期刊文献+
共找到7篇文章
< 1 >
每页显示 20 50 100
间硝基苯甲酰亚肼基二硫代碳酸苄酯的合成
1
作者 陈平生 罗书平 +1 位作者 王文静 郑鹛 《应用化工》 CAS CSCD 2003年第4期44-46,共3页
以间硝基苯甲酸为原料,经酯化、取代等多步反应,合成间硝基苯甲酰亚肼基二硫代碳酸苄酯,优化了各步反应条件。结果表明,合成间硝基苯甲酰亚肼基二硫代碳酸苄酯的优化条件为:催化剂浓硫酸用量3g/mol,间硝基苯甲酸甲酯与水合肼的摩尔比为1... 以间硝基苯甲酸为原料,经酯化、取代等多步反应,合成间硝基苯甲酰亚肼基二硫代碳酸苄酯,优化了各步反应条件。结果表明,合成间硝基苯甲酰亚肼基二硫代碳酸苄酯的优化条件为:催化剂浓硫酸用量3g/mol,间硝基苯甲酸甲酯与水合肼的摩尔比为1∶1.15,间硝基苯甲酰肼与二硫化碳、氢氧化钾的物质的量比为1∶1.05∶2.0,滴加二硫化碳的温度为0~5℃,亲核取代反应温度为80℃。产品收率77.3%,产物结构通过红外、核磁和气 质联用进行了表征。 展开更多
关键词 硝基苯甲酰亚肼基碳酸苄酯 硝基苯甲酰肼 硝基苯甲酸甲酯 合成
下载PDF
HLA配型相合母子间移植1例 被引量:3
2
作者 沈建良 罗晖 +2 位作者 杨平地 岑坚 黄友章 《海军总医院学报》 2001年第4期238-239,共2页
本文报告了1例母子间外周血干细胞移植病例。供受者HLA表型完全相合.但供者CMV—IgG(+),IgM(+)。预处理为全身照射(TBI)加环磷酰胺(CY)方案,环孢素A(CSA)加甲氨喋呤(MTX)方案预防GVHD。... 本文报告了1例母子间外周血干细胞移植病例。供受者HLA表型完全相合.但供者CMV—IgG(+),IgM(+)。预处理为全身照射(TBI)加环磷酰胺(CY)方案,环孢素A(CSA)加甲氨喋呤(MTX)方案预防GVHD。输入MNC 3.3×103/kg,CD34+CD38—11.8×106/kg。WBC下降到最低点(0.1×109/L)为移植后第7天,血小板下降到最低点(7×109/L)为第8天。WBC超过1.0×109/L为第19天,血小板达到20×109/L上下为第25天。移植后第30天、58天两次行细胞遗传学检查,结果均为46(X,X)。移植后产生了IV度aGVHD和CMV间质性肺炎,经积极治疗后均得到控制。移植后已近2年,现血象基本正常,有局限性cGVHD表现。仍在服用环胞素A胶囊中。本文对二代间移植的相关问题进行了讨论。 展开更多
关键词 外周血干细胞移植 异基因 HLA相合 二代间 血液疾病 治疗
下载PDF
Synthesis and Characterization of Novel N-doped TiO2 Photocatalyst with Visible Light Active
3
作者 彭峰 刘义 +2 位作者 王红娟 余皓 杨剑 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2010年第4期437-441,I0001,I0002,共7页
A novel N-doped TiO2 (N1-N2-TiO2) with substitutional and interstitial N impurities simultaneously was successfully synthesized. The catalyst was characterized by X-ray diffraction, X-ray photoelectron spectroscopy,... A novel N-doped TiO2 (N1-N2-TiO2) with substitutional and interstitial N impurities simultaneously was successfully synthesized. The catalyst was characterized by X-ray diffraction, X-ray photoelectron spectroscopy, diffuse reflectance spectroscopy, photoluminescence, and electron paramagnetic resonance. The results demonstrated that the nitrogen was substituted for the lattice oxygen atoms, and was also interstitially doped into the TiO2 lattice. The photocatalytic tests indicated that the N1-N2-TiO2 showed the highest photocatalytic activities of all the N-doped TiO2 under visible light, attributing to the synergetic effect of substitutional and interstitial nitrogen of N-doped TiO2. 展开更多
关键词 Nitrogen doped titania PHOTOCATALYSIS X-ray photoelectron spectroscopy Substitutional nitrogen Interstitial nitrogen
下载PDF
寒山寺和寒山寺碑
4
作者 陈浩望 《华夏文化》 1999年第1期39-40,共2页
“月落乌啼霜满天,江枫渔火对愁眠。姑苏城外寒山寺,夜半钟声到客船。”这是唐代诗人张继的一首枫桥夜泊诗,凭着这首诗在后世读者中的辗转传诵,就使枫桥和寒山寺享了大名,并永垂不朽。寒山寺在江苏省吴县西十里的枫桥旁,因此又称... “月落乌啼霜满天,江枫渔火对愁眠。姑苏城外寒山寺,夜半钟声到客船。”这是唐代诗人张继的一首枫桥夜泊诗,凭着这首诗在后世读者中的辗转传诵,就使枫桥和寒山寺享了大名,并永垂不朽。寒山寺在江苏省吴县西十里的枫桥旁,因此又称枫桥寺;始建于梁代天监年间,原名妙... 展开更多
关键词 寒山寺 诗碑 《枫桥夜泊》 江苏省 书画家 文物保护单位 张继 寒山子 二代间 康有为
下载PDF
Design and Analysis of Integrated Predictive Iterative Learning Control for Batch Process Based on Two-dimensional System Theory 被引量:3
5
作者 陈宸 熊智华 钟宜生 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2014年第7期762-768,共7页
Based on the two-dimensional (2D) system theory, an integrated predictive iterative learning control (2D-IPILC) strategy for batch processes is presented. First, the output response and the error transition model ... Based on the two-dimensional (2D) system theory, an integrated predictive iterative learning control (2D-IPILC) strategy for batch processes is presented. First, the output response and the error transition model predictions along the batch index can be calculated analytically due to the 2D Roesser model of the batch process. Then, an integrated framework of combining iterative learning control (ILC) and model predictive control (MPC) is formed reasonably. The output of feedforward ILC is estimated on the basis of the predefined process 2D model. By min- imizing a quadratic objective function, the feedback MPC is introduced to obtain better control performance for tracking problem of batch processes. Simulations on a typical batch reactor demonstrate that the satisfactory tracking performance as well as faster convergence speed can be achieved than traditional proportion type (P- t-we) ILC despite the model error and disturbances. 展开更多
关键词 lterative learning control Model predictive control Integrated control Batch process Two-dimensional systems
下载PDF
Quadric Completion of Operator Partial Matrices (Ⅰ) 被引量:1
6
作者 崔建莲 侯晋川 《Journal of Mathematical Research and Exposition》 CSCD 2000年第3期317-326,共10页
For a given quadric polynomial p(t), the necessary and sufficient conditions are obtained for operator partial matrices of the form (~A C) to be completed to an operator T such that p(T) = 0. Moreover, all such poss... For a given quadric polynomial p(t), the necessary and sufficient conditions are obtained for operator partial matrices of the form (~A C) to be completed to an operator T such that p(T) = 0. Moreover, all such possible completions, if exist, are presented parametrically. 展开更多
关键词 operator matrix completion.
下载PDF
ON THE SECOND GREEDY WEIGHT FOR LINEAR CODES SATISFYING THE FULLRANK CONDITION
7
作者 CHENWende KLOVETorleiv 《Journal of Systems Science & Complexity》 SCIE EI CSCD 2005年第1期55-66,共12页
The maximum of g2-d2 for linear [n, k, d; q] codes C is studied. Here d2 is the smallest size of the support of 2-dimensional subcodes of C and g2 is the smallest size of the support of 2-dimensional subcodes of C whi... The maximum of g2-d2 for linear [n, k, d; q] codes C is studied. Here d2 is the smallest size of the support of 2-dimensional subcodes of C and g2 is the smallest size of the support of 2-dimensional subcodes of C which contains a codeword of weight d. The extra cost to the greedy adversary to get two symbols of information using some algorithm is g2-d2. For codes satisfying the fullrank condition of general dimensions, upper bounds on the maximum of g2-d2 are given. Under some condition we have got code C where g2-d2 reaches the upper bound. 展开更多
关键词 greedy weight linear code BOUNDS
原文传递
上一页 1 下一页 到第
使用帮助 返回顶部