The time-varying difference-in-difference model is used to identify the impact of payment technology on residents’consumption,and the moderation effect analysis method is used to identify its mechanism.It is found th...The time-varying difference-in-difference model is used to identify the impact of payment technology on residents’consumption,and the moderation effect analysis method is used to identify its mechanism.It is found that payment technology promotes consumption capacity expansion and quality improvement(CEQI)through three pathways of alleviating liquidity constraints,reducing transaction costs and weakening the payment of pain.The parallel and serial mechanisms of the three are further explored.The effect of payment technology on the CEQI of residents’consumption shows obvious heterogeneity due to differences in urban and rural household registration and financial literacy.Based on the empirical research results and the national conditions of China,targeted policy recommendations are proposed from the demand side,the supply side and the technological side.展开更多
Aiming at the problems such as low reconstruction efficiency,fuzzy texture details,and difficult convergence of reconstruction network face image super-resolution reconstruction algorithms,a new super-resolution recon...Aiming at the problems such as low reconstruction efficiency,fuzzy texture details,and difficult convergence of reconstruction network face image super-resolution reconstruction algorithms,a new super-resolution reconstruction algorithm with residual concern was proposed.Firstly,to solve the influence of redundant and invalid information about the face image super-resolution reconstruction network,an attention mechanism was introduced into the feature extraction module of the network,which improved the feature utilization rate of the overall network.Secondly,to alleviate the problem of gradient disappearance,the adaptive residual was introduced into the network to make the network model easier to converge during training,and features were supplemented according to the needs during training.The experimental results showed that the proposed algorithm had better reconstruction performance,more facial details,and clearer texture in the reconstructed face image than the comparison algorithm.In objective evaluation,the proposed algorithm's peak signalto-noise ratio and structural similarity were also better than other algorithms.展开更多
In order to evaluate the spontaneous combustion hazard of sulfide concentrates in storage, three different kinds of sulfide concentrates (sulfur-rich sulfide concentrate, iron sulfide concentrate and copper sulfide c...In order to evaluate the spontaneous combustion hazard of sulfide concentrates in storage, three different kinds of sulfide concentrates (sulfur-rich sulfide concentrate, iron sulfide concentrate and copper sulfide concentrate) were obtained from a storage yard in Dongguashan Copper Mine, China. The reaction processes at different heating rates of 5, 10, 15, 20, and 25 ℃/min in air flow from ambient temperature to 1 000 ℃ were studied by TG-DTG-DSC analysis. By the peak temperatures of DTG curves, the whole reaction process for each sample was divided into different stages, and the corresponding apparent activation energies were calculated by the Ozawa-Flynn-Wall method. It is found that the reaction process of each sample is considerably complex; the apparent activation energy values change from 36 to 160 kJ/mol in different temperature ranges; sulfur-rich sulfide and iron sulfide concentrates have lower apparent activation energy than copper sulfide concentrate below 150 ℃; so they are more inclined to cause spontaneous combustion at ambient temperature.展开更多
Analysis of genetic main effects and genotype x environment (GE) interaction effects for brown rice weight (BRW) at four different filling stages in indica lice (Oryza sativa L.) was conducted for two-year experimenta...Analysis of genetic main effects and genotype x environment (GE) interaction effects for brown rice weight (BRW) at four different filling stages in indica lice (Oryza sativa L.) was conducted for two-year experimental data by using developmental genetic models and corresponding statistical approaches for quantitative traits of seeds in cereal crops. It was indicated that the genetic main effects and their GE interaction effects of triploid endosperm, cytoplasmic and diploid maternal plant genes were important for BRW at different filling stages of rice, especially for endosperm or maternal additive main effects and their additive interaction effects. Because of the higher additive effects and additive interaction effects for BRW at different filling stages, the better improving effects for this trait could be expected by selection in rice breeding. The results of conditional genetic variance components showed that the new expression of quantitative genes in endosperm and maternal plant for BRW was mostly found at all different filling stages of rice. The gene expression, however, was most active at the early filling stages especially for the first (1-7 d) and the second filling stages (8-14 d after flowering). The phenomena that some genes were spasmodically expressible among filling stages of rice were detected for some genetic effects especially for net cytoplasmic main effects or its interaction effects and net dominance main effects. Predicted genetic effects at different filling stages of rice showed that some parents such as V20 and Zuo 5 were better than others for improving the BRW.展开更多
The un-coincide coordinate error in the single-axis rotating fiber optic strap-down inertial navigation system(SINS) is analyzed. Firstly, a rotating modulation technology is presented for SINS. The method provides ...The un-coincide coordinate error in the single-axis rotating fiber optic strap-down inertial navigation system(SINS) is analyzed. Firstly, a rotating modulation technology is presented for SINS. The method provides the enhanced property of SINS when using the same-leveled inertial measurement units. Then, the rotating struc- ture modification is derived and augmented to resolve the un-modulated error-accumulated problem. As the insuf- ficient machine processing, the horizontal and the vertical errors on the machine surface are inevitable, and the in- volved coordinates are difficult to get the exact coincident. So, two major kinds of coordinate situation are stud- ied. The equivalent error models on gyro and acceleration outputs are built for each situation, and the impact is analyzed for compensation. The part of attitude and position error models caused by the built angle-rate error is established to calculate the un-eoincident impact. Considering these conditions of different gyro accuracy and mo- tion states simultaneously, numerical simulations are implemented. Results indicate that the SINS modulation ac- curacy is seriously affected by the combined factors on gyro accuracy and motion conditions.展开更多
In this paper we address the dynamics of compensation cutting process from both Laplace s frequency domain and the time domain of the first time, using the two computer aided analyzing softwares: MATLAB and SIMULI...In this paper we address the dynamics of compensation cutting process from both Laplace s frequency domain and the time domain of the first time, using the two computer aided analyzing softwares: MATLAB and SIMULINK. Theoretical analysis and simulation experiments firstly show that not only the systematical stiffness of workpiece, spindle and tools, but also the regenerated coefficient affects the compensation displacement effect. The results show that the SREC is practicable in reality to decease the spindle induced errors in many engineering applications such as hard boring through simulation and the preliminary experiment results.展开更多
Since real world communication channels are not error free, the coded data transmitted on them may be corrupted, and block based image coding systems are vulnerable to transmission impairment. So the best neighborh...Since real world communication channels are not error free, the coded data transmitted on them may be corrupted, and block based image coding systems are vulnerable to transmission impairment. So the best neighborhood match method using genetic algorithm is used to conceal the error blocks. Experimental results show that the searching space can be greatly reduced by using genetic algorithm compared with exhaustive searching method, and good image quality is achieved. The peak signal noise ratios(PSNRs) of the restored images are increased greatly.展开更多
This paper reports the effect of sol size on nanofiltration performances of sol–gel derived microporous zirconia membranes. Microstructure, pure water flux, molecular weight cut-off(MWCO) and salt retention of zircon...This paper reports the effect of sol size on nanofiltration performances of sol–gel derived microporous zirconia membranes. Microstructure, pure water flux, molecular weight cut-off(MWCO) and salt retention of zirconia membranes derived from zirconia sols with different sizes were characterized. Thermal evolution, phase composition, microstructure and chemical stability of unsupported zirconia membranes(powder) were determined by thermogravimetric and differential thermal analysis, X-ray diffraction, nitrogen adsorption–desorption and static solubility measurements. Results show that nanofiltration performance of zirconia membranes is highly dependent on sol size. The sol with an average size of 3.8 nm, which is smaller than the pore size of the γ-Al2O3support(pore size: 5–6 nm), forms a discontinuous zirconia separation layer because of excessive penetration of sol into the support. This zirconia membrane displays a MWCO value towards polyethylene glycol higher than 4000 Da. A smooth and defect-free zirconia membrane with a MWCO value of 1195 Da(pore size: 1.75 nm) and relative high retention rates towards Mg Cl2(76%) and Ca Cl2(64%) was successfully fabricated by dip-coating the sol with an appropriate size of 8.6 nm. Zirconia sol with an average size of 12 nm exhibits colloidal nature and forms a zirconia membrane with a MWCO value of 2332 Da(pore size: 2.47 nm). This promising microporous zirconia membrane presents sufficiently high chemical stability in a wide p H range of 1–12.展开更多
A promising preparation method for lithium hexafluorophosphate(LiPF6)was introduced.Phosphorus pentafluoride(PF5) was first prepared using CaF2 and P2O5 at 280℃for 3 h.LiPF6 was synthesized in acetonitrile solvent by...A promising preparation method for lithium hexafluorophosphate(LiPF6)was introduced.Phosphorus pentafluoride(PF5) was first prepared using CaF2 and P2O5 at 280℃for 3 h.LiPF6 was synthesized in acetonitrile solvent by LiF and PF5 at room temperature(20-30℃)for 4 h.The synthesized LiPF6 was characterized by infrared spectrometry and X-ray diffraction(XRD). Atomic absorption and ion chromatography results show that the purity of synthesized LiPF6 reaches 99.98%.Thermal stability of self-synthesized LiPF6 was analyzed by differential thermal analysis and thermogravimetry.The results indicate that the self-synthesized LiPF6 has higher purity,lower impurity contents and better thermal stability than the commercial LiPF6.展开更多
Because of the quantization noise introduced during the compression,super-resolution reconstruction(SRR)techniques are complicated for the compressed images.This paper aims to incorporate the prior knowledge of discre...Because of the quantization noise introduced during the compression,super-resolution reconstruction(SRR)techniques are complicated for the compressed images.This paper aims to incorporate the prior knowledge of discrete cosine transform(DCT)coefficients into modeling the quantization noise.The spatial covariance matrix of the quantization noise is estimated by utilizing the Laplacian distribution of the alternating current(AC)coefficients.After estimating the spatial joint covariance of overall noises for the imaging system,we propose a general Bayesian framework to enhance the resolution for compressed images.Experiments demonstrate the effectiveness of the proposed algorithm and show the superiority to previous methods in objective and subjective aspects.展开更多
Based on the orbit integration and orbit fitting method, the influence of the characters of the gravity model, with different precisions, on the movement of low Earth orbit satellites was studied. The way and the effe...Based on the orbit integration and orbit fitting method, the influence of the characters of the gravity model, with different precisions, on the movement of low Earth orbit satellites was studied. The way and the effect of absorbing the influence of gravity model error on CHAMP and GRACE satellite orbits, using linear and periodical empirical acceleration models and the so-called "pseudo-stochastic pulses" model, were also analyzed.展开更多
Maximum rate of food consumption (C max) was determined for juvenile Sebastodes fuscescens (Houttuyn) at water temperature of 10, 15, 20 and 25℃. The relationships of C max to the body weight (W) at each temperature ...Maximum rate of food consumption (C max) was determined for juvenile Sebastodes fuscescens (Houttuyn) at water temperature of 10, 15, 20 and 25℃. The relationships of C max to the body weight (W) at each temperature were described by a power equation: lnC max = a + b lnW. Covariance analysis revealed significant interaction of the temperature and body weight. The relationship of adjusted C max to water temperature (T) was described by a quadratic equation: C max =-0.369 + 0.456T - 0.0117T 2. The optimal feeding temperature calculated from this equation was 19.5℃. The coefficients of the multiple regression estimation relating C max to body weight (W) and water temperature (T) were given in the Table 2.展开更多
In order to improve tracking accuracy when initial estimate is inaccurate or outliers exist,a bearings-only tracking approach called the robust range-parameterized cubature Kalman filter(RRPCKF)was proposed.Firstly,th...In order to improve tracking accuracy when initial estimate is inaccurate or outliers exist,a bearings-only tracking approach called the robust range-parameterized cubature Kalman filter(RRPCKF)was proposed.Firstly,the robust extremal rule based on the pollution distribution was introduced to the cubature Kalman filter(CKF)framework.The improved Turkey weight function was subsequently constructed to identify the outliers whose weights were reduced by establishing equivalent innovation covariance matrix in the CKF.Furthermore,the improved range-parameterize(RP)strategy which divides the filter into some weighted robust CKFs each with a different initial estimate was utilized to solve the fuzzy initial estimation problem efficiently.Simulations show that the result of the RRPCKF is more accurate and more robust whether outliers exist or not,whereas that of the conventional algorithms becomes distorted seriously when outliers appear.展开更多
Double-wavelength recording used in a pulsed digital micro-holographic system to record ultra-fast processing of the order of femto-second is reported for the first time, where a BBO crystal is used to generate harmon...Double-wavelength recording used in a pulsed digital micro-holographic system to record ultra-fast processing of the order of femto-second is reported for the first time, where a BBO crystal is used to generate harmonic wave of the incident laser wave, and both of the basic and the frequency doubled waves are time-delayed and introduced to a Michelson's interferometer to record two sub-holograms with different spatial frequencies on a single frame of a CCD. In the experiment, an ultrafast dynamic process of air ionization induced by a single femto-second laser pulse is recorded with holography by this system, and both of intensity and phase difference images digitally reconstructed are obtained through Fourier transformation and digital faltering, which show clearly the dynamic process of formation and propagation of the plasma, with a time resolution of the order of femto-second.展开更多
In order to further clarify the spraying performance of siphonic nozzle, the spray rate of siponic cone nozzle with aperture of 1.0 mm was determined at 15 different air pressure levels and 12 gravity drop levels, and...In order to further clarify the spraying performance of siphonic nozzle, the spray rate of siponic cone nozzle with aperture of 1.0 mm was determined at 15 different air pressure levels and 12 gravity drop levels, and DPS and SPSS were used to make the difference analysis and modeling, which clarified the relationship between the spray rate of the siphonic cone nozzle with aperture of 1.0 mm and air pressure and gravity drop, getting the regression equation of Y=406.854P+ 1.904G+77.524. The study could provide a theoretical basis for the optimization and improvement of plant protection spraying equipment.展开更多
The heated process of raw materials for electron trapping materials (ETM) is investigated by thermo-analysis method. The temperature ranges of raw materials experienced some physical and chemical change processes, suc...The heated process of raw materials for electron trapping materials (ETM) is investigated by thermo-analysis method. The temperature ranges of raw materials experienced some physical and chemical change processes, such as dehydration, organic solvent removal, crystal sulphur burning, oxidation of alkaline earth sulfides and solid phase reaction (rare earth doped) and so on, are obtained. The experimental results also show that the presence of trace oxygen in shielded gas is very harmful to prepare the ETM.The raw material thermo-analysis results provide very important experimental reference for optimizing the ETM preparation techniques.展开更多
Based on the fact that 3-D model discretization by artificial could not always be successfully implemented especially for large-scaled problems when high accuracy and efficiency were required, a new adaptive multigrid...Based on the fact that 3-D model discretization by artificial could not always be successfully implemented especially for large-scaled problems when high accuracy and efficiency were required, a new adaptive multigrid finite element method was proposed. In this algorithm, a-posteriori error estimator was employed to generate adaptively refined mesh on a given initial mesh. On these iterative meshes, V-cycle based multigrid method was adopted to fast solve each linear equation with each initial iterative term interpolated from last mesh. With this error estimator, the unknowns were nearly optimally distributed on the final mesh which guaranteed the accuracy. The numerical results show that the multigrid solver is faster and more stable compared with ICCG solver. Meanwhile, the numerical results obtained from the final model discretization approximate the analytical solutions with maximal relative errors less than 1%, which remarkably validates this algorithm.展开更多
A new so called truncation error reduction method (TERM) is developed in this work. This is an iterative process which uses a coarse grid (2 h ) to estimate the truncation error and then reduces the error on the or...A new so called truncation error reduction method (TERM) is developed in this work. This is an iterative process which uses a coarse grid (2 h ) to estimate the truncation error and then reduces the error on the original grid ( h ). The purpose is to use coarse grids to get more accurate results and to develop a new method which could do coarse grid direct numerical simulation (DNS) for more accurate and acceptable DNS solutions.展开更多
The wide-field electromagnetic method is widely used in hydrocarbon exploration,mineral deposit detection,and geological disaster prediction.However,apparent resistivity and normalized field amplitude exceeding 2048 H...The wide-field electromagnetic method is widely used in hydrocarbon exploration,mineral deposit detection,and geological disaster prediction.However,apparent resistivity and normalized field amplitude exceeding 2048 Hz often exhibit upward warping in data,making geophysical inversion and interpretation challenging.The cumulative error of the crystal oscillator in signal transmission and acquisition contributes to an upturned apparent resistivity curve.To address this,a high-frequency information extraction method is proposed based on time-domain signal reconstruction,which helps to record a complete current data sequence;moreover,it helps estimate the crystal oscillator error for the transmitted signal.Considering the recorded error,a received signal was corrected using a set of reconstruction algorithms.After processing,the high-frequency component of the wide-field electromagnetic data was not upturned,while accurate high-frequency information was extracted from the signal.Therefore,the proposed method helped effectively extract high-frequency components of all wide-field electromagnetic data.展开更多
基金Foundation items:National Natural Science Foundation of China(No.71874027)Ministry of Education Humanities and Social Sciences Research Youth Fund Project(No.23YJC760028)。
文摘The time-varying difference-in-difference model is used to identify the impact of payment technology on residents’consumption,and the moderation effect analysis method is used to identify its mechanism.It is found that payment technology promotes consumption capacity expansion and quality improvement(CEQI)through three pathways of alleviating liquidity constraints,reducing transaction costs and weakening the payment of pain.The parallel and serial mechanisms of the three are further explored.The effect of payment technology on the CEQI of residents’consumption shows obvious heterogeneity due to differences in urban and rural household registration and financial literacy.Based on the empirical research results and the national conditions of China,targeted policy recommendations are proposed from the demand side,the supply side and the technological side.
基金supported by National Natural Science Foundation of China(No.62063014)。
文摘Aiming at the problems such as low reconstruction efficiency,fuzzy texture details,and difficult convergence of reconstruction network face image super-resolution reconstruction algorithms,a new super-resolution reconstruction algorithm with residual concern was proposed.Firstly,to solve the influence of redundant and invalid information about the face image super-resolution reconstruction network,an attention mechanism was introduced into the feature extraction module of the network,which improved the feature utilization rate of the overall network.Secondly,to alleviate the problem of gradient disappearance,the adaptive residual was introduced into the network to make the network model easier to converge during training,and features were supplemented according to the needs during training.The experimental results showed that the proposed algorithm had better reconstruction performance,more facial details,and clearer texture in the reconstructed face image than the comparison algorithm.In objective evaluation,the proposed algorithm's peak signalto-noise ratio and structural similarity were also better than other algorithms.
基金Project (2006BAK04B03) supported by the National Science and Technology Pillar Program during the 11th Five-Year Plan Period of ChinaProject (kjdb200902-7) supported by Doctoral Candidate Innovation Research Support Program of Science & Technology Review, China+1 种基金Project (1960-71131100023) supported by Postgraduate Dissertation Innovation Foundation of Central South University, ChinaProject (ZKJ2009008) supported by Precious Apparatus Opening Center Foundation of Central South University, China
文摘In order to evaluate the spontaneous combustion hazard of sulfide concentrates in storage, three different kinds of sulfide concentrates (sulfur-rich sulfide concentrate, iron sulfide concentrate and copper sulfide concentrate) were obtained from a storage yard in Dongguashan Copper Mine, China. The reaction processes at different heating rates of 5, 10, 15, 20, and 25 ℃/min in air flow from ambient temperature to 1 000 ℃ were studied by TG-DTG-DSC analysis. By the peak temperatures of DTG curves, the whole reaction process for each sample was divided into different stages, and the corresponding apparent activation energies were calculated by the Ozawa-Flynn-Wall method. It is found that the reaction process of each sample is considerably complex; the apparent activation energy values change from 36 to 160 kJ/mol in different temperature ranges; sulfur-rich sulfide and iron sulfide concentrates have lower apparent activation energy than copper sulfide concentrate below 150 ℃; so they are more inclined to cause spontaneous combustion at ambient temperature.
文摘Analysis of genetic main effects and genotype x environment (GE) interaction effects for brown rice weight (BRW) at four different filling stages in indica lice (Oryza sativa L.) was conducted for two-year experimental data by using developmental genetic models and corresponding statistical approaches for quantitative traits of seeds in cereal crops. It was indicated that the genetic main effects and their GE interaction effects of triploid endosperm, cytoplasmic and diploid maternal plant genes were important for BRW at different filling stages of rice, especially for endosperm or maternal additive main effects and their additive interaction effects. Because of the higher additive effects and additive interaction effects for BRW at different filling stages, the better improving effects for this trait could be expected by selection in rice breeding. The results of conditional genetic variance components showed that the new expression of quantitative genes in endosperm and maternal plant for BRW was mostly found at all different filling stages of rice. The gene expression, however, was most active at the early filling stages especially for the first (1-7 d) and the second filling stages (8-14 d after flowering). The phenomena that some genes were spasmodically expressible among filling stages of rice were detected for some genetic effects especially for net cytoplasmic main effects or its interaction effects and net dominance main effects. Predicted genetic effects at different filling stages of rice showed that some parents such as V20 and Zuo 5 were better than others for improving the BRW.
基金Supported by the National Natural Science Foundation of China(60702003)the Aviation Science Foundation(20080852011)+1 种基金the Specialized Research Fund for the Doctoral Program of Higher Education of China(20070287045)the NUAA Research Fundation(NS2010066)~~
文摘The un-coincide coordinate error in the single-axis rotating fiber optic strap-down inertial navigation system(SINS) is analyzed. Firstly, a rotating modulation technology is presented for SINS. The method provides the enhanced property of SINS when using the same-leveled inertial measurement units. Then, the rotating struc- ture modification is derived and augmented to resolve the un-modulated error-accumulated problem. As the insuf- ficient machine processing, the horizontal and the vertical errors on the machine surface are inevitable, and the in- volved coordinates are difficult to get the exact coincident. So, two major kinds of coordinate situation are stud- ied. The equivalent error models on gyro and acceleration outputs are built for each situation, and the impact is analyzed for compensation. The part of attitude and position error models caused by the built angle-rate error is established to calculate the un-eoincident impact. Considering these conditions of different gyro accuracy and mo- tion states simultaneously, numerical simulations are implemented. Results indicate that the SINS modulation ac- curacy is seriously affected by the combined factors on gyro accuracy and motion conditions.
文摘In this paper we address the dynamics of compensation cutting process from both Laplace s frequency domain and the time domain of the first time, using the two computer aided analyzing softwares: MATLAB and SIMULINK. Theoretical analysis and simulation experiments firstly show that not only the systematical stiffness of workpiece, spindle and tools, but also the regenerated coefficient affects the compensation displacement effect. The results show that the SREC is practicable in reality to decease the spindle induced errors in many engineering applications such as hard boring through simulation and the preliminary experiment results.
文摘Since real world communication channels are not error free, the coded data transmitted on them may be corrupted, and block based image coding systems are vulnerable to transmission impairment. So the best neighborhood match method using genetic algorithm is used to conceal the error blocks. Experimental results show that the searching space can be greatly reduced by using genetic algorithm compared with exhaustive searching method, and good image quality is achieved. The peak signal noise ratios(PSNRs) of the restored images are increased greatly.
基金Supported by the National Natural Science Foundation of China(20906047,21276123)the National High Technology Research and Development Program of China(2012AA03A606)+3 种基金State Key Laboratory of Materials-Oriented Chemical Engineering(ZK201002)the Natural Science Research Plan of Jiangsu Universities(11KJB530006)the"Summit of the Six Top Talents"Program of Jiangsu Provincea Project Funded by the Priority Academic Program development of Jiangsu Higher Education Institutions(PAPD)
文摘This paper reports the effect of sol size on nanofiltration performances of sol–gel derived microporous zirconia membranes. Microstructure, pure water flux, molecular weight cut-off(MWCO) and salt retention of zirconia membranes derived from zirconia sols with different sizes were characterized. Thermal evolution, phase composition, microstructure and chemical stability of unsupported zirconia membranes(powder) were determined by thermogravimetric and differential thermal analysis, X-ray diffraction, nitrogen adsorption–desorption and static solubility measurements. Results show that nanofiltration performance of zirconia membranes is highly dependent on sol size. The sol with an average size of 3.8 nm, which is smaller than the pore size of the γ-Al2O3support(pore size: 5–6 nm), forms a discontinuous zirconia separation layer because of excessive penetration of sol into the support. This zirconia membrane displays a MWCO value towards polyethylene glycol higher than 4000 Da. A smooth and defect-free zirconia membrane with a MWCO value of 1195 Da(pore size: 1.75 nm) and relative high retention rates towards Mg Cl2(76%) and Ca Cl2(64%) was successfully fabricated by dip-coating the sol with an appropriate size of 8.6 nm. Zirconia sol with an average size of 12 nm exhibits colloidal nature and forms a zirconia membrane with a MWCO value of 2332 Da(pore size: 2.47 nm). This promising microporous zirconia membrane presents sufficiently high chemical stability in a wide p H range of 1–12.
基金Project(2007CB613607)supported by the National Basic Research Program of China
文摘A promising preparation method for lithium hexafluorophosphate(LiPF6)was introduced.Phosphorus pentafluoride(PF5) was first prepared using CaF2 and P2O5 at 280℃for 3 h.LiPF6 was synthesized in acetonitrile solvent by LiF and PF5 at room temperature(20-30℃)for 4 h.The synthesized LiPF6 was characterized by infrared spectrometry and X-ray diffraction(XRD). Atomic absorption and ion chromatography results show that the purity of synthesized LiPF6 reaches 99.98%.Thermal stability of self-synthesized LiPF6 was analyzed by differential thermal analysis and thermogravimetry.The results indicate that the self-synthesized LiPF6 has higher purity,lower impurity contents and better thermal stability than the commercial LiPF6.
基金The Advanced Research of Shanghai Technical Committee(No.03DZ05020)
文摘Because of the quantization noise introduced during the compression,super-resolution reconstruction(SRR)techniques are complicated for the compressed images.This paper aims to incorporate the prior knowledge of discrete cosine transform(DCT)coefficients into modeling the quantization noise.The spatial covariance matrix of the quantization noise is estimated by utilizing the Laplacian distribution of the alternating current(AC)coefficients.After estimating the spatial joint covariance of overall noises for the imaging system,we propose a general Bayesian framework to enhance the resolution for compressed images.Experiments demonstrate the effectiveness of the proposed algorithm and show the superiority to previous methods in objective and subjective aspects.
基金Funded by the Natural Science Foundation of China (No. 40504002)the 973 Program of China (No. 2006CB701301).
文摘Based on the orbit integration and orbit fitting method, the influence of the characters of the gravity model, with different precisions, on the movement of low Earth orbit satellites was studied. The way and the effect of absorbing the influence of gravity model error on CHAMP and GRACE satellite orbits, using linear and periodical empirical acceleration models and the so-called "pseudo-stochastic pulses" model, were also analyzed.
文摘Maximum rate of food consumption (C max) was determined for juvenile Sebastodes fuscescens (Houttuyn) at water temperature of 10, 15, 20 and 25℃. The relationships of C max to the body weight (W) at each temperature were described by a power equation: lnC max = a + b lnW. Covariance analysis revealed significant interaction of the temperature and body weight. The relationship of adjusted C max to water temperature (T) was described by a quadratic equation: C max =-0.369 + 0.456T - 0.0117T 2. The optimal feeding temperature calculated from this equation was 19.5℃. The coefficients of the multiple regression estimation relating C max to body weight (W) and water temperature (T) were given in the Table 2.
基金Projects(51377172,51577191) supported by the National Natural Science Foundation of China
文摘In order to improve tracking accuracy when initial estimate is inaccurate or outliers exist,a bearings-only tracking approach called the robust range-parameterized cubature Kalman filter(RRPCKF)was proposed.Firstly,the robust extremal rule based on the pollution distribution was introduced to the cubature Kalman filter(CKF)framework.The improved Turkey weight function was subsequently constructed to identify the outliers whose weights were reduced by establishing equivalent innovation covariance matrix in the CKF.Furthermore,the improved range-parameterize(RP)strategy which divides the filter into some weighted robust CKFs each with a different initial estimate was utilized to solve the fuzzy initial estimation problem efficiently.Simulations show that the result of the RRPCKF is more accurate and more robust whether outliers exist or not,whereas that of the conventional algorithms becomes distorted seriously when outliers appear.
基金This work is financially supported by the National Natural Sci-ence Foundation of China (Grant No. 60377008)
文摘Double-wavelength recording used in a pulsed digital micro-holographic system to record ultra-fast processing of the order of femto-second is reported for the first time, where a BBO crystal is used to generate harmonic wave of the incident laser wave, and both of the basic and the frequency doubled waves are time-delayed and introduced to a Michelson's interferometer to record two sub-holograms with different spatial frequencies on a single frame of a CCD. In the experiment, an ultrafast dynamic process of air ionization induced by a single femto-second laser pulse is recorded with holography by this system, and both of intensity and phase difference images digitally reconstructed are obtained through Fourier transformation and digital faltering, which show clearly the dynamic process of formation and propagation of the plasma, with a time resolution of the order of femto-second.
基金Supported by the Special Key Fund for Science and Technology of Anhui Province(15CZZ03132)the Special Fund for Talent Development of Anhui Province(13C1109)the Agricultural Science and Technology Innovation Fund Project of Anhui Province(16A1132)~~
文摘In order to further clarify the spraying performance of siphonic nozzle, the spray rate of siponic cone nozzle with aperture of 1.0 mm was determined at 15 different air pressure levels and 12 gravity drop levels, and DPS and SPSS were used to make the difference analysis and modeling, which clarified the relationship between the spray rate of the siphonic cone nozzle with aperture of 1.0 mm and air pressure and gravity drop, getting the regression equation of Y=406.854P+ 1.904G+77.524. The study could provide a theoretical basis for the optimization and improvement of plant protection spraying equipment.
文摘The heated process of raw materials for electron trapping materials (ETM) is investigated by thermo-analysis method. The temperature ranges of raw materials experienced some physical and chemical change processes, such as dehydration, organic solvent removal, crystal sulphur burning, oxidation of alkaline earth sulfides and solid phase reaction (rare earth doped) and so on, are obtained. The experimental results also show that the presence of trace oxygen in shielded gas is very harmful to prepare the ETM.The raw material thermo-analysis results provide very important experimental reference for optimizing the ETM preparation techniques.
基金Projects(2006AA06Z105, 2007AA06Z134) supported by the National High-Tech Research and Development Program of ChinaProjects(2007, 2008) supported by China Scholarship Council (CSC)
文摘Based on the fact that 3-D model discretization by artificial could not always be successfully implemented especially for large-scaled problems when high accuracy and efficiency were required, a new adaptive multigrid finite element method was proposed. In this algorithm, a-posteriori error estimator was employed to generate adaptively refined mesh on a given initial mesh. On these iterative meshes, V-cycle based multigrid method was adopted to fast solve each linear equation with each initial iterative term interpolated from last mesh. With this error estimator, the unknowns were nearly optimally distributed on the final mesh which guaranteed the accuracy. The numerical results show that the multigrid solver is faster and more stable compared with ICCG solver. Meanwhile, the numerical results obtained from the final model discretization approximate the analytical solutions with maximal relative errors less than 1%, which remarkably validates this algorithm.
文摘A new so called truncation error reduction method (TERM) is developed in this work. This is an iterative process which uses a coarse grid (2 h ) to estimate the truncation error and then reduces the error on the original grid ( h ). The purpose is to use coarse grids to get more accurate results and to develop a new method which could do coarse grid direct numerical simulation (DNS) for more accurate and acceptable DNS solutions.
基金Project(42004056)supported by the National Natural Science Foundation of ChinaProject(ZR2020QD052)supported by the Natural Science Foundation of Shandong Province,ChinaProject(2019YFC0604902)supported by the National Key Research and Development Program of China。
文摘The wide-field electromagnetic method is widely used in hydrocarbon exploration,mineral deposit detection,and geological disaster prediction.However,apparent resistivity and normalized field amplitude exceeding 2048 Hz often exhibit upward warping in data,making geophysical inversion and interpretation challenging.The cumulative error of the crystal oscillator in signal transmission and acquisition contributes to an upturned apparent resistivity curve.To address this,a high-frequency information extraction method is proposed based on time-domain signal reconstruction,which helps to record a complete current data sequence;moreover,it helps estimate the crystal oscillator error for the transmitted signal.Considering the recorded error,a received signal was corrected using a set of reconstruction algorithms.After processing,the high-frequency component of the wide-field electromagnetic data was not upturned,while accurate high-frequency information was extracted from the signal.Therefore,the proposed method helped effectively extract high-frequency components of all wide-field electromagnetic data.