development trend with increasing confining pressure were discussed. The results show that additional stresses are derived due to the lateral deformation constraints near the strong-weak interface area, which results in the strength increasing in weak body and strength decreasing in strong body. The weakly consolidated soft rock and coal cementation exhibit significant strain softening behavior and bear compound tension-shear failure under uni-axial compression. With the increase of confining pressure, the tensile failure disappears from the model, and the failure type of composed model changes to local shear failure with different number of shearing bands and plastic failure zones. This work shows important guiding significance for the mechanism study of seismic, rock burst, and coal bump.展开更多
By using Bayesian and multiple Bayesian method, the failure probability, reliability and mean time to failure(MTTF) of series system with cold standby units are estimated. At last, we compare the two estimators by mea...By using Bayesian and multiple Bayesian method, the failure probability, reliability and mean time to failure(MTTF) of series system with cold standby units are estimated. At last, we compare the two estimators by means of Monte_Carlo simulation.展开更多
To investigate the effects of various random factors on the preventive maintenance (PM) decision-making of one type of two-unit series system, an optimal quasi-periodic PM policy is introduced. Assume that PM is per...To investigate the effects of various random factors on the preventive maintenance (PM) decision-making of one type of two-unit series system, an optimal quasi-periodic PM policy is introduced. Assume that PM is perfect for unit 1 and only mechanical service for unit 2 in the model. PM activity is randomly performed according to a dynamic PM plan distributed in each implementation period. A replacement is determined based on the competing results of unplanned and planned replacements. The unplanned replacement is trigged by a catastrophic failure of unit 2, and the planned replacement is executed when the PM number reaches the threshold N. Through modeling and analysis, a solution algorithm for an optimal implementation period and the PM number is given, and optimal process and parametric sensitivity are provided by a numerical example. Results show that the implementation period should be decreased as soon as possible under the condition of meeting the needs of practice, which can increase mean operating time and decrease the long-run cost rate.展开更多
[Objective]The aim was to identify the composition of pigments from Jujube fruit skin.[Method]Pigments were extracted from'Lubei Dongzao','Lajiao Zao','Chengwu Dongzao','Dabailing'and identificated by using hi...[Objective]The aim was to identify the composition of pigments from Jujube fruit skin.[Method]Pigments were extracted from'Lubei Dongzao','Lajiao Zao','Chengwu Dongzao','Dabailing'and identificated by using high performance liquid chromatography-mass spectrometry(HPLC-MS).[Result]The results showed that eight flavanols and four to five flavonols were detected,no anthocyanins was detected.The contents of flavonoids were differnt in four varieties.The contents of flavanols(11 mg/g) and flavonols(1.78 mg/g) in'Dabailing' were one-time higher than other varieties.Quercetin 3 rutinoside was the major flavonol.[Conclusion]The research provided theoretical basis for further study on mechanism of Jujube pigment turnning into the red.展开更多
[Objective] A method was developed for the determination of 10 pyrethroids pesticide residues in rice by GC-MS-MS. [Method] Pyrethroids were extracted with acetonitrile, followed by a salting-out step with anhydrous m...[Objective] A method was developed for the determination of 10 pyrethroids pesticide residues in rice by GC-MS-MS. [Method] Pyrethroids were extracted with acetonitrile, followed by a salting-out step with anhydrous magnesium sulfate and sodium chloride, cleaned up by florisil solid phase extraction (SPE) cartridge, and determined by multiple reaction monitoring mode. [Result] The method showed good linearity over the range of 0.010-0.500 mg/L for 10 pyrethroid pesticide with correlation coefficients over 0.99. The detection limits were 0.005 -0.010 mg/kg. The method was validated by analyzing samples spiked with 0.05, 0.10, 0.20 mg/kg of 10 pyrethroid pesticides, respectively. The average recoveries in rice ranged from 75.0-115.5%, and the relative standard deviations (RSD) were between 3.9%-6.9%. [Conclusion] The method is easy, accurate and reliable, which can meet the requirement for the simultaneous determination and confirmation of pyrethroid pesticide residues in rice.展开更多
To improve the performance of the short interleaved serial concatenated convolutional code(SCCC) with low decoding iterative times, the structure of Log MAP algorithm is introduced into the conventional SOVA decoder...To improve the performance of the short interleaved serial concatenated convolutional code(SCCC) with low decoding iterative times, the structure of Log MAP algorithm is introduced into the conventional SOVA decoder to improve its performance at short interleaving delay. The combination of Log MAP and SOVA avoids updating the matrices of the maximum path, and also makes a contribution to the requirement of short delay. The simulation results of several SCCCs show that the improved decoder can obtain satisfied performance with short frame interleaver and it is suitable to the high bit rate low delay communication systems.展开更多
The effects of several factors on mobility in 4H-SiC buried-channel (BC) MOSFETs are studied,A simple model that gives a quantitative analysis of series resistance effects on the effective mobility and field-effect ...The effects of several factors on mobility in 4H-SiC buried-channel (BC) MOSFETs are studied,A simple model that gives a quantitative analysis of series resistance effects on the effective mobility and field-effect mobility is proposed.A series resistance not only decreases field-effect mobility but also reduces the gate voltage corresponding to the peak field-effect mobility. The dependence of the peak field-effect mobility on series resistance follows a simple quadratic polynomial. The effects of uniform and exponential interface state distributions in the forbidden band on field-effect mobility are analyzed with an analytical model. The effects of non-uniform interface states can be ignored at lower gate voltages but become more obvious as the gate bias increases.展开更多
To solve the low efficiency of electric excitation claw-pole synchronous generator(EECPSG) and regulate the magnetic field of permanent magnet (PM) claw-pole synchronous generator(PMCPSG), a novel hybrid excitat...To solve the low efficiency of electric excitation claw-pole synchronous generator(EECPSG) and regulate the magnetic field of permanent magnet (PM) claw-pole synchronous generator(PMCPSG), a novel hybrid excitation claw-pole synchronous generator (HECPSG)with magnetic circuit series connection is proposed. Through the simulation study on the generator using the calculation method for magnetic circuit and 3-D finite element method (FEA), the appropriate magnet thickness and the number of pole-pairs for the proposed generator are determined. Its off-loading characteristics, load characteristics, and regulation behaviors are investigated. The study shows that the appropriate number of pole-pairs in HECPSG with series magnetic circuits is two, and there exists an optimum magnet thickness. Compared to EECPSG, HECPSG realizes dual-directional control to the excitation current. Moreover, the generator can adjust the output voltage and keep the output voltage stable in a broad load range. Under the condition of same parametes, the motor has higer air-gap flux density and power density.展开更多
A novel parameter extraction technique suitable f or short channel length lightly-doped-drain (LDD) MOSFET's is proposed which seg ments the total gate bias range,and executes the linear regression in every subs ...A novel parameter extraction technique suitable f or short channel length lightly-doped-drain (LDD) MOSFET's is proposed which seg ments the total gate bias range,and executes the linear regression in every subs ections,yielding the gate bias dependent parameters,such as effective channel le ngth,parasitic resistance,and mobility,etc.This method avoids the gate bias rang e optimization,and retains the accuracy and simplicity of linear regression.The extracted gate bias dependent parameters are implemented in the compact I-V model which has been proposed for deep submicron LDD MOSFET's.The good agreemen ts between simulations and measurements of the devices on 0.18μm CMOS technolo gy indicate the effectivity of this technique.展开更多
To establish a rapid and effective method for analysis and identification of the alkaloids from Ranunculus japoni- cus Thunb by ultra-performance liquid chromatogaraphy with quadruple-time-of-flight mass spectrometry ...To establish a rapid and effective method for analysis and identification of the alkaloids from Ranunculus japoni- cus Thunb by ultra-performance liquid chromatogaraphy with quadruple-time-of-flight mass spectrometry (UPLC/Q-TOF- MS) and discuss their fragmentation regularity, the UPLC/Q-TOF-MS was used to identify the alkaloids from Ranunculus japonicus Thunb by their MS data, tandem characteristic fragment ions and standards. In the end, 12 alkaloids were identi- fied from Ranunculus japonicus for the first time, and their fragmentation regularity was discussed. Thus, a rapid and effec- tive analysis and identification method for the alkaloids from Ranunculus japonicus by UPLC/Q-TOF-MS is established.展开更多
In order to study the work-ability and establish the optimum hot formation processing parameters for industrial 1060 pure aluminum, the compressive deformation behavior of pure aluminum was investigated at temperature...In order to study the work-ability and establish the optimum hot formation processing parameters for industrial 1060 pure aluminum, the compressive deformation behavior of pure aluminum was investigated at temperatures of 523?823 K and strain rates of 0.005?10 s?1 on a Gleeble?1500 thermo-simulation machine. The influence rule of processing parameters (strain, strain rate and temperature) on flow stress of pure aluminum was investigated. Nine analysis factors consisting of material parameters and according weights were optimized. Then, the constitutive equations of multilevel series rules, multilevel parallel rules and multilevel series ¶llel rules were established. The correlation coefficients (R) are 0.992, 0.988 and 0.990, respectively, and the average absolute relative errors (AAREs) are 6.77%, 8.70% and 7.63%, respectively, which proves that the constitutive equations of multilevel series rules can predict the flow stress of pure aluminum with good correlation and precision.展开更多
Recent molecular cytogenetic studies demonstrate that extensive centromere-telomere fusions are the main chromosomal rearrangements underlying the karyotypic evolution of extant muntjacs. Although the molecular mechan...Recent molecular cytogenetic studies demonstrate that extensive centromere-telomere fusions are the main chromosomal rearrangements underlying the karyotypic evolution of extant muntjacs. Although the molecular mechanism of tandem fusions remains unknown, satellite DNA is believed to have facilitated chromosome fusions by non-allelic homologous recombination. Previous studies detected non-random hybridization signals of cloned satellite DNA at the postulated fusion sites on the chromosomes in Indian and Chinese muntjacs. But the genomic distribution and organization of satellite DNAs in other muntjacs have not been investigated. In this study, we have isolated four satellite DNA clones (BMCS, BM700, BM 1.1 k and FM700) from the black muntjac (Muntiacus crinifrons) and Fea's muntjac (M. feae), and hybridized these four clones onto chromosomes of four muntjac species (M. reevesi, M. crinifrons, M. gongshanenisis and M. feae). Besides the predominant centromeric signals, non-random interstitial hybridization signals from satellite I and II DNA clones (BMC5, BM700 and FM700) were also observed on the arms of chromosomes of these four muntjacs. Our results provide additional support for the notion that the karyotypes of M. crinifrons, M. feae and M. gongshanensis have evolved from a 2n = 70 ancestral karyotype by a series of chromosome fusions.展开更多
基金Supported by Agricultural Science and Technology Innovation Fund Project of Hunan Province(2022CX87)Huaihua Municipal Institute of Science and Technology Cooperation Project(2022N1203)Science and Technology Talent Lifting Project of Hunan Province—Training Plan for Young and Middle-aged Scholars(2023TJ-Z01)。
文摘Polyphenols were obtained from the natural dried Lonicerae flos by ultrasound-assisted extraction with ethanol as the solvent.Single factor experiment and response surface methodology were employed to optimize the extraction conditions.Ultra-performance liquid chromatrography(UPLC)-tandem mass spectrometry(MS/MS)was employed to identify polyphenols based on the plant widely targeted metabolomics database in a qualitative and quantitative manner.The results showed that the optimal extraction conditions for total phenols from Lonicerae flos were ultrasound-assisted extraction with a solid-to-liquid ratio of 10∶1 g/mL and 57%ethanol at 70 W and 60°C for 11 min.The yield of total phenols extracted under the optimal conditions reached 71.08 mg/g.The phenols in Lonicerae flos were mainly chlorogenic acid isomers,and the flavonoids were mainly nobiletin,galuteolin,and homoarbutin.
基金Project(51174128)supported by the National Natural Science Foundation of ChinaProject(20123718110007)supported by the Specialized Research Fund for the Doctoral Program of Higher Education of China
文摘Four different types of three-body model composed of rock and coal with different strength and stiffness were established in order to study the failure characteristics of compound model such as roof-coal-floor. Through stress analysis of the element with variable strength and stiffness extracted from the strong-weak interface, the tri-axial compressive strength of the weak body and strong body near the interface as well as the areas away from the contact surface was found. Then, on the basis of three-dimensional fast Lagrangian method of continua and strain softening constitutive model composed of Coulomb-Mohr shear failure with tensile cut-off, stress and strain relationship of the four three-body combined models were analyzed under different confining pressures by numerical simulation. Finally, the different features of local shear zones and plastic failure areas of the four different models and their development trend with increasing confining pressure were discussed. The results show that additional stresses are derived due to the lateral deformation constraints near the strong-weak interface area, which results in the strength increasing in weak body and strength decreasing in strong body. The weakly consolidated soft rock and coal cementation exhibit significant strain softening behavior and bear compound tension-shear failure under uni-axial compression. With the increase of confining pressure, the tensile failure disappears from the model, and the failure type of composed model changes to local shear failure with different number of shearing bands and plastic failure zones. This work shows important guiding significance for the mechanism study of seismic, rock burst, and coal bump.
文摘By using Bayesian and multiple Bayesian method, the failure probability, reliability and mean time to failure(MTTF) of series system with cold standby units are estimated. At last, we compare the two estimators by means of Monte_Carlo simulation.
基金The National Natural Science Foundation of China(No.51275090,71201025)the Program for Special Talent in Six Fields of Jiangsu Province(No.2008144)+1 种基金the Scientific Research Foundation of Graduate School of Southeast University(No.YBJJ1302)the Scientific Innovation Research of College Graduates in Jiangsu Province(No.CXLX12_0078)
文摘To investigate the effects of various random factors on the preventive maintenance (PM) decision-making of one type of two-unit series system, an optimal quasi-periodic PM policy is introduced. Assume that PM is perfect for unit 1 and only mechanical service for unit 2 in the model. PM activity is randomly performed according to a dynamic PM plan distributed in each implementation period. A replacement is determined based on the competing results of unplanned and planned replacements. The unplanned replacement is trigged by a catastrophic failure of unit 2, and the planned replacement is executed when the PM number reaches the threshold N. Through modeling and analysis, a solution algorithm for an optimal implementation period and the PM number is given, and optimal process and parametric sensitivity are provided by a numerical example. Results show that the implementation period should be decreased as soon as possible under the condition of meeting the needs of practice, which can increase mean operating time and decrease the long-run cost rate.
基金Supported by National Key Technology R & D Program 2006BAD01A1701 and 2006BAD18B02Shandong Agriculture Good Cultivar Engineering Project (2008LZ09)~~
文摘[Objective]The aim was to identify the composition of pigments from Jujube fruit skin.[Method]Pigments were extracted from'Lubei Dongzao','Lajiao Zao','Chengwu Dongzao','Dabailing'and identificated by using high performance liquid chromatography-mass spectrometry(HPLC-MS).[Result]The results showed that eight flavanols and four to five flavonols were detected,no anthocyanins was detected.The contents of flavonoids were differnt in four varieties.The contents of flavanols(11 mg/g) and flavonols(1.78 mg/g) in'Dabailing' were one-time higher than other varieties.Quercetin 3 rutinoside was the major flavonol.[Conclusion]The research provided theoretical basis for further study on mechanism of Jujube pigment turnning into the red.
文摘[Objective] A method was developed for the determination of 10 pyrethroids pesticide residues in rice by GC-MS-MS. [Method] Pyrethroids were extracted with acetonitrile, followed by a salting-out step with anhydrous magnesium sulfate and sodium chloride, cleaned up by florisil solid phase extraction (SPE) cartridge, and determined by multiple reaction monitoring mode. [Result] The method showed good linearity over the range of 0.010-0.500 mg/L for 10 pyrethroid pesticide with correlation coefficients over 0.99. The detection limits were 0.005 -0.010 mg/kg. The method was validated by analyzing samples spiked with 0.05, 0.10, 0.20 mg/kg of 10 pyrethroid pesticides, respectively. The average recoveries in rice ranged from 75.0-115.5%, and the relative standard deviations (RSD) were between 3.9%-6.9%. [Conclusion] The method is easy, accurate and reliable, which can meet the requirement for the simultaneous determination and confirmation of pyrethroid pesticide residues in rice.
文摘To improve the performance of the short interleaved serial concatenated convolutional code(SCCC) with low decoding iterative times, the structure of Log MAP algorithm is introduced into the conventional SOVA decoder to improve its performance at short interleaving delay. The combination of Log MAP and SOVA avoids updating the matrices of the maximum path, and also makes a contribution to the requirement of short delay. The simulation results of several SCCCs show that the improved decoder can obtain satisfied performance with short frame interleaver and it is suitable to the high bit rate low delay communication systems.
文摘The effects of several factors on mobility in 4H-SiC buried-channel (BC) MOSFETs are studied,A simple model that gives a quantitative analysis of series resistance effects on the effective mobility and field-effect mobility is proposed.A series resistance not only decreases field-effect mobility but also reduces the gate voltage corresponding to the peak field-effect mobility. The dependence of the peak field-effect mobility on series resistance follows a simple quadratic polynomial. The effects of uniform and exponential interface state distributions in the forbidden band on field-effect mobility are analyzed with an analytical model. The effects of non-uniform interface states can be ignored at lower gate voltages but become more obvious as the gate bias increases.
基金Supported by the National Natural Science Foundation of China(50337030)the Natural Science Foundation of Shanghai(08ZR1408600)the Natural Science Foundation of Shanghai Dianji University(08C410)~~
文摘To solve the low efficiency of electric excitation claw-pole synchronous generator(EECPSG) and regulate the magnetic field of permanent magnet (PM) claw-pole synchronous generator(PMCPSG), a novel hybrid excitation claw-pole synchronous generator (HECPSG)with magnetic circuit series connection is proposed. Through the simulation study on the generator using the calculation method for magnetic circuit and 3-D finite element method (FEA), the appropriate magnet thickness and the number of pole-pairs for the proposed generator are determined. Its off-loading characteristics, load characteristics, and regulation behaviors are investigated. The study shows that the appropriate number of pole-pairs in HECPSG with series magnetic circuits is two, and there exists an optimum magnet thickness. Compared to EECPSG, HECPSG realizes dual-directional control to the excitation current. Moreover, the generator can adjust the output voltage and keep the output voltage stable in a broad load range. Under the condition of same parametes, the motor has higer air-gap flux density and power density.
文摘A novel parameter extraction technique suitable f or short channel length lightly-doped-drain (LDD) MOSFET's is proposed which seg ments the total gate bias range,and executes the linear regression in every subs ections,yielding the gate bias dependent parameters,such as effective channel le ngth,parasitic resistance,and mobility,etc.This method avoids the gate bias rang e optimization,and retains the accuracy and simplicity of linear regression.The extracted gate bias dependent parameters are implemented in the compact I-V model which has been proposed for deep submicron LDD MOSFET's.The good agreemen ts between simulations and measurements of the devices on 0.18μm CMOS technolo gy indicate the effectivity of this technique.
文摘To establish a rapid and effective method for analysis and identification of the alkaloids from Ranunculus japoni- cus Thunb by ultra-performance liquid chromatogaraphy with quadruple-time-of-flight mass spectrometry (UPLC/Q-TOF- MS) and discuss their fragmentation regularity, the UPLC/Q-TOF-MS was used to identify the alkaloids from Ranunculus japonicus Thunb by their MS data, tandem characteristic fragment ions and standards. In the end, 12 alkaloids were identi- fied from Ranunculus japonicus for the first time, and their fragmentation regularity was discussed. Thus, a rapid and effec- tive analysis and identification method for the alkaloids from Ranunculus japonicus by UPLC/Q-TOF-MS is established.
基金Project(51275414)supported by the National Natural Science Foundation of ChinaProject(2015JM5204)supported by the Natural Science Foundation of Shaanxi Province,China+1 种基金Project(Z2015064)supported by the Graduate Starting Seed Fund of the Northwestern Polytechnical University,ChinaProject(130-QP-2015)supported by the Research Fund of the State Key Laboratory of Solidification Processing(NWPU),China
文摘In order to study the work-ability and establish the optimum hot formation processing parameters for industrial 1060 pure aluminum, the compressive deformation behavior of pure aluminum was investigated at temperatures of 523?823 K and strain rates of 0.005?10 s?1 on a Gleeble?1500 thermo-simulation machine. The influence rule of processing parameters (strain, strain rate and temperature) on flow stress of pure aluminum was investigated. Nine analysis factors consisting of material parameters and according weights were optimized. Then, the constitutive equations of multilevel series rules, multilevel parallel rules and multilevel series ¶llel rules were established. The correlation coefficients (R) are 0.992, 0.988 and 0.990, respectively, and the average absolute relative errors (AAREs) are 6.77%, 8.70% and 7.63%, respectively, which proves that the constitutive equations of multilevel series rules can predict the flow stress of pure aluminum with good correlation and precision.
基金the grant from the National Natural Science Foundation of China (30270719)
文摘Recent molecular cytogenetic studies demonstrate that extensive centromere-telomere fusions are the main chromosomal rearrangements underlying the karyotypic evolution of extant muntjacs. Although the molecular mechanism of tandem fusions remains unknown, satellite DNA is believed to have facilitated chromosome fusions by non-allelic homologous recombination. Previous studies detected non-random hybridization signals of cloned satellite DNA at the postulated fusion sites on the chromosomes in Indian and Chinese muntjacs. But the genomic distribution and organization of satellite DNAs in other muntjacs have not been investigated. In this study, we have isolated four satellite DNA clones (BMCS, BM700, BM 1.1 k and FM700) from the black muntjac (Muntiacus crinifrons) and Fea's muntjac (M. feae), and hybridized these four clones onto chromosomes of four muntjac species (M. reevesi, M. crinifrons, M. gongshanenisis and M. feae). Besides the predominant centromeric signals, non-random interstitial hybridization signals from satellite I and II DNA clones (BMC5, BM700 and FM700) were also observed on the arms of chromosomes of these four muntjacs. Our results provide additional support for the notion that the karyotypes of M. crinifrons, M. feae and M. gongshanensis have evolved from a 2n = 70 ancestral karyotype by a series of chromosome fusions.