钢中不稳定和微细析出相定量分析时的清洗方法

本文研究了相分析清洗过程误差的来源和减小的方法。发现传统的清洗方法不适用于不稳定和微细相的分析,必须加以改进。因为这种清洗过程中由于析出物的分解和损失造成的误差远大于清洗企图减小的误差。

非定常不稳定气固两相流动的离散涡数值仿真 Ⅲ .非定常不稳定气固两相流动中颗粒运动与旋涡的相关结构

基于气固两相流动的离散涡模型与数值仿真方法,分别模拟了与重力方向垂直和与重力方向平行的平面内气固两相圆柱绕流(其中颗粒的St数为1.0),得到了流场中颗粒分布与旋涡分布的时间序列,由此进一步证明了高雷诺数下的二维气固两相流动中固体颗粒运动与流体旋涡存在着明确的相关结构:气体流经圆柱体时产生不稳定的剧烈分离流动,在圆柱绕流的尾迹区内存在着复杂的旋涡发展演化过程,由于流体旋涡对其周围固体颗粒的诱导作用,使得在尾迹区内中等尺度(St～o(1.0))的固体颗粒从均匀气固混合物中分离出来而往旋涡区运动,并最终在旋涡结构的外沿聚集.

60Si_2MnREB弹簧钢中的碳硼化相的研究

使用X射线衍射和电子探针微区分析方法对 6 0Si2 MnREB弹簧钢中的碳硼相进行了综合分析 .当样品中的硼含量超过 0 .0 0 3% ,在 85 0℃淬火后 ,沿奥氏体晶界出现不连续的Fe2 3 (B ,C)网 ,使材质变脆 .95 0℃正火后 ,晶界仅有少量粒状Fe3 (B ,C)相存在 .研究了这两种碳硼相的析出与转变机制 .

Effects of Xin Mai Tong Capsule on Vasoregulatory Peptides in the Patients of Coronary Heart Disease

In order to inquire into the therapeutic effects of Xin Mai Tong Capsule (心脉通胶囊) on coronary heart disease with myocardial ischemia, 40 patients were randomly divided into two groups (Xin Mai Tong group and the control group). The plasma endothelin (ET) levels in the two groups of patients were markedly higher than that of the healthy people (P<0.001), and the calcitonin gene related peptide (CGRP) was similar to that of the healthy people (P>0.05). After treatment, ET and symptomatic scores in the two groups decreased markedly (P<0.01), and their S-T segments were elevated obviously (P<0.01). But the decrease of ET and symptomatic scores and elevation of S-T segment in Xin Mai Tong group were superior to those of the control group (P<0.05～0.01). The CGRP level in the control group did not vary obviously post-treatment, but it increased markedly (P<0.01) with the addition of Xin Mai Tong Capsule in Xin Mai Tong group.

Magnetoelastic Instability in Ring-Shaped Molecule Magnets with Next-Nearest Neighbor Coupling

In considering next-nearest neighbor （NNN） coupling, we numerically investigate the magnetoelastic instability in ring-shaped mesoscopic antiferromagnetic Heisenberg spin 1/2 systems with spin-phonon interaction. The results indicate that, for antiferromagnetic NNN coupling J2, there may be a critical value J2^c, at which the ground state is dimerized for arbitrary lattice spring constant and beyond and below which the magnetoelastic instability behavior is different from each other. The values of J2^c are irrelevant to the system size. For ferromagnetic NNN coupling, only continuous transition is present from dimerized phase to uniform phase as lattice spring constant is increased.

Modulational Instability of Ion—Acoustic Waves in a Warm Plasma with a Relativistic Electron Beam

The modulational instability of ion-acoustic wave in a collisionless, unmagnetized plasma consisting of warm ions, hot isothermal electrons, and relativistic electron beam is studied. A modified nonlinear Schr?dinger equation including one additional term that comes from the effect of relativistic electron beam is derived. It is found that the inclusion of a relativistic electron beam would modify the modulational instability of the wave packet and could not admit any stationary soliton waves.

Charge Densities of Unstable Nuclei with Electron Scattering

Relativistic mean-field theory and phase-shift analysis are combined together to investigate the elasticCoulomb scattering between electrons and unstable nuclei.Electron scattering at several different energies is studiedand compared,in order to see the energy dependence of electron-nucleus scattering.It is shown that electron scattering at200 MeV or 300 MeV can be used to reveal electron-nucleus scattering information around the first diffraction minimum-Shiftsin opposite directions are obtained for the first diffraction minima of the electron scattering off the ground andfirst excited states of ^(17)F with ^(16)O as reference,and similar effects are obtained for ^(18)Ne.Besides,some neutron-richN = 8 isotones are also studied.Results show that electron scattering will be very useful and important in studyingboth proton- and neutron-rich nuclei in the future.

Mass Spectrometric Characterization of a Thermolabile Metabolite of Camazepam

Incubation of camazepam [3-(N,N-dimethyl) carbamoyloxy-7-chloro-1- methyl-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-one] with rat liver microsomes and cofactors produced a 3-(N-methyl-N-hydroxymethyl) carbamoyloxy derivative as the most abundant metabolite.This metabolite was thermally unstable and was isolated from a metabolite mixture by normal-phase High-Performance Liquid Chromatography.Its struc- ture was established by chemical ionization and ^(252)Cf plasma desorption time-of-flight mass spectral analyses.

State of Pepsin and Acidic Protease in Solid Phase System and the Factors Increasing Their Destabilization

The adsorption state and catalytic properties of pepsin and acidic protease from microorganisms Asp. awamori and Asp. oryzae were studied in solid phase system （in presence of sorsilen, DEAE- and CM-cellulose）. According to the results, adsorption capacity and catalytic activity of enzymes depend on the physical nature of surface groups of the solid phase. Changing the stability of enzymes in the system with solid phase is observed even the adsorption bond is less stable （in the case of DEAE- and CM-cellulose in acidic media）. Injection to the medium ethanol, surfactants, sodium chloride and changing the temperature of the incubation medium could prevent the negative effects of the solid phases. When sorsilen is used as solid phase, pepsin and acidic protease from Asp. awamori suffer from high surface inactivation. Various surfactants influence adsorption state of enzymes differently. Non-ionic surfactants （Triton X-100） prevent adsorption and restore catalytic properties of enzymes.

On Relative Stability in 4-Dimensional Duck Solution

This paper gives the existence of a relatively stable duck solution in a slow-fast system in R2＋2 with an invariant manifold. The slow-fast system in R2＋： has a 2-dimensional slow vector field and a 2-dimensional fast vector field. The fast vector field restricts a feasible region of the slow vector field strictly. In the case of the slow-fast system in R2＋1 , that is, the fast vector field is l-dimension, it is classified according to its sign, because it gives only negative（-）, positive（＋） or zero sign. Then it is attractive, repulsive or stationary. On the other hand, in R2~2 , the fast vector field has combinatorial cases. It causes a complex state to analyze the system. First, we introduce a local model near the pseudo singular point on which we classify the fast vector field attractive（-,-）, attractive-repulsive（-,＋） or repulsive（＋,＋）, simply as possible. We prove the existence of a 4-dimensional duck solution in the local model. Secondarily, we assume that the slow-fast system has an invariant manifold near the pseudo singular point. When the invariant manifold has a homoclinic point near the pseudo singular point, we show that the slow-fast sytem has a 4-dimensional duck solution having a relatively stable region.

Attributional Styles in Adolescents with Transfusion-dependent Thalassemia

This study focused on the way that Adolescents with Transfusion- dependent thalassemia explained negative or positive events in their life （Attributional Styles）. It is defined by three dimensions describing the cognitive appraisal of the events： internal-external, stable-unstable, and global-specific. With cross-sectional research design, the observations consist of 102 adolescents （48 males, 54 females） who diagnosed with Transfusion-dependent thalassemia （more than 50 times for blood transfusions） completed the measure of Attributional Styles and Anxiety Questionnaires. The correlations in the predicted directions among variables examine with Pearson product-moment correlation coefficients, t-test, and One-way ANOVA to ascertain a significant between the group differences on attributional factors and levels of anxiety symptoms. The results show that Adolescent samples with higher levels of anxiety revealed statistically significant relationship among three negative attributional dimensions （overall composite F = 4.5, p 〈 0.05; negative composite F = 4.99, p 〈 0.01; negative-internality F = 4.99 p 〈 0.01; negative-stability F = 3.42, p 〈 0.05 and negative-globality F = 3.77, p 〈 0.05）. In addition, significant age- group differences were found for the total negative-globality （t = 2.05, p 〈 0.05） and negative- globality （t = -2.22, p 〈 0.05）. These data are consistent with the reformulated learned helplessness model of depression. In finding, the individuals who attribute negative life events to internal, stable, and global causes will be more vulnerable to anxiety than those who make external, unstable, and specific attributions. Most interestingly, those adolescents more than 17 years evidence more negative-globality attfibutional style than group less than 16 years, and female adolescents may influence this pattern. These results suggest that targeting Adolescents with Transfusion-dependent thalassemia may be important for improving aspect of coping on psychological adjustment to their chronic illness.

原子核多重碎裂的静态理论I.相变和多重碎裂

在温度、密度和动量相关的平均场下，对有限核１９７Ａｕ，得到了其状态方程的５个不同的相，即液相、汽相、超热液相、超冷汽相和力学不稳定相，当温度Ｔ＝６ＭｅＶ时，在坐标和动量空间对这些相进行了模拟，并采用并合模型对形成的核碎片进行了分类，关联分析表明。

Influence of the instability of angular velocity of the rotating carrier itself on the stability of silicon micromachined gyroscope

In order to find out the influence of the instability of angular velocity of the rotating carrier itself on the stability of silicon micromachined gyroscope, the digital models for relative error of the high and low damping gyroscope's output signal are given respectively, based on the motion equations of the silicon micromachined gyroscope. Theory proves that the output signal error of the silicon micromachined sensor is mainly caused by the instability of damping factor and the angular velocity of the rotating carrier itself. The experiment result indicates that the error of proportionality coefficient of output voltage which is caused by the instability of the angular velocity of the rotating carrier itself reaches to 4.1 %. Theoretical demonstration and experimental verification show that the instability of angular velocity of the rotating carrier itself has an important effect on the stability of low damping silicon micromachined gyroscope.

1070℃热暴露对一种单晶高温合金组织的影响

研究了一种镍基单晶高温合金在1 070℃热暴露不同时间后的组织变化。结果表明:合金的热处理组织由立方化较好γ'相和基体γ相组成。经过1 070℃热暴露处理后,γ相基体通道宽度增加,γ'强化相合并长大;热暴露200 h后,合金没有析出不稳定相(TCP相)。热暴露400 h后,少量TCP相开始在枝晶干区域以细针状的形态析出。经过800 h处理后,显微组织呈现出明显的筏排结构。随热暴露时间增加TCP相析出量明显增多,并由枝晶干范围向枝晶间区域生长。TCP相含有Re、W、Mo和Co等合金元素,衍射分析为σ相,与合金基体取向关系为(110)_σ∥(220)_γ,[012]_σ∥[001]_γ。

Experimental Investigation of Forced Convective Boiling Flow Instabilities in Horizontal Helically Coiled Tubes

An experimental investigation is described for the characteristics of convective boiling flow instabilities in horizontally helically coiled tubes using a steam-water two-phase closed circulation test loop at pressure from 0.5 MPa to 3.5 MPa. Three kinds of oscillation are reported: density waves; pressure drop excursions; thermal fluctuations. We describe their dependence on main system parameters such as system pressure, mass flowrate, inlet subcooling, compressible volume and heat flux. Utilizing the experimental data together with conservation constraints, a dimensionless correlation is proposed for the occurrence of density waves.

Natures of Rotating Stall Cell in a Diagonal Flow Fan

In order to clarify the natures of a rotating stall cell, the experimental investigation was carried out in a high specific-speed diagonal flow fan. The pressure field on the casing wall and the velocity fields at the rotor inlet and outlet were measured under rotating stall condition with a fast response pressure transducer and a single slant hot-wire probe, respectively. The data were processed using the “Double Phase-Locked Averaging (DPLA)”technique, which enabled to obtain the unsteady flow field with a rotating stall cell in the relative co-ordinate system fixed to the rotor. As a result, the structure and behavior of the rotating stall cell in a high specific-speed diagonal flow fan were shown.

Slip synergism of planar strike-slip fault during meta-instable state:Experimental research based on digital image correlation analysis

The meta-instable state(MIS)is the final stage before fault instability during stick-slip movement.Thus,identification of MIS is of great significance for assessing earthquake hazard in fault zones.A rock sample with a precut planar fault was loaded on a horizontally biaxial servo-controlled press machine to create stick-slip conditions.Digital images of the sample surface were taken by a high-speed camera at a rate of 1000 frames per second during the stick-slip motion and processed using a 2D digital image correlation method to obtain the displacement field.We define a synergism coefficient that describes the relative dispersion of the accumulative fault slip.The results reveal that:(1)a local pre-slip area spreads very slowly along the fault before the MIS develops.It extends at a higher but still slow speed during meta-instable state I(MIS-I).During the final^1.5%of MIS,in meta-instable state II(MIS-II),the local pre-slip area first extends at a speed of^0.9 m/s,and then expands out of the observed image area at a very high speed.These results indicate that the local pre-slip area transforms from a state of quasi-static extension in MIS-I to quasi-dynamic extension in MIS-II.(2)The synergism coefficient of the fault slip decreases to half of its original value in MIS-I and to a quarter of its original value in MIS-II.This continuous decrease of synergism coefficient indicates that the strengthening of fault slip synergism is a characteristic of MIS.(3)Furthermore,the unstable sliding stage includes three sliding processes:initial-,fast-,and adjusted-sliding.There are two pauses between the three sliding processes.

Relay camera videometrics based conversion method for unstable platform to static reference

This article proposes a relay camera videometrics based method to convert an unstable measuring platform to a static reference to solve the problems of large error or invalidation caused by measuring platform instability in photogrammetric and videometric measurements.The method installs a relay camera on the unstable platform and captures images of a reference marker fixed on a static reference or vice versa to resolve the 3D movement of the unstable platform relative to the static reference,based on which it corrects the error of the measured results and thus eliminating the influence of the platform movement.It finds new and important applications for videometrics by making high-precision dynamic measurement possible on unstable platforms.Verification experiments and numerical simulations have proven its validity and practicability.

Experimental Investigation of Boiling Two-phase Flow Instability of Nitrogen in a Vertical Tube

Boiling flow instability of nitrogen in a vertical tube is experimentally investigated in the present study. The experiments reveal that pressure has a significant effect on the characteristics of the heat flux-mass flux type boiling flow instability.First.the pressure has strong effects on both the developing time and the fluctuation amplitude.Especially increasing pressure leads to decrease the fluctuating amplitude of mass flux.Then,the mass flux evolving curves under different pressures feature out a shape like a leaf.The characteristics of the heat flux-mass flux type boiling flow instability under lower pressure are very complicated,however,with increasing pressure,this type of instability is gradually suppressed.

Weibel Instability Growth Rate in Magnetized Plasmas with Quasi-Relativistic Distribution Function

The mechanism of the Weibel instability is investigated for dense magnetized plasmas. As we know, due to the electron velocity distribution, the Coulomb collision effect of electron-ion and the relativistic properties play an important role in such study. In this study an analytical expression for the growth rate and the condition of restricting the Weibel instability are derived for low-frequency limit. These calculations are done for the oscillation frequency dependence on the electron cyclotron frequency. It is shown that, the relativistic properties of the particle lead to increasing the growth rate of the instability. On the other hand the collision effects and background magnetic field try to decrease the growth rate by decreasing the temperature anisotropy and restricting the particles movement.