The Spurge family (Euphorbiaceae) is a large family of flowering plants. Two plant species of this family were collected from the Egyptian desert, extracted with methanol subjected to silica gel column chromatograph...The Spurge family (Euphorbiaceae) is a large family of flowering plants. Two plant species of this family were collected from the Egyptian desert, extracted with methanol subjected to silica gel column chromatography to give six compounds, three compounds from each plant. The compounds isolated from the methanol extract of Euphorbia retusa Forssk were identified as kaempferol-3-beta-D glucopyranosyl (1), 3-O-alpha-L-xylopyranosyl (1→3)-alpha-L xylopyranosyl (1→2), beta-D glucopyranosyllup 1,12-diene-3,21-diol (2) and 5,7,8,3',4'-pentahydroxy-3-methoxyflavone (3) and the compounds isolated from Euphorbia paralais L. identified as 3,5,3'-trihydroxy-6,7-d-methoxy-4' (7"-hydroxygeranyl-1"-ether) flavones (4), 3-O-syringic acid (1→4)-alpha-L- xylopyranosyl (1→3), beta-D-rahminopyranosyl hederagenin (5) and 3-O-syringic acid (1→4), beta-D-rahminopyranosyl (1→3),beta-D-rahminopyranosyl hederagenin (6). The structure of the isolated compounds was elucidated by chemical and spectrometric analysis such as Infera red (IR), proton and carbon nuclear magnetic resonance (1H-, 13C-NMR) and chemical ionization mass spectrometry (CI-MS).展开更多
文摘The Spurge family (Euphorbiaceae) is a large family of flowering plants. Two plant species of this family were collected from the Egyptian desert, extracted with methanol subjected to silica gel column chromatography to give six compounds, three compounds from each plant. The compounds isolated from the methanol extract of Euphorbia retusa Forssk were identified as kaempferol-3-beta-D glucopyranosyl (1), 3-O-alpha-L-xylopyranosyl (1→3)-alpha-L xylopyranosyl (1→2), beta-D glucopyranosyllup 1,12-diene-3,21-diol (2) and 5,7,8,3',4'-pentahydroxy-3-methoxyflavone (3) and the compounds isolated from Euphorbia paralais L. identified as 3,5,3'-trihydroxy-6,7-d-methoxy-4' (7"-hydroxygeranyl-1"-ether) flavones (4), 3-O-syringic acid (1→4)-alpha-L- xylopyranosyl (1→3), beta-D-rahminopyranosyl hederagenin (5) and 3-O-syringic acid (1→4), beta-D-rahminopyranosyl (1→3),beta-D-rahminopyranosyl hederagenin (6). The structure of the isolated compounds was elucidated by chemical and spectrometric analysis such as Infera red (IR), proton and carbon nuclear magnetic resonance (1H-, 13C-NMR) and chemical ionization mass spectrometry (CI-MS).