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高效液相色谱-荧光检测法测定罐头食品中的双酚A、BADGE及其衍生物 被引量:26
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作者 葛宇 印杰 +5 位作者 曹程明 叶天 宁啸骏 虞成华 熊薇 忻元庆 《食品与发酵工业》 CAS CSCD 北大核心 2009年第9期119-123,共5页
研究建立了一种罐头食品中的双酚A、BADGE及其衍生物含量的高效液相色谱-荧光检测法。前处理包括乙腈萃取,超声,旋转蒸发,压滤等步骤。样品经ZORBAX SB-C18柱(4.6 mm×250 mm)分离,以0.02 mol/L乙酸铵溶液和甲醇为流动相,在激发波长... 研究建立了一种罐头食品中的双酚A、BADGE及其衍生物含量的高效液相色谱-荧光检测法。前处理包括乙腈萃取,超声,旋转蒸发,压滤等步骤。样品经ZORBAX SB-C18柱(4.6 mm×250 mm)分离,以0.02 mol/L乙酸铵溶液和甲醇为流动相,在激发波长225 nm、发射波长305 nm下进行荧光检测。检出限达到0.04-0.1μg/mL。6次重复实验的相对标准偏差分别为BADGE.2H2O 0.60%、BPA 0.83%、BADGE.H2O 1.02%、BADGE.H2O.HCl 0.66%、BADGE 0.59%、BADGE.HCl 0.37%、BADGE.2HCl 1.81%,方法回收率分别为BADGE.2H2O 93%-105%、BPA97%-104%、BADGE.H2O 85%-101%、BADGE.H2O.HCl 92%-102%、BADGE 96%-99%、BADGE.HCl 95%-106%、BADGE.2HCl 87%-111%,满足痕量分析要求。该方法简便快速,灵敏可靠,适用于罐头食品中双酚A和6种BADGE衍生物含量的同时检测。 展开更多
关键词 高效液相色谱-荧光法 罐头食品 badge及其衍生物 检测
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超高效液相色谱-串联质谱法同时测定鱼、肉类罐头食品中的BADGE、NOGE及其衍生物 被引量:3
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作者 林赛君 陈思 +1 位作者 薛鸣 张虹 《食品与发酵工业》 CAS CSCD 北大核心 2011年第8期155-160,共6页
建立了一种罐头食品中的BADGE(bisphenol A diglycidyl ether,双酚A-二环氧甘油醚)、NOGE(novolacglycidyl ether,酚醛清漆甘油醚)及其衍生物含量的超高效液相色谱-串联质谱检测法。前处理包括正己烷/丙酮微波辅助萃取,Varain-PS-DVB固... 建立了一种罐头食品中的BADGE(bisphenol A diglycidyl ether,双酚A-二环氧甘油醚)、NOGE(novolacglycidyl ether,酚醛清漆甘油醚)及其衍生物含量的超高效液相色谱-串联质谱检测法。前处理包括正己烷/丙酮微波辅助萃取,Varain-PS-DVB固相萃取柱净化等。样品经BEH C18色谱柱(100 mm×2.1 mm,1.7μm)分离,以乙腈和0.2%甲酸水为流动相,进行梯度洗脱,在API 4000-QTRAP质谱仪电喷雾正离子、多反应监测(MRM)模式下进行检测。分析物检出限达到0.010 2 ng/g到0.197 2 ng/g,三水平加标回收率在65.7%~99.1%。 展开更多
关键词 超高效液相色谱-串联质谱法 罐头食品 badge NOGE 衍生物 检测
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Symbolic Images of Colors, Animals and Machines in The Red Badge of Courage
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作者 王晓俊 《英语广场(学术研究)》 2014年第1期23-27,30,共6页
Abstract:Stephen Crane was an outstanding American novelist,poet,and journalist.He achieved great success in his literary works during his brief career.Crane’s most well-known work,The Red Badge of Courage,is commonl... Abstract:Stephen Crane was an outstanding American novelist,poet,and journalist.He achieved great success in his literary works during his brief career.Crane’s most well-known work,The Red Badge of Courage,is commonly believed to be the first great novel of the American Civil War,largely because of its vivid and detailed description of the experience of warfare.This paper analyzes the images of color,animal and machine,which convey Crane’s thoughts of war:war is full of chaos,brutality,and confusion,without any romantic elements or heroism. 展开更多
关键词 The Red badge of Courage symbolic images color images animal images machine images
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Symbolic Images of Figures in The Red Badge of Courage
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作者 王晓俊 《海外英语》 2014年第3X期5-7,9,共4页
Crane’s most well-known work,The Red Badge of Courage,is commonly believed to be the first great novel of the American Civil War,largely because of its vivid and detailed description of the experience of warfare.This... Crane’s most well-known work,The Red Badge of Courage,is commonly believed to be the first great novel of the American Civil War,largely because of its vivid and detailed description of the experience of warfare.This paper conveys figure images symbolize that human life is insignificant in an indifferent universe in the novel,which are perfect symbolic images distinguish Crane as a forerunner of modernistic writers. 展开更多
关键词 CRANE The Red badge of COURAGE SYMBOLIC images FIG
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Filter badge SO_2捕集-离子色谱法测定空气中二氧化硫 被引量:3
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作者 陈秀娟 谭红 +1 位作者 洪涛 沈方祥 《中国环境监测》 CAS CSCD 北大核心 2009年第5期45-46,共2页
用Filter badge SO2捕集空气中SO2。用双氧水将捕集到的SO2氧化成SO42-,再用离子色谱法测定SO42-的浓度,按公式f SO2=2082×103×(T/τ)X计算,即可得到捕集时间内的平均SO2浓度f SO2(ppb)。
关键词 FILTER badge SO2 二氧化硫 离子色谱
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日本航空自卫队基地防空地面设施(BADGE)系统 被引量:1
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作者 刘春阳 《现代防御技术》 2001年第6期10-15,20,共7页
分别讨论航空自卫队BADGE系统的指挥控制、通信、侦察监视和预警以及电子战系统 ,介绍其历史沿革、现状和发展趋势 。
关键词 日本 航空自卫队 C^3I指挥控制 军事通信 侦察监视 防空预警 电子战 基地防空设施 badge系统
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Literature Review on The Red Badge of Courage
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作者 李翠翠 《海外英语》 2010年第6X期228-229,共2页
The Red Badge of Courage is one of the most controversial works of Stephen Crane.Critics have long debated whether this novel should be considered a product of any specific literary movement or method,which is listed ... The Red Badge of Courage is one of the most controversial works of Stephen Crane.Critics have long debated whether this novel should be considered a product of any specific literary movement or method,which is listed in this literature review. 展开更多
关键词 The RED badge of COURAGE Stephen CRANE LITERATURE review
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A Research on Symbolism in The Red Badge of Courage
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作者 曾杰 《海外英语》 2010年第12X期242-244,共3页
Stephen Crane(Stephen Crane,1871-1900),a famous American novelist and poet.The Red Badge of Courage,his masterwork,published in book form in 1895,has been widely acknowledged as a classic in American literary history.... Stephen Crane(Stephen Crane,1871-1900),a famous American novelist and poet.The Red Badge of Courage,his masterwork,published in book form in 1895,has been widely acknowledged as a classic in American literary history.In most cases,symbolism is considered to be a technique used by Crane to convey its naturalistic theme.This thesis attempts to make a detailed analysis of the system of symbols in The Red Badge of Courage to show that symbolism is used by Crane to better convey his naturalistic ideas so that a better understanding and appreciation of the work can be achieved.Crane's symbolic style makes him become a pioneer modernistic writer who has influenced many later writers. 展开更多
关键词 Stephen CRANE The RED badge of COURAGE symbolism.
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An Analysis of Stephen Crane's The Red Badge of Courage
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作者 李楠 《疯狂英语(教师版)》 2012年第3期198-199,204,共3页
The Red Badge of Courage,the masterpiece of Stephen Crane,was "an episode of the American Civil War".It is written in a naturalistic style which indicates the trend of naturalistic writings in the 20th centu... The Red Badge of Courage,the masterpiece of Stephen Crane,was "an episode of the American Civil War".It is written in a naturalistic style which indicates the trend of naturalistic writings in the 20th century in America.As a naturalist novel,it takes survival,determinism,violence,and taboo as key themes,and shows indifference of the natural world. 展开更多
关键词 Stephen Crane The Red badge of Courage NATURALISM indifference of the nature
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高效液相色谱法测定食品用金属容器内壁涂料中的双酚A二缩水甘油醚(BADGE) 被引量:1
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作者 白彦坤 郭丽敏 +3 位作者 王琪 张敬轩 李文良 刘金鹏 《现代仪器》 2010年第5期88-89,69,共3页
建立一种测定食品用金属容器内涂料中的双酚A二缩水甘油醚(BADGE)的方法。采用选择不同的模拟条件提取样品,用高效液相色谱进行测定。方法的检出限为0.05μg/mL,回收率为85.2%~93.1%,相对标准偏差为2.9%~5.2%。
关键词 双酚A二缩水甘油醚(badge) 高效液相色谱 食品用金属容器
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Naturalistic Analysis on Stephen Crane's The Red Badge of Courage
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作者 李夏莲 胡笑瑛 《海外英语》 2015年第6期167-168,共2页
The Red Badge of Courage is the masterpiece of Stephen Crane. As a naturalist novel, its success is based on strong visual stimulation and the continuous auditory shock, a three-dimensional war movie which is cracklin... The Red Badge of Courage is the masterpiece of Stephen Crane. As a naturalist novel, its success is based on strong visual stimulation and the continuous auditory shock, a three-dimensional war movie which is crackling with sounds and colors was rendered so incisively and vividly. This paper aims to probe the naturalism in The Red Badge of Courage from two angles:visual aspects and auditory aspects. 展开更多
关键词 The Red badge of COURAGE NATURALISM visual ASPECTS AUDITORY ASPECTS
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The Red Badge of Courage: The Greatest Truth of War
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作者 张志远 《海外英语》 2017年第8期177-178,共2页
The Red Badge of Courage is a classic in American literature, which exerts a profound influence on war novels afterwards. Inthis novel, instead of depicting war as something heroic or glorious, Stephen Crane describe ... The Red Badge of Courage is a classic in American literature, which exerts a profound influence on war novels afterwards. Inthis novel, instead of depicting war as something heroic or glorious, Stephen Crane describe the war in an alarming way, thus uncoveringthe truth of war and highlighting its anti-war theme. 展开更多
关键词 WAR The Red badge of Courage BRUTALITY humbleness subhuman ANTI-WAR
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A Study of Irony in Stephen Crane's The Red Badge of Courage
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作者 鲍姗姗 《海外英语》 2018年第2期165-167,共3页
Stephen Crane is a famous naturalist writer in the nineteenth Century.He creates a new method of literary writing in America.His famous novel The Red Badge of Courage is an episode of the American civil war.The novel... Stephen Crane is a famous naturalist writer in the nineteenth Century.He creates a new method of literary writing in America.His famous novel The Red Badge of Courage is an episode of the American civil war.The novel’s rhetoric device"irony"is worthy of contemporary scholars to carry out in-depth research.Crane adopts irony in his works to enhance the performance of language tension and the profound theme of the novel.The artistic features of irony appear in the novel frequently,such as verbal irony,scene irony and structural irony,which constructs the basic framework and structure of this novel and makes it more humorous,more ironic and more meaningful. 展开更多
关键词 Stephen Crane The Red badge of Courage verbal irony scene irony structural irony
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Study on Human Weaknesses in Henry in The Red Badge of Courage
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作者 CHU Shi-qi 《Journal of Literature and Art Studies》 2022年第12期1257-1260,共4页
As one of Crane’s most representative works,The Red Badge of Courage has been paid much attention to and studied by scholars at home and abroad from different perspectives since its publication.As for me,I’d like to... As one of Crane’s most representative works,The Red Badge of Courage has been paid much attention to and studied by scholars at home and abroad from different perspectives since its publication.As for me,I’d like to study on human weaknesses in Henry in The Red Badge of Courage to give an analysis of the three main human weaknesses existing in Henry and explore the underlying causes.It will be of great benefit to promote our understanding of the novel from this angle,thus bringing us much practical significance. 展开更多
关键词 The Red badge of Courage human weaknesses Henry
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The First Modern Novel of War in American Literature──On The Red Badge of Courage
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作者 陈许 《盐城师范学院学报(人文社会科学版)》 1997年第1期52-57,共6页
关键词 On The Red badge of Courage
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LC-MS/MS分析罐装食品和饮料中的双酚A-缩水甘油醚(BADGE)、双酚F-缩水甘油醚(BFDGE)及其衍生物
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作者 Hector Gallart-Ayala Encamacion Moyano +1 位作者 M,T. Galceran Claudia EB Martins 《中国食品》 2012年第12期60-63,共4页
双酚A缩水甘油醚(BADGE)和双酚F-缩水甘油醚(BFDGE)经常被用于罐装食品和饮料中,但它们及它们的衍生物存在着潜在的致突变性、遗传毒性和抗雄激素作用,欧盟已对其总量作了限制。本文的目的就是开发一种能同时定量测定罐装食品和... 双酚A缩水甘油醚(BADGE)和双酚F-缩水甘油醚(BFDGE)经常被用于罐装食品和饮料中,但它们及它们的衍生物存在着潜在的致突变性、遗传毒性和抗雄激素作用,欧盟已对其总量作了限制。本文的目的就是开发一种能同时定量测定罐装食品和饮料中BADGE、BFDGE及其衍生物的快速灵敏的LC-MS/MS方法。 展开更多
关键词 badge BFDGE LC-MS/MS 食品安全
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ITMA ASIA + CITME 2010 Exhibition Space Sold Out Visitors offered convenient online registration and badge printing service
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《China Textile》 2010年第5期22-22,共1页
The reputation of ITMA ASIA+ClTME 2010 as Asia’s premier textile industry platform has been given a further boost following an announcement from the show organizers that all exhibition space has now been sold. Over 1... The reputation of ITMA ASIA+ClTME 2010 as Asia’s premier textile industry platform has been given a further boost following an announcement from the show organizers that all exhibition space has now been sold. Over 1,100 textile and garment machinery manufacturers have applied successfully to exhibit at the second combined show,taking up 100,000 square meters of Shanghai New International Expo Centre. 展开更多
关键词 ITMA ASIA ASIA CITME 2010 Exhibition Space Sold Out Visitors offered convenient online registration and badge printing service 2010
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劳斯莱斯魅影Black Badge 暗夜之光
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作者 刘承重 刘谱 《轿车情报》 2017年第10期90-93,共4页
当圣洁的欢庆女神幻化为一袭黑衣的魅惑女郎,她将引领你进入暗夜中的极乐世界。这部特殊的劳斯莱斯名为魅影Black Badge。在它周身上下正缭绕着一层神秘而深邃的黑色迷雾。车头的欢乐女神在迷雾中挥动着翅膀。只是这次,圣洁的女神已经... 当圣洁的欢庆女神幻化为一袭黑衣的魅惑女郎,她将引领你进入暗夜中的极乐世界。这部特殊的劳斯莱斯名为魅影Black Badge。在它周身上下正缭绕着一层神秘而深邃的黑色迷雾。车头的欢乐女神在迷雾中挥动着翅膀。只是这次,圣洁的女神已经幻化为身着黑衣的魅惑女郎,就像一只在黑夜中振翅的性感精灵。 展开更多
关键词 劳斯莱斯 BLACK badge 制动系统 自动变速器 空气悬架 碳纤维材料 路感 最大扭矩 轮圈 双涡轮增压
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在线评论一致性对消费者决策的影响
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作者 王洪伟 赵家玲 +1 位作者 黄宇欣 冯素玲 《工业技术经济》 北大核心 2024年第8期139-149,共11页
信任是共享经济发展的关键因素,而基于情感的信任作为其中重要一环,通过在线评论效价影响消费者的决策。本文从在线评论的总评分和细节评分两个维度出发构建了共享短租消费者情感信任的影响机制,并利用2015~2022年中国北京和美国纽约的A... 信任是共享经济发展的关键因素,而基于情感的信任作为其中重要一环,通过在线评论效价影响消费者的决策。本文从在线评论的总评分和细节评分两个维度出发构建了共享短租消费者情感信任的影响机制,并利用2015~2022年中国北京和美国纽约的Airbnb平台订单数据实证分析情感信任对消费者决策的影响。研究结果显示,在线总评论和细节评论包含负面情感更易吸引消费者;当两类评分一致为高评分时消费者购买意愿显著下降。另外,“超赞房东”徽章和整租房源能积极调节两类评分一致性与消费者购买意愿的关系。中国房源对两类评分一致性与消费者购买意愿的关系有负向调节作用。因此,在交易过程中,消费者可多关注包含负面评价的评论信息,同时考虑拥有“超赞房东”徽章的整租房源。 展开更多
关键词 基于情感的信任 总评分 细节评分 评论一致性 入住意愿 共享短租 超赞房东 整租房源
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数字技术赋能职业教育评价路径及其对策研究
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作者 缪学梅 《青岛职业技术学院学报》 2024年第2期13-17,共5页
数字化是教育转型的重要载体和方向,随着数字技术与教育深度融合,新的数字教育形态正在涌现。传统教育评价主要存在评价方法简单粗糙、评价手段陈旧、评价内容片面、评价标准缺乏差异化、评价过程过分关注结果等问题。合理利用数字技术... 数字化是教育转型的重要载体和方向,随着数字技术与教育深度融合,新的数字教育形态正在涌现。传统教育评价主要存在评价方法简单粗糙、评价手段陈旧、评价内容片面、评价标准缺乏差异化、评价过程过分关注结果等问题。合理利用数字技术优势,解决当前职业教育评价过程中的难点堵点是时代发展的必然趋势。职业院校可以通过优化教育评价标准体系、引入信息技术培训资源、搭建数字技术教育评价平台、推广数字徽章与区块链技术、健全治理机制与隐私保护链等路径持续推进职业教育评价改革。 展开更多
关键词 数字技术 教育评价 数字徽章 评价路径
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