The aim of current study was to investigate the chemical constituents from the flowers of Rhododendron molle G. Don. The isolation and purification of components were achieved by a series of chromatography including s...The aim of current study was to investigate the chemical constituents from the flowers of Rhododendron molle G. Don. The isolation and purification of components were achieved by a series of chromatography including silica gel, Sephadex LH-20, and reversed-phase HPLC. Their structures were identified based on 1D, 2D NMR, and mass spectral analysis. Fifteen known compounds were isolated and their structures were identified as 2E,4Z-abscisic acid(1), 2α-hydroxy-oleanolic acid(2), oleanic acid(3), asiatic acid(4), benzyl glucoside(5), dibutyl phthalate(6), β-sitosterol(7), vitexin(8), quercetin(9), steraric acid(10), rhodomollein I(11), rhodojaponin VI(12), rhodomollein XI(13), rhodojaponin II(14), kalmanol(15). Compounds 1–10 were isolated from Rhododendron molle for the first time.展开更多
基金National Natural Science Foundation of China(Grant No.81172943)
文摘The aim of current study was to investigate the chemical constituents from the flowers of Rhododendron molle G. Don. The isolation and purification of components were achieved by a series of chromatography including silica gel, Sephadex LH-20, and reversed-phase HPLC. Their structures were identified based on 1D, 2D NMR, and mass spectral analysis. Fifteen known compounds were isolated and their structures were identified as 2E,4Z-abscisic acid(1), 2α-hydroxy-oleanolic acid(2), oleanic acid(3), asiatic acid(4), benzyl glucoside(5), dibutyl phthalate(6), β-sitosterol(7), vitexin(8), quercetin(9), steraric acid(10), rhodomollein I(11), rhodojaponin VI(12), rhodomollein XI(13), rhodojaponin II(14), kalmanol(15). Compounds 1–10 were isolated from Rhododendron molle for the first time.