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气相色谱–质谱联用法测定一次性使用空心纤维血液透析器中二酚基丙烷的溶出量
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作者 徐梦瑶 柳小军 +4 位作者 杨伟芳 张菁 田林奇 肖月丽 高誉鹏 《化学推进剂与高分子材料》 CAS 2023年第6期65-68,共4页
确立了测定在模拟临床试验条件下血液透析器中二酚基丙烷(BPA)溶出量的气相色谱–质谱联用法,模拟浸提溶液用体积分数为40%的乙醇/水混合溶液。实验论证,此方法在BPA质量浓度为0.02~10.0 mg/L时,BPA质量浓度与峰面积存在着良好的线性关... 确立了测定在模拟临床试验条件下血液透析器中二酚基丙烷(BPA)溶出量的气相色谱–质谱联用法,模拟浸提溶液用体积分数为40%的乙醇/水混合溶液。实验论证,此方法在BPA质量浓度为0.02~10.0 mg/L时,BPA质量浓度与峰面积存在着良好的线性关系(R2=0.9997),平均回收率为94.17%(相对标准偏差=0.70%,n=9),平均回收率在90.0%~110.0%。该测试方法操作简单,精密度、重现性、回收率均良好,能精确定性定量,适用于医疗器械产品空心纤维血液透析器中BPA溶出量的日常监管检验。 展开更多
关键词 血液透析器 BPA 乙醇/水混合溶液 测试方法
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Distribution and transformation behaviors of heavy metals during liquefaction process of sewage sludge in ethanol-water mixed solvents 被引量:4
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作者 PAN Zi-qian HUANG Hua-jun +4 位作者 ZHOU Chun-fei LAI Fa-ying HE Xiao-wu XIONG Jiang-bo XIAO Xiao-feng 《Journal of Central South University》 SCIE EI CAS CSCD 2019年第10期2771-2784,共14页
Liquefaction of sewage sludge(SS)in ethanol-water cosolvents is a promising process for the preparation of bio-oil/biochar products.Effect of the combined use of ethanol and water on the distribution/transformation be... Liquefaction of sewage sludge(SS)in ethanol-water cosolvents is a promising process for the preparation of bio-oil/biochar products.Effect of the combined use of ethanol and water on the distribution/transformation behaviors of heavy metals(HMs)contained in raw SS is a key issue on the safety and cleanness of above liquefaction process,which is explored in this study.The results show that pure ethanol facilitates the migration of HMs into biochar products.Pure water yields lower percentages of HMs in mobile/bioavailable speciation.Compared with sole solvent treatment,ethanol-water cosolvent causes a random/average effect on the distribution/transformation behaviors of HMs.After liquefaction of SS in pure water,the contamination degree of HMs is mitigated from high level(25.8(contamination factor))in raw SS to considerable grade(13.4)in biochar and the ecological risk is mitigated from moderate risk(164.5(risk index))to low risk(78.8).Liquefaction of SS in pure ethanol makes no difference to the pollution characteristics of HMs.The combined use of ethanol and water presents similar immobilization effects on HMs to pure water treatment.The contamination factor and risk index of HMs in biochars obtained in ethanol-water cosolvent treatment are 13.1-14.6(considerable grade)and 79.3-101.0(low risk),respectively.In order to further control the pollution of HMs,it is preferentially suggested to improve the liquefaction process of SS in ethanol-water mixed solvents by introducing conventional lignocellulosic/algal biomass,also known as co-liquefaction treatment. 展开更多
关键词 sewage sludge LIQUEFACTION ethanol-water cosolvent heavy metals contamination degree ecological risk
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Heat Transfer Properties and Chaotic Analysis of Parallel Type Pulsating Heat Pipe 被引量:2
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作者 史维秀 李惟毅 +1 位作者 潘利生 谈西峰 《Transactions of Tianjin University》 EI CAS 2011年第6期435-439,共5页
The refrigerant mixture of ethanol aqueous was applied to the parallel type pulsating heat pipe (PHP). The operation characteristics of the PHP were analyzed by means of experiment and nonlinear chaotic theory. Moreov... The refrigerant mixture of ethanol aqueous was applied to the parallel type pulsating heat pipe (PHP). The operation characteristics of the PHP were analyzed by means of experiment and nonlinear chaotic theory. Moreover, the relationship between the running state and attractor was described. The results indicate that starting power, stable running power and dry burning transition power are about 64.08 W, 148.68 W and 234.0 W respectively. The cycle and amplitude of PHP initially decrease and then increase with the increasing power. However, the data are welldistributed in a certain range. The running state is in agreement with the attractors, and the changing process for attractors is as follows: the attractors first disperse in the whole phase space, then present mass status, and finally show band distribution. 展开更多
关键词 parallel type pulsating heat pipe ethanol aqueous ATTRACTOR chaotic analysis
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