石油焦中硫含量二次标样的制备

本实验由两部分组成。第一部分内容主要是尝试制备用于测定石油焦中硫含量的二次标样,解决了因国内目前还没有石油焦中硫标样为分析带来的困难。还由于采用了二次标样,基本排除了基体对本方法测定结果的影响。本实验在尝试制备二次标样的过程中,用4种测试方法定值。首先对二次标样用方差法进行了均匀性检验。经检验合格后,用定值计算的数据统计方法(包括测定结果的离群值检验、数据分析正态性检验,各方法平均值间一致性检验和等精密度检验)进行定值。第二部分内容主要是使用所制备的二次标样,并用简单、快速的库仑滴定原理设计的快速定硫仪仪器分析替代了操作步骤复杂的管式炉法[1]来分析测定石油焦中硫含量。本方法具有操作简单、测定快速、结果准确及重复性好的优点。本方法基本满足了本公司铝工业用石油焦中硫含量的测定要求。本方法适用范围为0~2.0(m/m)%,方法标准偏差为1.2%。

中国东部地幔氧化—还原状态的演化及其意义

利用二次尖晶石标样法(secondary spinel standard)精确测定了中国东部新生代玄武岩中地幔包体的尖晶石的Fe^(3+)/∑Fe,并采用橄榄石- 斜方辉石- 尖晶石氧逸度计估算了63个地幔包体记录的氧逸度。结果显示,中国东部岩石圈地幔氧化状态具有南高北低特点,其中,华北克位通岩石圈地幔的氧化状态最低,与大洋地幔氧化状态相近。

A matting method based on color distance and differential distance

A new matting algorithm based on color distance and differential distance is proposed to deal with the problem that many matting methods perform poorly with complex natural images.The proposed method combines local sampling with global sampling to select foreground and background pairs for unknown pixels and then a new cost function is constructed based on color distance and differential distance to further optimize the selected sample pairs.Finally,a quadratic objective function is used based on matte Laplacian coming from KNN matting which is added with texture feature.Through experiments on various test images,it is confirmed that the results obtained by the proposed method are more accurate than those obtained by traditional methods.The four-error-metrics comparison on benchmark dataset among several algorithms also proves the effectiveness of the proposed method.