“素质教育”在《分析化学》实验课上的实践与研究

在《分析化学》实验课中要遵循实验教学规律,充分发挥教师的主导作用,对学生实际操作给予有计划、有针对性地指导,不做“巡逻兵”,不做顺手牵羊式的巡回指导。要重视实验课前的预习,培养学生良好的预习习惯。要将“严格要求”贯穿于实验教学的整个过程,保障实验活动的有序、有质量地进行,同时还要做好实验的总结。通过这样组织、实施实验课的教学,学生就可以在完成学习任务的同时,能力素质得到提高,为学生以后的学习发展奠定一定的能力基础。

《分析化学》实验教学改革探讨

分析化学是医学检验专业的基础课之一，学员能否正确规范使用仪器，对分析结果至关重要。几年来，我们不断改进实验教学，收到了较好的效果。

Computer Management of Quantitative Analysis Chemistry Experiment

The application of computer in the quantitative analysis chemistry experiment is a chemistry experiment teaching applications software, developed by Visual Basic （6.0）, based on the content of quantitative analysis chemistry experiment of chemistry major in higher institute. This software has the function of the automatic processing the experimental data, the automatic generation of test report copies, and the automatic evaluation of students＇ experimental results, which solve the reliability, objectivity and accuracy problems of the students＇ experiment data processing and evaluation, and avoid interference with human factors. The software has the characteristic of the easy installation, the easy operation, the strong practicability, pertinence, the systematicness and the running stability, so it provides a platform in the quantitative analysis chemistry experiment for the students＇ assessment system of automatic processing, and it has a high popularization value. The project＇s technical route design is reasonable, the research method is correct, and the experimental data processing results are reliable, which has reached the leading domestic level in the quantitative analysis chemistry experiment teaching field of computer data processing. And this project has been through the achievements appraisal of Gansu Provincial Sci. ＆ Tech. Department.

Experimental study and kinetic analysis of oxidant-free thermal-assisted UV digestion utilizing supported nano-TiO_2 photocatalyst for detection of total phosphorous

A novel thermal-assisted ultra-violet(UV) photocatalysis digestion method for the determination of total phosphorus(TP) in water samples was introduced in this work. The photocatalytic experiments for TP digestion were conducted using a 365 nm wavelength UV light and Ti O2 particles as the photocatalyst. Sodium tripolyphosphate and sodium glycerophosphate were used as the typical components of TP and the digested samples were then determined by spectrophotometry after phosphomolybdenum blue reaction. The effects of operational parameters such as reaction time and temperature were studied for the digestion of TP and the kinetic analysis of two typical components was performed in this paper. The pseudo-first-order rate constants k of two phosphorus compounds at different temperatures were obtained and the Arrhenius equation was employed to explain the effect of temperature on rate constant k. Compared with the conventional thermal digestion method for TP detection, it was found that the temperature was decreased from 120 °C to 60 °C with same conversion rate and time in this thermal-assisted UV digestion method, which enabled the digestion process work at normal pressure. Compared with the individual ultra-violet(UV) photocatalysis process, the digestion time was also decreased from several hours to half an hour using the thermal-assisted UV digestion method. This method will not lead to secondary pollution since no oxidant was needed in the thermal-assisted UV photocatalysis digestion process, which made it more compatible with electrochemical detection of TP.

Physicochemical Characterization of Water of Bir M＇Cherga Reservoir and Its Effluents

This study aims the physico-chemical characterization of surface water of the Bir M＇Cherga reservoir and its effluents which are located in Zaghouan governorate of Tunisia. It required measures in situ of physicochemical parameters and chemical analysis at laboratory of major element and nutritive salts. The results of this study revealed the presence of pollutants in the Miliane river at El Fahs area and the eutrophication of water in the Bit M＇Cherga reservoir. According to the classification of Stuyfzand and Piper, water in the wadis of Melah, Hdada, Miliane and Boudebbane respectively is brackish, salty, extremely hard, chlorinated, sulphated, calcic, and magnesic. Water in the Bir M＇Cherga reservoir is characterized by calcic facies chlorinated sulphated and sodic. Thus, the Bir M＇Cherga reservoir presents a worrying situation and a risk of qualitative degradation of its water.

Obtain Thematic Maps of Diyarbakir Basalt Aquifer＇s Water Quality Parameters with Using GIS Technique

In this study, groundwater quality and water features of Diyarbakir urban basalt aquifer which contains Baglar, Kayapmar, Sur and Yenisehir residential areas aimed to be determined. At this location, water wells opened for drinking water and irrigation water are used in the agricultural field. Therefore, in the study area, which opened in water samples taken from water wells were examined. It was reformed in the field, water samples were taken from the predrilled water wells. Water wells in the same coordinates are determined by Garmin etrex 30 handheld GPS system. Chemical analysis of water samples taken in the laboratory was made. The wells water＇s pH, Electrical Conductivity （EC） and Dissolved Solids （TDS） features were acquired by Portable Hanna HI 98125 pH/EC/TDS/℃ meter device at the field. At this study, basalt aquifer features are considered, and water quality and water chemical properties were determined in Diyarbakir city centre, pH, EC and TDS values of the water samples taken on site and those water chemical analyses were measured in the laboratory. Then, they were modelled by using ARC INFO 10.2.1 GIS programme and geostatistical analyst extension tool. At the end of this process, thematic map of Diyarbakir＇s basalt aquifer pH, EC and TDS were produced.

The optimal choice of chemotherapy regimens for patients with relapsed platinum-resistant epithelial ovarian cancer/primary peritoneal/fallopian tube cancer - protocol for a systematic review and network meta-analysis

Objective： Debulking surgery （residual disease of less than 1 cm） followed by platinum-taxane chemotherapy isthe current standard therapy for patients with epithelial ovarian cancer, primary peritoneal carcinoma and primaryfallopian cancer. But the prognosis remains poor. Several chemotherapy regimens could be selected for patientswith recrudescent cancer. However, the standard second chemotherapy regimen remains a subject of debate. Thepurpose of our study is to carry out a systematic review and network meta-analysis to compare the efficacy andsafety of different regimens for recurrent platinum-resistant ovarian cancer based on existing randomized controlledtrials （RCTs）. Methods and analysis： Medline, EMBASE, Cochrane Library and Cochrane Library databases,Science Citation Index Expanded, Conference Proceedings Citation Index-Science and ClinicalTrials.gov will besystematically searched for eligible studies. Randomized controlled trials （RCT） on chemotherapy, immune therapy,biological therapy, targeted therapy for recurrent platinum-resistant ovarian cancer with multiple outcome measureswill be included. The Cochrane Risk of Bias Tool will be used to assess the quality of included studies. The primaryoutcomes are overall survival and median survival time. The secondary outcomes include the safety and side effectsof these regimens. Direct meta-analysis and network meta-analysis （NMA） will be conducted to compare differentregimens. Conclusion： The results of this network meta-analysis will provide direct and indirect evidence oftreatments for recurrent platinum-resistant ovarian cancer, and it may provide a ranking of the chemotherapyregimens for patients and gynecological oncologists to help them select the best option.

Study on Using Mixed Fuel of Jet Fuel/Gasoline as Fuel of Gasoline Engine

This paper has integrated various methods such as laboratory physical and chemical analysis, engine bench test and actual road test, etc. to conduct a feasibility study on the emergency alternative fuel of gasoline by mixed jet fuel and gasoline. The study shows that both the evaporability and anti-knock quality decrease after mixing jet fuel with gasoline. While the mixing proportion increases, the engine power decreases and the fuel consumption increases gradually. When the proportion reaches 40%, the engine power drops by 5.3% to 11.7%, the fuel consumption rises by an average of 3.8%, and meantime the oil dilution and emission of the engine power become worse. Therefore, as for the gasoline engine, the mixed oil can only be used as emergency alternative fuel due to its harm to the engine.

Environmental Effects of Water Quality of Melendiz Stream and Mamasin Dam Site in Aksaray City in the Central Anatolia of Turkey

The main purpose of this study was to determine the changes in the water quality of Melendiz and Karasu streams, which recharge the Mamasin dam, and to evaluate its environmental impacts on the dam site that provides drinking water and irrigation demand in Aksaray city in the Central Anatolia of Turkey. The field researches were focused on estimating the main sources of contamination, determining and evaluating the changes in the water quality due to the direct wastewater discharges into the Melendiz and Karasu rivers, which recharge the Mamasin dam sites. During the study, water samples were collected from Melendiz and Karasu stream and Mamasin dam, and then, the physical and chemical analyses of water samples were conducted. The relevant in-situ and laboratory analyses were carried out during the dry and wet seasons. The results of the analyses showed that in term of the surface water quality criteria in terms of NO3-N value of both rivers and dam waters, the water quality is always considered as the 1st class in Melendiz stream, the 2nd class in Karasu stream and the 3rd class in Mamasin dam lake. Whereas, in terms of NO4-N values of both rivers and dam waters, the water quality is always considered as the 1st class in Melendiz stream, the 2nd-3rd class in Karasu stream. The total organic carbon （TOC） range for Karasu river is usually from 20 mg/L to 40 mg/L. The high value of organic matter in the Karasu stream can be explained by the availability of intensive green wetlands around this water resource. Finally, the Ministry of Forest and Water Authority give some suggestions for estimating protection zones of Melendiz stream and Mamasin basin＇s area, such as using the results of environmental tracers to investigate the agricultural contamination, including more sophisticated applications of multiple-tracer analyses to evaluate the travel time of contaminants and estimate the boundary of protection zones.