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微波辐射下固相反应合成二苯基甲基醚(英文)
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作者 路建美 纪顺俊 +1 位作者 朱秀林 程振平 《合成化学》 CAS CSCD 2000年第1期87-90,共4页
在常压下用微波辐射固相反应的方法合成了二苯基甲基醚 ,与用有机溶剂为介质及传统的热固相反应方法相比 ,其反应速率快 ,产率高。
关键词 二苯甲酮 二苯基甲基醚 微波辐射 合成 固相反应
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3,5-二氨基-4′-甲基-二苯基醚的合成
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作者 鲁顺保 温祖标 钱勇 《江西师范大学学报(自然科学版)》 CAS 北大核心 2008年第6期653-656,共4页
以3,5-二硝基溴苯与对甲基苯酚为原料,合成出中间产物3,5-二硝基-4′-甲基-二苯基醚,再用钯/碳还原得到3,5-二氨基-4′-甲基-二苯基醚,两步反应的产率分别为81.86%和89.16%.用元素分析、IR和1H-NMR确证了其结构.
关键词 3 5-二氨基-4’-甲基-二苯基 合成 表征
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Pomegranate (Punica granatum L.) Peel Extract as a Source of Natural Antioxidant
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作者 A.Padmaja N.B.L.Prasad 《Journal of Food Science and Engineering》 2011年第3期171-182,共12页
An increase in the demand for natural additives has shifted the attention from synthetic to natural antioxidants. Antioxidative components from pomegranate peel were extracted by using different solvents like methanol... An increase in the demand for natural additives has shifted the attention from synthetic to natural antioxidants. Antioxidative components from pomegranate peel were extracted by using different solvents like methanol, ethanol, acetone, chloroform and ethyl acetate. All the extracts were tested for Total phenolic content (TPC) and the methanol which proved to be best in extracting the phenolic compounds was used to assess the antioxidant property by using different methods like Diphenyl piridyl picryl hydrazyl (DPPH), Relative reducing power (RRP), Beta carotene bleaching and Ferric thiocyanate (FTC). The antioxidant activity (AA) of pomegranate peel extract (PPE) was compared with Butylated hydroxyl toluene (BHT) and Butylated hydroxyl anisole (BHA). The methanolic extract was examined by Liquid Chromatography and Mass Spectroscopy (LCMS) and the spectra showed the presence of different phenolic compounds. The extracts were tested for their efficiency in preventing rancidity of Refined Bleached Deodorized Soybean oil (RBDSBO) in comparison with BHT and control at 200 ppm concentration. The PPE proved to be best in preventing rancidity. Owing to the present results, the studies can further be extended to exploit the PPE for application into different food products. 展开更多
关键词 Pomegranate peel phenolics extraction antioxidant activity soybean oil
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