High-pressure phase behavior of supercritical (SC) CO2+ethanol system was investigated at 333.2 K,348.2K, 353.2K, 368.2K, 413.2K and 453.2K and pressure from 2.0MPa to 14.3MPa. The measurement was carried out in a cy...High-pressure phase behavior of supercritical (SC) CO2+ethanol system was investigated at 333.2 K,348.2K, 353.2K, 368.2K, 413.2K and 453.2K and pressure from 2.0MPa to 14.3MPa. The measurement was carried out in a cylindrical autoclave with a moveable piston and a window for adjustment and observation of phase equilibria at given T and p. The samples were taken from two coexisting phases and were analyzed to obtain their compositions. It is shown that the solubility of SC CO2 in ethanol increases drastically with pressures at the given temperature, but the content of ethanol in CO2-rich phase increase faintly.展开更多
A 3 × 3 matrix spectral problem and a Liouville integrable hierarchy are constructed by designing a new subalgebra of loop algebra A^-2. Furthermore, high-order binary symmetry constraints of the corresponding hi...A 3 × 3 matrix spectral problem and a Liouville integrable hierarchy are constructed by designing a new subalgebra of loop algebra A^-2. Furthermore, high-order binary symmetry constraints of the corresponding hierarchy are obtained by using the binary nonlinearization method. Finally, according to another new subalgebra of loop algebra A^-2, its integrable couplings are established.展开更多
Test coverage analysis is a structural testing technique, which helps to evaluate the sufficiency of software testing. This letter presents two test generation algorithms based on binary decision diagrams to produce t...Test coverage analysis is a structural testing technique, which helps to evaluate the sufficiency of software testing. This letter presents two test generation algorithms based on binary decision diagrams to produce tests for the Multiple-Condition Criterion(M-CC) and the Modified Condition/Decision Criterion(MC/DC), and describes the design of the C program Coverage Measurement Tool (CCMT), which can record dynamic behaviors of C programs and quantify test coverage.展开更多
Silica materials are located in various regions of Libya in large quantities and different mining conditions, so the purpose of this study is silica materials in the south-west of the Libyan region Edree in terms of q...Silica materials are located in various regions of Libya in large quantities and different mining conditions, so the purpose of this study is silica materials in the south-west of the Libyan region Edree in terms of quality and the possibility of using in various engineering industries, particularly construction. The results show that the sands of silica presented in Edree area are of a high degree of purity, as the percentage of silicon （SIO2） reached 99.5%, the percentage of impurities was negligible and represented in some chemical elements in different proportions, such as calcium 0.224%, sodium 0.004%, iron 0.0006%, zinc 0.0003%, boron 0.0003%, potassium 0.0001%, manganese 0.0001% and magnesium 0.0001%, making these materials very suitable in the manufacture of all types of glass, crystal and semi-crystalline high-quality without needing any important treatment, as well as its suitability as a refinement in manufacture of templates metal castings in addition to the possibility of use in the manufacture of cement, building materials and as a filler in paint and brick making and sand and concrete elements can also be used in electronic industries. A geological material of silica present in the form of a sequence of layers of clay and thin layers of sand stone and a large stock of high-quality near the surface, making mining operations of the type of surface and reduces the cost of extraction.展开更多
A series of novel pyrazoles compounds were synthesized by the reaction of five kinds of substitute α-bromoacetophenone with pyrazole intermediates which was prepared by the reaction of chalcones and thiosemicarbazone...A series of novel pyrazoles compounds were synthesized by the reaction of five kinds of substitute α-bromoacetophenone with pyrazole intermediates which was prepared by the reaction of chalcones and thiosemicarbazones. This method has some advantages such as mild reaction condition, easy operation and higher yield. All the compounds were confirmed by elemental analysis, IR and 1H NMR.展开更多
文摘High-pressure phase behavior of supercritical (SC) CO2+ethanol system was investigated at 333.2 K,348.2K, 353.2K, 368.2K, 413.2K and 453.2K and pressure from 2.0MPa to 14.3MPa. The measurement was carried out in a cylindrical autoclave with a moveable piston and a window for adjustment and observation of phase equilibria at given T and p. The samples were taken from two coexisting phases and were analyzed to obtain their compositions. It is shown that the solubility of SC CO2 in ethanol increases drastically with pressures at the given temperature, but the content of ethanol in CO2-rich phase increase faintly.
基金supported by China Postdoctoral Science Foundation and National Natural Science Foundation of China under Grant No.10471139
文摘A 3 × 3 matrix spectral problem and a Liouville integrable hierarchy are constructed by designing a new subalgebra of loop algebra A^-2. Furthermore, high-order binary symmetry constraints of the corresponding hierarchy are obtained by using the binary nonlinearization method. Finally, according to another new subalgebra of loop algebra A^-2, its integrable couplings are established.
文摘Test coverage analysis is a structural testing technique, which helps to evaluate the sufficiency of software testing. This letter presents two test generation algorithms based on binary decision diagrams to produce tests for the Multiple-Condition Criterion(M-CC) and the Modified Condition/Decision Criterion(MC/DC), and describes the design of the C program Coverage Measurement Tool (CCMT), which can record dynamic behaviors of C programs and quantify test coverage.
文摘Silica materials are located in various regions of Libya in large quantities and different mining conditions, so the purpose of this study is silica materials in the south-west of the Libyan region Edree in terms of quality and the possibility of using in various engineering industries, particularly construction. The results show that the sands of silica presented in Edree area are of a high degree of purity, as the percentage of silicon （SIO2） reached 99.5%, the percentage of impurities was negligible and represented in some chemical elements in different proportions, such as calcium 0.224%, sodium 0.004%, iron 0.0006%, zinc 0.0003%, boron 0.0003%, potassium 0.0001%, manganese 0.0001% and magnesium 0.0001%, making these materials very suitable in the manufacture of all types of glass, crystal and semi-crystalline high-quality without needing any important treatment, as well as its suitability as a refinement in manufacture of templates metal castings in addition to the possibility of use in the manufacture of cement, building materials and as a filler in paint and brick making and sand and concrete elements can also be used in electronic industries. A geological material of silica present in the form of a sequence of layers of clay and thin layers of sand stone and a large stock of high-quality near the surface, making mining operations of the type of surface and reduces the cost of extraction.
基金The authors are extremely grateful to the National Nature Science Foundation of China for supporting this research （No.20962018, No20862015, No.20762009 and No.20562011）.
文摘A series of novel pyrazoles compounds were synthesized by the reaction of five kinds of substitute α-bromoacetophenone with pyrazole intermediates which was prepared by the reaction of chalcones and thiosemicarbazones. This method has some advantages such as mild reaction condition, easy operation and higher yield. All the compounds were confirmed by elemental analysis, IR and 1H NMR.
